Pošarac, Milica B.

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Authority KeyName Variants
orcid::0000-0001-7830-8345
  • Pošarac, Milica B. (13)
  • Pošarac-Marković, Milica B. (7)
Projects

Author's Bibliography

Structural and morphological characterization of iron-doped sol-gel derived mullite powders

Ilić, Svetlana M.; Babić, Biljana M.; Bjelajac, Anđelika; Stoimenov, Nikolay; Kljajević, Ljiljana M.; Pošarac-Marković, Milica B.; Matović, Branko

(Elsevier Sci Ltd, Oxford, 2020)

TY  - JOUR
AU  - Ilić, Svetlana M.
AU  - Babić, Biljana M.
AU  - Bjelajac, Anđelika
AU  - Stoimenov, Nikolay
AU  - Kljajević, Ljiljana M.
AU  - Pošarac-Marković, Milica B.
AU  - Matović, Branko
PY  - 2020
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4515
AB  - The structural and morphological properties of iron-doped mullite powders are the subject of the present study. The powders of undoped and iron-doped mullite in the composition range of 3-15 wt% Fe2O3 were synthesized by a combination of sol-gel and combustion methods. The excess of water and urea were introduced in reaction solutions to enhance the copolymerization of aluminum and silicon species. The results of structural characterization revealed that the synthesized mullite powders were amorphous of a hybrid type. The specific surface area of the undoped mullite powder was 262 m(2) g(-1) with a maximum pore radius (d(p)) of 2 nm classifying it into mesoporous materials. The addition of iron has reduced the specific surface area, while the pore size value remained the same except for the sample with 3 wt% Fe2O3 (S-BET = 278 m(2) g(-1); d(p) = 3 nm). The presence of iron caused lowering the temperature of liquid phase formation, while present urea combusted providing the increase of the temperature locally that caused the sintering and formation of agglomerates of smaller particles. However, the results of the particle size analysis are not straightforward. The values of mean volume diameter (D[3,4]) indicated that the particle size increased to 6 wt% Fe2O3 (123.6 mu m), and then decreased and for the sample with 12 wt% Fe2O3, it was equal to 96.6 mu m. Thus, the added iron contributed to the more uniform particle size distribution. The SEM analysis has also shown the coarse powder particles consisted of the coalesced smaller particles.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - Structural and morphological characterization of iron-doped sol-gel derived mullite powders
EP  - 13113
IS  - 9
SP  - 13107
VL  - 46
DO  - 10.1016/j.ceramint.2020.02.083
ER  - 
@article{
author = "Ilić, Svetlana M. and Babić, Biljana M. and Bjelajac, Anđelika and Stoimenov, Nikolay and Kljajević, Ljiljana M. and Pošarac-Marković, Milica B. and Matović, Branko",
year = "2020",
abstract = "The structural and morphological properties of iron-doped mullite powders are the subject of the present study. The powders of undoped and iron-doped mullite in the composition range of 3-15 wt% Fe2O3 were synthesized by a combination of sol-gel and combustion methods. The excess of water and urea were introduced in reaction solutions to enhance the copolymerization of aluminum and silicon species. The results of structural characterization revealed that the synthesized mullite powders were amorphous of a hybrid type. The specific surface area of the undoped mullite powder was 262 m(2) g(-1) with a maximum pore radius (d(p)) of 2 nm classifying it into mesoporous materials. The addition of iron has reduced the specific surface area, while the pore size value remained the same except for the sample with 3 wt% Fe2O3 (S-BET = 278 m(2) g(-1); d(p) = 3 nm). The presence of iron caused lowering the temperature of liquid phase formation, while present urea combusted providing the increase of the temperature locally that caused the sintering and formation of agglomerates of smaller particles. However, the results of the particle size analysis are not straightforward. The values of mean volume diameter (D[3,4]) indicated that the particle size increased to 6 wt% Fe2O3 (123.6 mu m), and then decreased and for the sample with 12 wt% Fe2O3, it was equal to 96.6 mu m. Thus, the added iron contributed to the more uniform particle size distribution. The SEM analysis has also shown the coarse powder particles consisted of the coalesced smaller particles.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "Structural and morphological characterization of iron-doped sol-gel derived mullite powders",
pages = "13113-13107",
number = "9",
volume = "46",
doi = "10.1016/j.ceramint.2020.02.083"
}
Ilić, S. M., Babić, B. M., Bjelajac, A., Stoimenov, N., Kljajević, L. M., Pošarac-Marković, M. B.,& Matović, B.. (2020). Structural and morphological characterization of iron-doped sol-gel derived mullite powders. in Ceramics International
Elsevier Sci Ltd, Oxford., 46(9), 13107-13113.
https://doi.org/10.1016/j.ceramint.2020.02.083
Ilić SM, Babić BM, Bjelajac A, Stoimenov N, Kljajević LM, Pošarac-Marković MB, Matović B. Structural and morphological characterization of iron-doped sol-gel derived mullite powders. in Ceramics International. 2020;46(9):13107-13113.
doi:10.1016/j.ceramint.2020.02.083 .
Ilić, Svetlana M., Babić, Biljana M., Bjelajac, Anđelika, Stoimenov, Nikolay, Kljajević, Ljiljana M., Pošarac-Marković, Milica B., Matović, Branko, "Structural and morphological characterization of iron-doped sol-gel derived mullite powders" in Ceramics International, 46, no. 9 (2020):13107-13113,
https://doi.org/10.1016/j.ceramint.2020.02.083 . .
6
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7

Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit

Cocić, Mira; Matović, Branko; Pošarac, Milica B.; Volkov-Husović, Tatjana; Majstorović, Jelena; Tasić, Visa; Dević, Snežana; Vusović, Nenad

(Međunarodni Institut za nauku o sinterovanju, Beograd, 2017)

TY  - JOUR
AU  - Cocić, Mira
AU  - Matović, Branko
AU  - Pošarac, Milica B.
AU  - Volkov-Husović, Tatjana
AU  - Majstorović, Jelena
AU  - Tasić, Visa
AU  - Dević, Snežana
AU  - Vusović, Nenad
PY  - 2017
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3609
AB  - In this study, the behavior of glass-ceramics synthesized from a glass frit of FFW (Final Flotation Waste) originated from the RTB Bor Company was investigated. Thermal shock resistance was monitored in order to assess the possibility of application of such waste material. Thermal shock of the samples was conducted using water quench test. Image analysis and ultrasonic measurements were used as nondestructive methods for quantification of thermal shock damage at the surface and in the bulk of the specimens. Phase composition of samples was determined by X-ray powder diffraction (XRPD). The degradation level of samples was about 43 % after 20 cycles of water quench tests. The results pointed out that glass-ceramic material exhibited good thermal shock resistance.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit
EP  - 147
IS  - 2
SP  - 139
VL  - 49
DO  - 10.2298/SOS1702139C
ER  - 
@article{
author = "Cocić, Mira and Matović, Branko and Pošarac, Milica B. and Volkov-Husović, Tatjana and Majstorović, Jelena and Tasić, Visa and Dević, Snežana and Vusović, Nenad",
year = "2017",
abstract = "In this study, the behavior of glass-ceramics synthesized from a glass frit of FFW (Final Flotation Waste) originated from the RTB Bor Company was investigated. Thermal shock resistance was monitored in order to assess the possibility of application of such waste material. Thermal shock of the samples was conducted using water quench test. Image analysis and ultrasonic measurements were used as nondestructive methods for quantification of thermal shock damage at the surface and in the bulk of the specimens. Phase composition of samples was determined by X-ray powder diffraction (XRPD). The degradation level of samples was about 43 % after 20 cycles of water quench tests. The results pointed out that glass-ceramic material exhibited good thermal shock resistance.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit",
pages = "147-139",
number = "2",
volume = "49",
doi = "10.2298/SOS1702139C"
}
Cocić, M., Matović, B., Pošarac, M. B., Volkov-Husović, T., Majstorović, J., Tasić, V., Dević, S.,& Vusović, N.. (2017). Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 49(2), 139-147.
https://doi.org/10.2298/SOS1702139C
Cocić M, Matović B, Pošarac MB, Volkov-Husović T, Majstorović J, Tasić V, Dević S, Vusović N. Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit. in Science of Sintering. 2017;49(2):139-147.
doi:10.2298/SOS1702139C .
Cocić, Mira, Matović, Branko, Pošarac, Milica B., Volkov-Husović, Tatjana, Majstorović, Jelena, Tasić, Visa, Dević, Snežana, Vusović, Nenad, "Thermal Shock Properties of Glass-ceramics Synthesized From a Glass Frit" in Science of Sintering, 49, no. 2 (2017):139-147,
https://doi.org/10.2298/SOS1702139C . .
1
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Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material

Pošarac-Marković, Milica B.; Majstorović, Jelena; Devečerski, Aleksandar; Matović, Branko; Volkov-Husović, Tatjana

(Međunarodni Institut za nauku o sinterovanju, Beograd, 2015)

TY  - JOUR
AU  - Pošarac-Marković, Milica B.
AU  - Majstorović, Jelena
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
AU  - Volkov-Husović, Tatjana
PY  - 2015
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3003
AB  - Porous SiC/Cordierite Composite Material with graphite content (10%) was synthesized. Evaluation of Young modulus of elasticity and thermal shock behavior of these samples was presented. Thermal shock behavior was monitored using water quench test, and non destructive methods such are UPVT and image analysis were also used for accompaniment the level of destruction of the samples during water quench test. Based on the level of destruction graphical modeling of critical number of cycles was given. This approach was implemented on discussion of the influence of the graphite content on thermal stability behavior of the samples.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material
EP  - 297
IS  - 3
SP  - 289
VL  - 47
DO  - 10.2298/SOS1503289P
ER  - 
@article{
author = "Pošarac-Marković, Milica B. and Majstorović, Jelena and Devečerski, Aleksandar and Matović, Branko and Volkov-Husović, Tatjana",
year = "2015",
abstract = "Porous SiC/Cordierite Composite Material with graphite content (10%) was synthesized. Evaluation of Young modulus of elasticity and thermal shock behavior of these samples was presented. Thermal shock behavior was monitored using water quench test, and non destructive methods such are UPVT and image analysis were also used for accompaniment the level of destruction of the samples during water quench test. Based on the level of destruction graphical modeling of critical number of cycles was given. This approach was implemented on discussion of the influence of the graphite content on thermal stability behavior of the samples.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material",
pages = "297-289",
number = "3",
volume = "47",
doi = "10.2298/SOS1503289P"
}
Pošarac-Marković, M. B., Majstorović, J., Devečerski, A., Matović, B.,& Volkov-Husović, T.. (2015). Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 47(3), 289-297.
https://doi.org/10.2298/SOS1503289P
Pošarac-Marković MB, Majstorović J, Devečerski A, Matović B, Volkov-Husović T. Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material. in Science of Sintering. 2015;47(3):289-297.
doi:10.2298/SOS1503289P .
Pošarac-Marković, Milica B., Majstorović, Jelena, Devečerski, Aleksandar, Matović, Branko, Volkov-Husović, Tatjana, "Young's Modulus Evaluation and Thermal Shock Behavior of a Porous SiC/cordierite Composite Material" in Science of Sintering, 47, no. 3 (2015):289-297,
https://doi.org/10.2298/SOS1503289P . .
1
1
1

Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content

Pošarac-Marković, Milica B.; Veljović, Đorđe; Devečerski, Aleksandar; Matović, Branko; Volkov-Husović, Tatjana

(Inst Za Kovinske Materiale I In Tehnologie, Ljubjana, 2015)

TY  - JOUR
AU  - Pošarac-Marković, Milica B.
AU  - Veljović, Đorđe
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
AU  - Volkov-Husović, Tatjana
PY  - 2015
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2995
AB  - A cordierite/SiC composite was created in situ with reactive sintering at 1250 degrees C and 1300 degrees C. The cordierite precursor was made from commercially available spinel, alumina and quartz and was mixed with the comercial SiC powder to obtain composite materials during the sintering. It was found that cordierite particles bind efficiently with the SiC powder during sintering and that reactive sintering is an effective way to produce ceramics at a relativly low temperature. The goal of this investigation was to check the possibilities of using the silicon carbide-cordierite composite as a material resistant to the erosive wear. The fluid dynamic system of the experimental methodology was used here to produce ultrasonic erosive wear. Two kinds of SiC/cordierite samples were investigated, KS 50 and KS 30, with different mass contents of cordierite (w = 50 % and w = 30 % of cordierite). The mass loss and the level of surface degradation were measured before and during the experiment. The level of surface degradation of the samples was monitored using the Image-Pro Plus program for the image analysis. It was found that after 150 min the mass loss was below 1.3 mg and the surface degradation was below 7 %. The obtained results indicated that both samples exhibited an excellent erosion resistance during the cavitation experiment.
PB  - Inst Za Kovinske Materiale I In Tehnologie, Ljubjana
T2  - Materiali in Tehnologije
T1  - Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content
EP  - 370
IS  - 3
SP  - 365
VL  - 49
DO  - 10.17222/mit.2014.071
ER  - 
@article{
author = "Pošarac-Marković, Milica B. and Veljović, Đorđe and Devečerski, Aleksandar and Matović, Branko and Volkov-Husović, Tatjana",
year = "2015",
abstract = "A cordierite/SiC composite was created in situ with reactive sintering at 1250 degrees C and 1300 degrees C. The cordierite precursor was made from commercially available spinel, alumina and quartz and was mixed with the comercial SiC powder to obtain composite materials during the sintering. It was found that cordierite particles bind efficiently with the SiC powder during sintering and that reactive sintering is an effective way to produce ceramics at a relativly low temperature. The goal of this investigation was to check the possibilities of using the silicon carbide-cordierite composite as a material resistant to the erosive wear. The fluid dynamic system of the experimental methodology was used here to produce ultrasonic erosive wear. Two kinds of SiC/cordierite samples were investigated, KS 50 and KS 30, with different mass contents of cordierite (w = 50 % and w = 30 % of cordierite). The mass loss and the level of surface degradation were measured before and during the experiment. The level of surface degradation of the samples was monitored using the Image-Pro Plus program for the image analysis. It was found that after 150 min the mass loss was below 1.3 mg and the surface degradation was below 7 %. The obtained results indicated that both samples exhibited an excellent erosion resistance during the cavitation experiment.",
publisher = "Inst Za Kovinske Materiale I In Tehnologie, Ljubjana",
journal = "Materiali in Tehnologije",
title = "Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content",
pages = "370-365",
number = "3",
volume = "49",
doi = "10.17222/mit.2014.071"
}
Pošarac-Marković, M. B., Veljović, Đ., Devečerski, A., Matović, B.,& Volkov-Husović, T.. (2015). Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content. in Materiali in Tehnologije
Inst Za Kovinske Materiale I In Tehnologie, Ljubjana., 49(3), 365-370.
https://doi.org/10.17222/mit.2014.071
Pošarac-Marković MB, Veljović Đ, Devečerski A, Matović B, Volkov-Husović T. Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content. in Materiali in Tehnologije. 2015;49(3):365-370.
doi:10.17222/mit.2014.071 .
Pošarac-Marković, Milica B., Veljović, Đorđe, Devečerski, Aleksandar, Matović, Branko, Volkov-Husović, Tatjana, "Erosive wear resistance of silicon carbide-cordierite ceramics: influence of the cordierite content" in Materiali in Tehnologije, 49, no. 3 (2015):365-370,
https://doi.org/10.17222/mit.2014.071 . .
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4

Sol-gel synthesis and characterization of iron doped mullite

Ilić, Svetlana M.; Zec, Slavica; Miljković, Miroslav; Poleti, Dejan; Pošarac-Marković, Milica B.; Janaćković, Đorđe; Matović, Branko

(Elsevier Science Sa, Lausanne, 2014)

TY  - JOUR
AU  - Ilić, Svetlana M.
AU  - Zec, Slavica
AU  - Miljković, Miroslav
AU  - Poleti, Dejan
AU  - Pošarac-Marković, Milica B.
AU  - Janaćković, Đorđe
AU  - Matović, Branko
PY  - 2014
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2687
AB  - Amorphous powders of iron doped 3:2 mullite (3Al(2)O(3)center dot 2SiO(2)) were prepared by sol-gel combustion process using ethanol-water solutions of Al(III) nitrate, Fe(III) nitrate, TEOS and urea. Compositions up to 15 wt% of Fe2O3 were investigated. After combustion and heat treatment at 800 degrees C for 4 h, XRD analysis confirmed that the powders were amorphous. This is in agreement with the thermodynamic predictions that direct formation of mullite has not occurred during the aluminum nitrate - urea combustion reaction. XRD patterns of uniaxially pressed and sintered pellets at 1550 degrees C for 4 h revealed the crystal structure of orthorhombic mullite. The lattice parameters and unit cell volume increases as the mullite solid solutions were enriched by iron. The TGA/DSC analysis showed the reducing of crystallization temperature of iron doped mullites with increasing of iron content in reaction mixtures. The mullitization reaction is two-step process including formation of transient spinel phase below 1000 degrees C and mullite crystallization at temperatures about 1200 degrees C. The SEM micrographs of the sintered samples reveal elongated mullite grains with grain length up to 40 mu m. Increasing of the iron content in the reaction mixture enhances the grain size and the grains become elongated and better packed increasing the density of sintered samples.
PB  - Elsevier Science Sa, Lausanne
T2  - Journal of Alloys and Compounds
T1  - Sol-gel synthesis and characterization of iron doped mullite
EP  - 264
SP  - 259
VL  - 612
DO  - 10.1016/j.jallcom.2014.05.204
ER  - 
@article{
author = "Ilić, Svetlana M. and Zec, Slavica and Miljković, Miroslav and Poleti, Dejan and Pošarac-Marković, Milica B. and Janaćković, Đorđe and Matović, Branko",
year = "2014",
abstract = "Amorphous powders of iron doped 3:2 mullite (3Al(2)O(3)center dot 2SiO(2)) were prepared by sol-gel combustion process using ethanol-water solutions of Al(III) nitrate, Fe(III) nitrate, TEOS and urea. Compositions up to 15 wt% of Fe2O3 were investigated. After combustion and heat treatment at 800 degrees C for 4 h, XRD analysis confirmed that the powders were amorphous. This is in agreement with the thermodynamic predictions that direct formation of mullite has not occurred during the aluminum nitrate - urea combustion reaction. XRD patterns of uniaxially pressed and sintered pellets at 1550 degrees C for 4 h revealed the crystal structure of orthorhombic mullite. The lattice parameters and unit cell volume increases as the mullite solid solutions were enriched by iron. The TGA/DSC analysis showed the reducing of crystallization temperature of iron doped mullites with increasing of iron content in reaction mixtures. The mullitization reaction is two-step process including formation of transient spinel phase below 1000 degrees C and mullite crystallization at temperatures about 1200 degrees C. The SEM micrographs of the sintered samples reveal elongated mullite grains with grain length up to 40 mu m. Increasing of the iron content in the reaction mixture enhances the grain size and the grains become elongated and better packed increasing the density of sintered samples.",
publisher = "Elsevier Science Sa, Lausanne",
journal = "Journal of Alloys and Compounds",
title = "Sol-gel synthesis and characterization of iron doped mullite",
pages = "264-259",
volume = "612",
doi = "10.1016/j.jallcom.2014.05.204"
}
Ilić, S. M., Zec, S., Miljković, M., Poleti, D., Pošarac-Marković, M. B., Janaćković, Đ.,& Matović, B.. (2014). Sol-gel synthesis and characterization of iron doped mullite. in Journal of Alloys and Compounds
Elsevier Science Sa, Lausanne., 612, 259-264.
https://doi.org/10.1016/j.jallcom.2014.05.204
Ilić SM, Zec S, Miljković M, Poleti D, Pošarac-Marković MB, Janaćković Đ, Matović B. Sol-gel synthesis and characterization of iron doped mullite. in Journal of Alloys and Compounds. 2014;612:259-264.
doi:10.1016/j.jallcom.2014.05.204 .
Ilić, Svetlana M., Zec, Slavica, Miljković, Miroslav, Poleti, Dejan, Pošarac-Marković, Milica B., Janaćković, Đorđe, Matović, Branko, "Sol-gel synthesis and characterization of iron doped mullite" in Journal of Alloys and Compounds, 612 (2014):259-264,
https://doi.org/10.1016/j.jallcom.2014.05.204 . .
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26

Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development

Krsmanović, Radenka; Antić, Željka; Milićević, Bojana R.; Pošarac-Marković, Milica B.; Janaćković, Đorđe; Dramićanin, Miroslav; Brik, Mikhail G.; Steins, Ints; Veljović, Đorđe

(Elsevier Sci Ltd, Oxford, 2014)

TY  - JOUR
AU  - Krsmanović, Radenka
AU  - Antić, Željka
AU  - Milićević, Bojana R.
AU  - Pošarac-Marković, Milica B.
AU  - Janaćković, Đorđe
AU  - Dramićanin, Miroslav
AU  - Brik, Mikhail G.
AU  - Steins, Ints
AU  - Veljović, Đorđe
PY  - 2014
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2857
AB  - Using Spark Plasma Sintering it is possible to produce polycrystalline ceramics of very fine microstructure and good mechanical properties. This work presents the fabrication of such ceramics using Eu3+-doped (Y0.7Gd0.3)(2)O-3 nanopowder as a starting material. We monitored the changes in the morphology of ceramic samples and their consolidation with additional thermal treatments at 650 degrees C and 1100 degrees C. The ceramics grain size remained in the sub-micron domain, even when elevated temperatures were used for annealing. The best results were obtained for the sample sintered at 1100 degrees C for 20 min, which had the smallest grain size, theoretical density, and the most intensive photoluminescence, along with the maximum hardness and appropriate fracture toughness. The Judd-Ofelt intensity parameters and branching ratios were calculated, taking into account the difference in the effective refractive index for the nanopowder and ceramic samples.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development
EP  - 8862
IS  - 6
SP  - 8853
VL  - 40
DO  - 10.1016/j.ceramint.2014.01.108
ER  - 
@article{
author = "Krsmanović, Radenka and Antić, Željka and Milićević, Bojana R. and Pošarac-Marković, Milica B. and Janaćković, Đorđe and Dramićanin, Miroslav and Brik, Mikhail G. and Steins, Ints and Veljović, Đorđe",
year = "2014",
abstract = "Using Spark Plasma Sintering it is possible to produce polycrystalline ceramics of very fine microstructure and good mechanical properties. This work presents the fabrication of such ceramics using Eu3+-doped (Y0.7Gd0.3)(2)O-3 nanopowder as a starting material. We monitored the changes in the morphology of ceramic samples and their consolidation with additional thermal treatments at 650 degrees C and 1100 degrees C. The ceramics grain size remained in the sub-micron domain, even when elevated temperatures were used for annealing. The best results were obtained for the sample sintered at 1100 degrees C for 20 min, which had the smallest grain size, theoretical density, and the most intensive photoluminescence, along with the maximum hardness and appropriate fracture toughness. The Judd-Ofelt intensity parameters and branching ratios were calculated, taking into account the difference in the effective refractive index for the nanopowder and ceramic samples.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development",
pages = "8862-8853",
number = "6",
volume = "40",
doi = "10.1016/j.ceramint.2014.01.108"
}
Krsmanović, R., Antić, Ž., Milićević, B. R., Pošarac-Marković, M. B., Janaćković, Đ., Dramićanin, M., Brik, M. G., Steins, I.,& Veljović, Đ.. (2014). Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development. in Ceramics International
Elsevier Sci Ltd, Oxford., 40(6), 8853-8862.
https://doi.org/10.1016/j.ceramint.2014.01.108
Krsmanović R, Antić Ž, Milićević BR, Pošarac-Marković MB, Janaćković Đ, Dramićanin M, Brik MG, Steins I, Veljović Đ. Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development. in Ceramics International. 2014;40(6):8853-8862.
doi:10.1016/j.ceramint.2014.01.108 .
Krsmanović, Radenka, Antić, Željka, Milićević, Bojana R., Pošarac-Marković, Milica B., Janaćković, Đorđe, Dramićanin, Miroslav, Brik, Mikhail G., Steins, Ints, Veljović, Đorđe, "Polycrystalline (Y0.7Gd0.3)(2)O-3:Eu3+ ceramics fabricated by Spark Plasma Sintering: Densification and microstructure development" in Ceramics International, 40, no. 6 (2014):8853-8862,
https://doi.org/10.1016/j.ceramint.2014.01.108 . .
11
10
12

Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear

Pošarac-Marković, Milica B.; Veljović, Đorđe; Devečerski, Aleksandar; Matović, Branko; Volkov-Husović, Tatjana

(Elsevier Sci Ltd, Oxford, 2013)

TY  - JOUR
AU  - Pošarac-Marković, Milica B.
AU  - Veljović, Đorđe
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
AU  - Volkov-Husović, Tatjana
PY  - 2013
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2393
AB  - Covalent bond in SiC ceramic request high temperature for its sintering. In order to put down sintering temperature of SiC ceramics we choose cordierite as phase between SiC particles. Reactive sintering is an effective way to produce ceramics at relatively low temperature. We have created in situ SiC/cordierite composite at 1250 degrees C. Cordierite precursor was made from commercially available spinel, alumina and quartz. The possibilities of using silicon carbide-cordierite material as resistant to the erosive wear was goal of this investigation. The fluid dynamic system of the experimental methodology was used here to produce ultrasonic erosive wear. Mass loss and level of degradation were measured before and during the experiment. Level of degradation of the samples was monitored using Image Pro Plus program for image analysis. Average erosion ring diameter as well as average erosion area were monitored during experiment. Obtained results pointed out that after 150 min sample exhibited excellent erosion resistance compared to metal and ceramic samples.
PB  - Elsevier Sci Ltd, Oxford
T2  - Materials & Design
T1  - Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear
EP  - 299
SP  - 295
VL  - 52
DO  - 10.1016/j.matdes.2013.05.053
ER  - 
@article{
author = "Pošarac-Marković, Milica B. and Veljović, Đorđe and Devečerski, Aleksandar and Matović, Branko and Volkov-Husović, Tatjana",
year = "2013",
abstract = "Covalent bond in SiC ceramic request high temperature for its sintering. In order to put down sintering temperature of SiC ceramics we choose cordierite as phase between SiC particles. Reactive sintering is an effective way to produce ceramics at relatively low temperature. We have created in situ SiC/cordierite composite at 1250 degrees C. Cordierite precursor was made from commercially available spinel, alumina and quartz. The possibilities of using silicon carbide-cordierite material as resistant to the erosive wear was goal of this investigation. The fluid dynamic system of the experimental methodology was used here to produce ultrasonic erosive wear. Mass loss and level of degradation were measured before and during the experiment. Level of degradation of the samples was monitored using Image Pro Plus program for image analysis. Average erosion ring diameter as well as average erosion area were monitored during experiment. Obtained results pointed out that after 150 min sample exhibited excellent erosion resistance compared to metal and ceramic samples.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Materials & Design",
title = "Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear",
pages = "299-295",
volume = "52",
doi = "10.1016/j.matdes.2013.05.053"
}
Pošarac-Marković, M. B., Veljović, Đ., Devečerski, A., Matović, B.,& Volkov-Husović, T.. (2013). Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear. in Materials & Design
Elsevier Sci Ltd, Oxford., 52, 295-299.
https://doi.org/10.1016/j.matdes.2013.05.053
Pošarac-Marković MB, Veljović Đ, Devečerski A, Matović B, Volkov-Husović T. Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear. in Materials & Design. 2013;52:295-299.
doi:10.1016/j.matdes.2013.05.053 .
Pošarac-Marković, Milica B., Veljović, Đorđe, Devečerski, Aleksandar, Matović, Branko, Volkov-Husović, Tatjana, "Nondestructive evaluation of surface degradation of silicon carbide-cordierite ceramics subjected to the erosive wear" in Materials & Design, 52 (2013):295-299,
https://doi.org/10.1016/j.matdes.2013.05.053 . .
7
9

Mechanical properties correlation to processing parameters for advanced alumina based refractories

Dimitrijević, Marija; Veljović, Đorđe; Pošarac-Marković, Milica B.; Jančić-Heinemann, Radmila; Volkov-Husović, Tatjana; Zrilić, Milorad

(International Institute for the Science of Sintering, Beograd, 2012)

TY  - JOUR
AU  - Dimitrijević, Marija
AU  - Veljović, Đorđe
AU  - Pošarac-Marković, Milica B.
AU  - Jančić-Heinemann, Radmila
AU  - Volkov-Husović, Tatjana
AU  - Zrilić, Milorad
PY  - 2012
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2053
AB  - Alumina based refractories are usually used in metallurgical furnaces and their thermal shock resistance is of great importance. In order to improve thermal shock resistance and mechanical properties of alumina based refractories short ceramic fibers were added to the material. SEM technique was used to compare the microstructure of specimens and the observed images gave the porosity and morphological characteristics of pores in the specimens. Standard compression test was used to determine the modulus of elasticity and compression strength. Results obtained from thermal shock testing and mechanical properties measurements were used to establish regression models that correlated specimen properties to process parameters.
AB  - Aluminozni vatrostalni materijali najčešće se koriste u pećima u metalurškom inženjerstvu gde je od izuzetne važnosti njihova termostabilnost (otpornost na termošok). U cilju poboljšavanja termostabilnosti i mehaničkih svojstava ove grupe materijala dodavana su kratka keramička vlakna. Karakterizacija mikrostrukture uzoraka određena je skening elektronskom mikroskopijom (SEM), a rezultati su korišćeni radi poređenja poroznosti i morfoloških karakteristika posmatranih uzoraka. Korišćena je standardna laboratorijska metoda određivanja čvrstoće i Jungovog modula elastičnosti. Dobijeni rezultati vezani za termostabilnost i mehanička svojstva poslužila su za formiranje modela koji povezuje svojstva uzorka sa procesnim parametrima.
PB  - International Institute for the Science of Sintering, Beograd
T2  - Science of Sintering
T1  - Mechanical properties correlation to processing parameters for advanced alumina based refractories
EP  - 33
IS  - 1
SP  - 25
VL  - 44
UR  - https://hdl.handle.net/21.15107/rcub_technorep_2053
ER  - 
@article{
author = "Dimitrijević, Marija and Veljović, Đorđe and Pošarac-Marković, Milica B. and Jančić-Heinemann, Radmila and Volkov-Husović, Tatjana and Zrilić, Milorad",
year = "2012",
abstract = "Alumina based refractories are usually used in metallurgical furnaces and their thermal shock resistance is of great importance. In order to improve thermal shock resistance and mechanical properties of alumina based refractories short ceramic fibers were added to the material. SEM technique was used to compare the microstructure of specimens and the observed images gave the porosity and morphological characteristics of pores in the specimens. Standard compression test was used to determine the modulus of elasticity and compression strength. Results obtained from thermal shock testing and mechanical properties measurements were used to establish regression models that correlated specimen properties to process parameters., Aluminozni vatrostalni materijali najčešće se koriste u pećima u metalurškom inženjerstvu gde je od izuzetne važnosti njihova termostabilnost (otpornost na termošok). U cilju poboljšavanja termostabilnosti i mehaničkih svojstava ove grupe materijala dodavana su kratka keramička vlakna. Karakterizacija mikrostrukture uzoraka određena je skening elektronskom mikroskopijom (SEM), a rezultati su korišćeni radi poređenja poroznosti i morfoloških karakteristika posmatranih uzoraka. Korišćena je standardna laboratorijska metoda određivanja čvrstoće i Jungovog modula elastičnosti. Dobijeni rezultati vezani za termostabilnost i mehanička svojstva poslužila su za formiranje modela koji povezuje svojstva uzorka sa procesnim parametrima.",
publisher = "International Institute for the Science of Sintering, Beograd",
journal = "Science of Sintering",
title = "Mechanical properties correlation to processing parameters for advanced alumina based refractories",
pages = "33-25",
number = "1",
volume = "44",
url = "https://hdl.handle.net/21.15107/rcub_technorep_2053"
}
Dimitrijević, M., Veljović, Đ., Pošarac-Marković, M. B., Jančić-Heinemann, R., Volkov-Husović, T.,& Zrilić, M.. (2012). Mechanical properties correlation to processing parameters for advanced alumina based refractories. in Science of Sintering
International Institute for the Science of Sintering, Beograd., 44(1), 25-33.
https://hdl.handle.net/21.15107/rcub_technorep_2053
Dimitrijević M, Veljović Đ, Pošarac-Marković MB, Jančić-Heinemann R, Volkov-Husović T, Zrilić M. Mechanical properties correlation to processing parameters for advanced alumina based refractories. in Science of Sintering. 2012;44(1):25-33.
https://hdl.handle.net/21.15107/rcub_technorep_2053 .
Dimitrijević, Marija, Veljović, Đorđe, Pošarac-Marković, Milica B., Jančić-Heinemann, Radmila, Volkov-Husović, Tatjana, Zrilić, Milorad, "Mechanical properties correlation to processing parameters for advanced alumina based refractories" in Science of Sintering, 44, no. 1 (2012):25-33,
https://hdl.handle.net/21.15107/rcub_technorep_2053 .
12
13

SiC synthesis using natural Mg-silicates

Devečerski, Aleksandar; Pošarac, Milica B.; Dimitrijević, M.; Rosić, M.; Volkov-Husović, Tatjana; Branković, Goran

(International Institute for the Science of Sintering, Beograd, 2012)

TY  - JOUR
AU  - Devečerski, Aleksandar
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Rosić, M.
AU  - Volkov-Husović, Tatjana
AU  - Branković, Goran
PY  - 2012
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2047
AB  - The silicon carbide powders are prepared by carbothermal reduction of domestic mineral resources (white and brown sepiolite), at relatively low temperatures (1200 - 1600oC). Carbothermal reduction process is greatly influenced by chemical composition of sepiolites and type of carbon used. Obtained SiC powders consist of fine β-SiC particles and did not retain the fibrous morphology of sepiolites. Catalytical influence of Fe is attributed to formation of iron-silicide and its potentionaly important role in removal of Mg-species, i.e. reduction of Mg2SiO4 and MgO into Mg(g).
AB  - Silicijum karbidni (SiC) prahovi su sintetisani metodom karbotermalne redukcije na relativno niskim temperaturama (1200-1600oS). Kao polazna sirovina odnosno izvor silicijuma, korišćene su domaće mineralne sirovine (beli sepiolit i braon sepiolit). Ustanovljeno je da i hemijski sastav sepiolita i tip korišćenog ugljenika (redukciono sredstvo), veoma utiču na sam proces karbotermalne redukcije. Dobijeni silicijum karbidni prahovi se sastoje od finih čestica beta silicijum karbida i nisu zadržali vlaknastu morfologiju polaznih sirovina tj. sepiolita. Opaženi katalitički uticaj gvožđa (Fe) je pripisan formiranju gvožđe silicida i njihovoj ulozi u olakšanom uklanjanju magnezijumovih jedinjenja (Mg2SiO4 i MgO), tj. redukciji istih u gasoviti magnezijum - Mg(g ).
PB  - International Institute for the Science of Sintering, Beograd
T2  - Science of Sintering
T1  - SiC synthesis using natural Mg-silicates
EP  - 94
IS  - 1
SP  - 81
VL  - 44
UR  - https://hdl.handle.net/21.15107/rcub_technorep_2047
ER  - 
@article{
author = "Devečerski, Aleksandar and Pošarac, Milica B. and Dimitrijević, M. and Rosić, M. and Volkov-Husović, Tatjana and Branković, Goran",
year = "2012",
abstract = "The silicon carbide powders are prepared by carbothermal reduction of domestic mineral resources (white and brown sepiolite), at relatively low temperatures (1200 - 1600oC). Carbothermal reduction process is greatly influenced by chemical composition of sepiolites and type of carbon used. Obtained SiC powders consist of fine β-SiC particles and did not retain the fibrous morphology of sepiolites. Catalytical influence of Fe is attributed to formation of iron-silicide and its potentionaly important role in removal of Mg-species, i.e. reduction of Mg2SiO4 and MgO into Mg(g)., Silicijum karbidni (SiC) prahovi su sintetisani metodom karbotermalne redukcije na relativno niskim temperaturama (1200-1600oS). Kao polazna sirovina odnosno izvor silicijuma, korišćene su domaće mineralne sirovine (beli sepiolit i braon sepiolit). Ustanovljeno je da i hemijski sastav sepiolita i tip korišćenog ugljenika (redukciono sredstvo), veoma utiču na sam proces karbotermalne redukcije. Dobijeni silicijum karbidni prahovi se sastoje od finih čestica beta silicijum karbida i nisu zadržali vlaknastu morfologiju polaznih sirovina tj. sepiolita. Opaženi katalitički uticaj gvožđa (Fe) je pripisan formiranju gvožđe silicida i njihovoj ulozi u olakšanom uklanjanju magnezijumovih jedinjenja (Mg2SiO4 i MgO), tj. redukciji istih u gasoviti magnezijum - Mg(g ).",
publisher = "International Institute for the Science of Sintering, Beograd",
journal = "Science of Sintering",
title = "SiC synthesis using natural Mg-silicates",
pages = "94-81",
number = "1",
volume = "44",
url = "https://hdl.handle.net/21.15107/rcub_technorep_2047"
}
Devečerski, A., Pošarac, M. B., Dimitrijević, M., Rosić, M., Volkov-Husović, T.,& Branković, G.. (2012). SiC synthesis using natural Mg-silicates. in Science of Sintering
International Institute for the Science of Sintering, Beograd., 44(1), 81-94.
https://hdl.handle.net/21.15107/rcub_technorep_2047
Devečerski A, Pošarac MB, Dimitrijević M, Rosić M, Volkov-Husović T, Branković G. SiC synthesis using natural Mg-silicates. in Science of Sintering. 2012;44(1):81-94.
https://hdl.handle.net/21.15107/rcub_technorep_2047 .
Devečerski, Aleksandar, Pošarac, Milica B., Dimitrijević, M., Rosić, M., Volkov-Husović, Tatjana, Branković, Goran, "SiC synthesis using natural Mg-silicates" in Science of Sintering, 44, no. 1 (2012):81-94,
https://hdl.handle.net/21.15107/rcub_technorep_2047 .
1
1

Mechanical properties of biomorphic silicon carbide ceramics

Gordić, Milan V.; Babić, Biljana M.; Stašić, J.M.; Trtica, M.S.; Volkov-Husović, Tatjana; Pošarac, Milica B.; Matović, Branko

(International Institute for the Science of Sintering, Beograd, 2011)

TY  - JOUR
AU  - Gordić, Milan V.
AU  - Babić, Biljana M.
AU  - Stašić, J.M.
AU  - Trtica, M.S.
AU  - Volkov-Husović, Tatjana
AU  - Pošarac, Milica B.
AU  - Matović, Branko
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1841
AB  - Biomorphous β-SiC ceramics were produced from linden wood by impregnation with tetraethyl orthosilicate (TEOS), followed pyrolysis and high temperature treatment at 1580°C. Six specimen groups included charcoal and five groups with different number of impregnation were analyzed. Flexural and compressional strength of charcoal and woodlike SiC ceramic were characterized using three-point and compression testing. Mechanicall properties increased slightly with number of impregnation cycles. Ultrasonic pulse velocity testing (UPVT) was used to determine dynamic young modulus of elasticity. Laser surface modification was studied by interaction with Nd:YAG laser, operating at 1064 or 532 nm wavelengthss and pulse duration of 150 ps.
AB  - Biomorfna keramika β-SiC je dobijena od karbonizovane lipe uz impregnaciju tetraetil ortosilikatom (TEOS), sa karbotermalnom redukcijom na 1580°C. Ispitivano je šest grupa uzoraka - karbonizovano drvo i pet grupa biomorfnog SiC sa različitim brojem impregnacija. Čvrstoće na savijanje i kompresiju karbonizovanog drveta i biomorfnog SiC je merena primenom metoda savijanja u tri tačke i testiranja kompresije. Mehanička svojstva su se postepeno poboljšavala sa brojem ciklusa impregnacije. Određivanje dinamičkog modula elastičnosti je vršeno pomoću merenja brzine ultrazvučnih impulsa (UPVT). Za proučavanje površinske interakcije sa laserskim zračenjem korišćen je Nd:YAG laser koji je emitovao zračenje na talasnim dužinama 1064 i 532 nm i trajanjem impulsa 150 ps.
PB  - International Institute for the Science of Sintering, Beograd
T2  - Science of Sintering
T1  - Mechanical properties of biomorphic silicon carbide ceramics
EP  - 223
IS  - 2
SP  - 215
VL  - 43
UR  - https://hdl.handle.net/21.15107/rcub_technorep_1841
ER  - 
@article{
author = "Gordić, Milan V. and Babić, Biljana M. and Stašić, J.M. and Trtica, M.S. and Volkov-Husović, Tatjana and Pošarac, Milica B. and Matović, Branko",
year = "2011",
abstract = "Biomorphous β-SiC ceramics were produced from linden wood by impregnation with tetraethyl orthosilicate (TEOS), followed pyrolysis and high temperature treatment at 1580°C. Six specimen groups included charcoal and five groups with different number of impregnation were analyzed. Flexural and compressional strength of charcoal and woodlike SiC ceramic were characterized using three-point and compression testing. Mechanicall properties increased slightly with number of impregnation cycles. Ultrasonic pulse velocity testing (UPVT) was used to determine dynamic young modulus of elasticity. Laser surface modification was studied by interaction with Nd:YAG laser, operating at 1064 or 532 nm wavelengthss and pulse duration of 150 ps., Biomorfna keramika β-SiC je dobijena od karbonizovane lipe uz impregnaciju tetraetil ortosilikatom (TEOS), sa karbotermalnom redukcijom na 1580°C. Ispitivano je šest grupa uzoraka - karbonizovano drvo i pet grupa biomorfnog SiC sa različitim brojem impregnacija. Čvrstoće na savijanje i kompresiju karbonizovanog drveta i biomorfnog SiC je merena primenom metoda savijanja u tri tačke i testiranja kompresije. Mehanička svojstva su se postepeno poboljšavala sa brojem ciklusa impregnacije. Određivanje dinamičkog modula elastičnosti je vršeno pomoću merenja brzine ultrazvučnih impulsa (UPVT). Za proučavanje površinske interakcije sa laserskim zračenjem korišćen je Nd:YAG laser koji je emitovao zračenje na talasnim dužinama 1064 i 532 nm i trajanjem impulsa 150 ps.",
publisher = "International Institute for the Science of Sintering, Beograd",
journal = "Science of Sintering",
title = "Mechanical properties of biomorphic silicon carbide ceramics",
pages = "223-215",
number = "2",
volume = "43",
url = "https://hdl.handle.net/21.15107/rcub_technorep_1841"
}
Gordić, M. V., Babić, B. M., Stašić, J.M., Trtica, M.S., Volkov-Husović, T., Pošarac, M. B.,& Matović, B.. (2011). Mechanical properties of biomorphic silicon carbide ceramics. in Science of Sintering
International Institute for the Science of Sintering, Beograd., 43(2), 215-223.
https://hdl.handle.net/21.15107/rcub_technorep_1841
Gordić MV, Babić BM, Stašić J, Trtica M, Volkov-Husović T, Pošarac MB, Matović B. Mechanical properties of biomorphic silicon carbide ceramics. in Science of Sintering. 2011;43(2):215-223.
https://hdl.handle.net/21.15107/rcub_technorep_1841 .
Gordić, Milan V., Babić, Biljana M., Stašić, J.M., Trtica, M.S., Volkov-Husović, Tatjana, Pošarac, Milica B., Matović, Branko, "Mechanical properties of biomorphic silicon carbide ceramics" in Science of Sintering, 43, no. 2 (2011):215-223,
https://hdl.handle.net/21.15107/rcub_technorep_1841 .
1
5

Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock

Dimitrijević, Marija; Jančić-Heinemann, Radmila; Volkov-Husović, Tatjana; Pošarac, Milica B.; Majstorović, Jelena

(Elsevier Science Bv, Amsterdam, 2011)

TY  - JOUR
AU  - Dimitrijević, Marija
AU  - Jančić-Heinemann, Radmila
AU  - Volkov-Husović, Tatjana
AU  - Pošarac, Milica B.
AU  - Majstorović, Jelena
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1880
AB  - Thermal stability of the alumina based samples were measured using the water immersion test. Mechanical characteristics such as strength, dynamic modulus of elasticity resulting from resonance frequency measurements were considered. Image analysis was used to measure the fiber lengths distribution, homogeneity of fiber distribution in the matrix and finally the measurement and characterization of surface degradation of specimens during thermal stability testing. The morphology of resulting surface destruction was analyzed using mathematical morphology tools.
PB  - Elsevier Science Bv, Amsterdam
T2  - 11th International Conference on the Mechanical Behavior of Materials (ICM11)
T1  - Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock
VL  - 10
DO  - 10.1016/j.proeng.2011.04.356
ER  - 
@article{
author = "Dimitrijević, Marija and Jančić-Heinemann, Radmila and Volkov-Husović, Tatjana and Pošarac, Milica B. and Majstorović, Jelena",
year = "2011",
abstract = "Thermal stability of the alumina based samples were measured using the water immersion test. Mechanical characteristics such as strength, dynamic modulus of elasticity resulting from resonance frequency measurements were considered. Image analysis was used to measure the fiber lengths distribution, homogeneity of fiber distribution in the matrix and finally the measurement and characterization of surface degradation of specimens during thermal stability testing. The morphology of resulting surface destruction was analyzed using mathematical morphology tools.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "11th International Conference on the Mechanical Behavior of Materials (ICM11)",
title = "Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock",
volume = "10",
doi = "10.1016/j.proeng.2011.04.356"
}
Dimitrijević, M., Jančić-Heinemann, R., Volkov-Husović, T., Pošarac, M. B.,& Majstorović, J.. (2011). Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock. in 11th International Conference on the Mechanical Behavior of Materials (ICM11)
Elsevier Science Bv, Amsterdam., 10.
https://doi.org/10.1016/j.proeng.2011.04.356
Dimitrijević M, Jančić-Heinemann R, Volkov-Husović T, Pošarac MB, Majstorović J. Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock. in 11th International Conference on the Mechanical Behavior of Materials (ICM11). 2011;10.
doi:10.1016/j.proeng.2011.04.356 .
Dimitrijević, Marija, Jančić-Heinemann, Radmila, Volkov-Husović, Tatjana, Pošarac, Milica B., Majstorović, Jelena, "Morphological analysis of surface degradation of advanced alumina based refactories subjected to thermal shock" in 11th International Conference on the Mechanical Behavior of Materials (ICM11), 10 (2011),
https://doi.org/10.1016/j.proeng.2011.04.356 . .
2
4
3

SiC synthesis using domestic mineral resources

Devečerski, Aleksandar; Pošarac, Milica B.; Egelja, Adela; Rosić, Milena; Volkov-Husović, Tatjana; Matović, Branko

(University of Novi Sad, 2011)

TY  - JOUR
AU  - Devečerski, Aleksandar
AU  - Pošarac, Milica B.
AU  - Egelja, Adela
AU  - Rosić, Milena
AU  - Volkov-Husović, Tatjana
AU  - Matović, Branko
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1825
AB  - The possibility of using domestic Mg-silicate (sepiolite, white) as Si source and novolac resin (as carbon source), for synthesis of fine β-SiC powder at relatively low temperatures (1673-1873 K), was demonstrated. Obtained SiC powders consist of fine β-SiC particles and did not retain the fibrous morphology of starting sepiolites. Carbothermal reduction process, which was used in this study, is greatly influenced by catalyst addition (FeCl3, FeSi). In order to obtain pure SiC powders, it is necessary to completely remove all Mg-species, and catalytic influence of Fe is attributed to FeSi important role in reduction of Mg2SiO4 and MgO into Mg(g). Formation of SiC whiskers is observed only in samples with Fe introduced in form of iron-silicide (FeSi).
PB  - University of Novi Sad
T2  - Processing and Application of Ceramics
T1  - SiC synthesis using domestic mineral resources
EP  - 67
IS  - 2
SP  - 63
VL  - 5
UR  - https://hdl.handle.net/21.15107/rcub_technorep_1825
ER  - 
@article{
author = "Devečerski, Aleksandar and Pošarac, Milica B. and Egelja, Adela and Rosić, Milena and Volkov-Husović, Tatjana and Matović, Branko",
year = "2011",
abstract = "The possibility of using domestic Mg-silicate (sepiolite, white) as Si source and novolac resin (as carbon source), for synthesis of fine β-SiC powder at relatively low temperatures (1673-1873 K), was demonstrated. Obtained SiC powders consist of fine β-SiC particles and did not retain the fibrous morphology of starting sepiolites. Carbothermal reduction process, which was used in this study, is greatly influenced by catalyst addition (FeCl3, FeSi). In order to obtain pure SiC powders, it is necessary to completely remove all Mg-species, and catalytic influence of Fe is attributed to FeSi important role in reduction of Mg2SiO4 and MgO into Mg(g). Formation of SiC whiskers is observed only in samples with Fe introduced in form of iron-silicide (FeSi).",
publisher = "University of Novi Sad",
journal = "Processing and Application of Ceramics",
title = "SiC synthesis using domestic mineral resources",
pages = "67-63",
number = "2",
volume = "5",
url = "https://hdl.handle.net/21.15107/rcub_technorep_1825"
}
Devečerski, A., Pošarac, M. B., Egelja, A., Rosić, M., Volkov-Husović, T.,& Matović, B.. (2011). SiC synthesis using domestic mineral resources. in Processing and Application of Ceramics
University of Novi Sad., 5(2), 63-67.
https://hdl.handle.net/21.15107/rcub_technorep_1825
Devečerski A, Pošarac MB, Egelja A, Rosić M, Volkov-Husović T, Matović B. SiC synthesis using domestic mineral resources. in Processing and Application of Ceramics. 2011;5(2):63-67.
https://hdl.handle.net/21.15107/rcub_technorep_1825 .
Devečerski, Aleksandar, Pošarac, Milica B., Egelja, Adela, Rosić, Milena, Volkov-Husović, Tatjana, Matović, Branko, "SiC synthesis using domestic mineral resources" in Processing and Application of Ceramics, 5, no. 2 (2011):63-67,
https://hdl.handle.net/21.15107/rcub_technorep_1825 .

Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock

Pošarac, Milica B.; Dimitrijević, M.; Majstorović, Jelena; Volkov-Husović, Tatjana; Matović, Branko

(Taylor & Francis Inc, Philadelphia, 2010)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Majstorović, Jelena
AU  - Volkov-Husović, Tatjana
AU  - Matović, Branko
PY  - 2010
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1681
AB  - Two different types cordierite/silicon carbide composite ceramic materials (KS 50 and KZ 50) were used for this investigation. Both materials were exposed to the water quench test from 950 degrees C, applying various numbers of thermal cycles. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore, measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of ultrasonic velocity technique and image analysis for simple and reliable nondestructive methods of characterization was presented in this investigation. It was found that both composite materials exhibit good thermal shock resistance.
PB  - Taylor & Francis Inc, Philadelphia
T2  - Research in Nondestructive Evaluation
T1  - Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock
EP  - 59
IS  - 1
SP  - 48
VL  - 21
DO  - 10.1080/09349840903381044
ER  - 
@article{
author = "Pošarac, Milica B. and Dimitrijević, M. and Majstorović, Jelena and Volkov-Husović, Tatjana and Matović, Branko",
year = "2010",
abstract = "Two different types cordierite/silicon carbide composite ceramic materials (KS 50 and KZ 50) were used for this investigation. Both materials were exposed to the water quench test from 950 degrees C, applying various numbers of thermal cycles. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore, measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of ultrasonic velocity technique and image analysis for simple and reliable nondestructive methods of characterization was presented in this investigation. It was found that both composite materials exhibit good thermal shock resistance.",
publisher = "Taylor & Francis Inc, Philadelphia",
journal = "Research in Nondestructive Evaluation",
title = "Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock",
pages = "59-48",
number = "1",
volume = "21",
doi = "10.1080/09349840903381044"
}
Pošarac, M. B., Dimitrijević, M., Majstorović, J., Volkov-Husović, T.,& Matović, B.. (2010). Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock. in Research in Nondestructive Evaluation
Taylor & Francis Inc, Philadelphia., 21(1), 48-59.
https://doi.org/10.1080/09349840903381044
Pošarac MB, Dimitrijević M, Majstorović J, Volkov-Husović T, Matović B. Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock. in Research in Nondestructive Evaluation. 2010;21(1):48-59.
doi:10.1080/09349840903381044 .
Pošarac, Milica B., Dimitrijević, M., Majstorović, Jelena, Volkov-Husović, Tatjana, Matović, Branko, "Nondestructive testing of thermal shock resistance of cordierite/silicon carbide composite materials after cyclic thermal shock" in Research in Nondestructive Evaluation, 21, no. 1 (2010):48-59,
https://doi.org/10.1080/09349840903381044 . .
2
3
3

The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel

Pošarac, Milica B.; Devečerski, Aleksandar; Volkov-Husović, Tatjana; Matović, Branko; Minić, Dragica M.

(International Institute for the Science of Sintering, Beograd, 2009)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Devečerski, Aleksandar
AU  - Volkov-Husović, Tatjana
AU  - Matović, Branko
AU  - Minić, Dragica M.
PY  - 2009
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1459
AB  - The effect of yttria additive on the thermal shock behavior of magnesium aluminate spinel has been investigated. As a starting material we used spinel (MgAl2O4) obtained by the modified glycine nitrate procedure (MGNP). Sintered products were characterized in terms of phase analysis, densities, thermal shock, monitoring the damaged surface area in the refractory specimen during thermal shock and ultrasonic determination of the Dynamic Young modulus of elasticity. It was found that a new phase between yttria and alumina is formed, which improved thermal shock properties of the spinel refractories. Also densification of samples is enhanced by yttria addition.
AB  - U ovom radu je ispitivana otpornost spinela, MgAl2O4, prema termošoku u prisustvu Y2O3 kao aditiva. Kao polazni materijal korišćen je spinel dobijen modifikovanom glicin-nitratnom metodom. Analiza sinterovanih uzoraka podrazumevala je određivanje faznog sastava, praćenje oštećenja površine uzoraka usled termošoka, određivanje dinamičkog Jungovog (Young) modula elastičnosti ultrazvučnom metodom. Nađeno je da reakcijom spinela sa Y2O3 dolazi do formiranja nove faze koja poboljšava otpornost spinelne keramike prema termošoku. Takođe je utvrđen pozitivan uticaj dodatka Y2O3 na densifikaciju spinelne keramike.
PB  - International Institute for the Science of Sintering, Beograd
T2  - Science of Sintering
T1  - The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel
EP  - 81
IS  - 1
SP  - 75
VL  - 41
UR  - https://hdl.handle.net/21.15107/rcub_technorep_1459
ER  - 
@article{
author = "Pošarac, Milica B. and Devečerski, Aleksandar and Volkov-Husović, Tatjana and Matović, Branko and Minić, Dragica M.",
year = "2009",
abstract = "The effect of yttria additive on the thermal shock behavior of magnesium aluminate spinel has been investigated. As a starting material we used spinel (MgAl2O4) obtained by the modified glycine nitrate procedure (MGNP). Sintered products were characterized in terms of phase analysis, densities, thermal shock, monitoring the damaged surface area in the refractory specimen during thermal shock and ultrasonic determination of the Dynamic Young modulus of elasticity. It was found that a new phase between yttria and alumina is formed, which improved thermal shock properties of the spinel refractories. Also densification of samples is enhanced by yttria addition., U ovom radu je ispitivana otpornost spinela, MgAl2O4, prema termošoku u prisustvu Y2O3 kao aditiva. Kao polazni materijal korišćen je spinel dobijen modifikovanom glicin-nitratnom metodom. Analiza sinterovanih uzoraka podrazumevala je određivanje faznog sastava, praćenje oštećenja površine uzoraka usled termošoka, određivanje dinamičkog Jungovog (Young) modula elastičnosti ultrazvučnom metodom. Nađeno je da reakcijom spinela sa Y2O3 dolazi do formiranja nove faze koja poboljšava otpornost spinelne keramike prema termošoku. Takođe je utvrđen pozitivan uticaj dodatka Y2O3 na densifikaciju spinelne keramike.",
publisher = "International Institute for the Science of Sintering, Beograd",
journal = "Science of Sintering",
title = "The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel",
pages = "81-75",
number = "1",
volume = "41",
url = "https://hdl.handle.net/21.15107/rcub_technorep_1459"
}
Pošarac, M. B., Devečerski, A., Volkov-Husović, T., Matović, B.,& Minić, D. M.. (2009). The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel. in Science of Sintering
International Institute for the Science of Sintering, Beograd., 41(1), 75-81.
https://hdl.handle.net/21.15107/rcub_technorep_1459
Pošarac MB, Devečerski A, Volkov-Husović T, Matović B, Minić DM. The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel. in Science of Sintering. 2009;41(1):75-81.
https://hdl.handle.net/21.15107/rcub_technorep_1459 .
Pošarac, Milica B., Devečerski, Aleksandar, Volkov-Husović, Tatjana, Matović, Branko, Minić, Dragica M., "The effect of Y2O3 addition on thermal shock behavior of magnesium aluminate spinel" in Science of Sintering, 41, no. 1 (2009):75-81,
https://hdl.handle.net/21.15107/rcub_technorep_1459 .
21
33

Behavior of silicon carbide/cordierite composite material after cyclic thermal shock

Dimitrijević, M.; Pošarac, Milica B.; Majstorović, Jelena; Volkov-Husović, Tatjana; Matović, Branko

(Elsevier Sci Ltd, Oxford, 2009)

TY  - JOUR
AU  - Dimitrijević, M.
AU  - Pošarac, Milica B.
AU  - Majstorović, Jelena
AU  - Volkov-Husović, Tatjana
AU  - Matović, Branko
PY  - 2009
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1482
AB  - In the present work Mg-exchanged zeolite and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 30:70. Samples were exposed to the water quench test from 950 degrees C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore by measuring these properties one can directly monitor the development of thermal shock damage level. Dynamic Young's modulus of elasticity and strength degradation were calculated using measured values. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of non-destructive test methods such as: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive characterization are presented.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - Behavior of silicon carbide/cordierite composite material after cyclic thermal shock
EP  - 1081
IS  - 3
SP  - 1077
VL  - 35
DO  - 10.1016/j.ceramint.2008.04.029
ER  - 
@article{
author = "Dimitrijević, M. and Pošarac, Milica B. and Majstorović, Jelena and Volkov-Husović, Tatjana and Matović, Branko",
year = "2009",
abstract = "In the present work Mg-exchanged zeolite and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 30:70. Samples were exposed to the water quench test from 950 degrees C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore by measuring these properties one can directly monitor the development of thermal shock damage level. Dynamic Young's modulus of elasticity and strength degradation were calculated using measured values. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of non-destructive test methods such as: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive characterization are presented.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "Behavior of silicon carbide/cordierite composite material after cyclic thermal shock",
pages = "1081-1077",
number = "3",
volume = "35",
doi = "10.1016/j.ceramint.2008.04.029"
}
Dimitrijević, M., Pošarac, M. B., Majstorović, J., Volkov-Husović, T.,& Matović, B.. (2009). Behavior of silicon carbide/cordierite composite material after cyclic thermal shock. in Ceramics International
Elsevier Sci Ltd, Oxford., 35(3), 1077-1081.
https://doi.org/10.1016/j.ceramint.2008.04.029
Dimitrijević M, Pošarac MB, Majstorović J, Volkov-Husović T, Matović B. Behavior of silicon carbide/cordierite composite material after cyclic thermal shock. in Ceramics International. 2009;35(3):1077-1081.
doi:10.1016/j.ceramint.2008.04.029 .
Dimitrijević, M., Pošarac, Milica B., Majstorović, Jelena, Volkov-Husović, Tatjana, Matović, Branko, "Behavior of silicon carbide/cordierite composite material after cyclic thermal shock" in Ceramics International, 35, no. 3 (2009):1077-1081,
https://doi.org/10.1016/j.ceramint.2008.04.029 . .
22
23
32

The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens

Pošarac, Milica B.; Dimitrijević, M.; Volkov-Husović, Tatjana; Maistorović, J.; Matović, Branko

(Elsevier Sci Ltd, Oxford, 2009)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Volkov-Husović, Tatjana
AU  - Maistorović, J.
AU  - Matović, Branko
PY  - 2009
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1436
AB  - In the present work, Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 50:50. Samples were exposed to the water quench test from 950 degrees C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored using Image Pro Plus program for image analysis. The capability of non-destructive test methods such are: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive methods of characterization were presented in this paper.
PB  - Elsevier Sci Ltd, Oxford
T2  - Materials & Design
T1  - The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens
EP  - 3343
IS  - 8
SP  - 3338
VL  - 30
DO  - 10.1016/j.matdes.2008.11.017
ER  - 
@article{
author = "Pošarac, Milica B. and Dimitrijević, M. and Volkov-Husović, Tatjana and Maistorović, J. and Matović, Branko",
year = "2009",
abstract = "In the present work, Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 50:50. Samples were exposed to the water quench test from 950 degrees C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored using Image Pro Plus program for image analysis. The capability of non-destructive test methods such are: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive methods of characterization were presented in this paper.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Materials & Design",
title = "The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens",
pages = "3343-3338",
number = "8",
volume = "30",
doi = "10.1016/j.matdes.2008.11.017"
}
Pošarac, M. B., Dimitrijević, M., Volkov-Husović, T., Maistorović, J.,& Matović, B.. (2009). The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens. in Materials & Design
Elsevier Sci Ltd, Oxford., 30(8), 3338-3343.
https://doi.org/10.1016/j.matdes.2008.11.017
Pošarac MB, Dimitrijević M, Volkov-Husović T, Maistorović J, Matović B. The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens. in Materials & Design. 2009;30(8):3338-3343.
doi:10.1016/j.matdes.2008.11.017 .
Pošarac, Milica B., Dimitrijević, M., Volkov-Husović, Tatjana, Maistorović, J., Matović, Branko, "The ultrasonic and image analysis method for non-destructive quantification of the thermal shock damage in refractory specimens" in Materials & Design, 30, no. 8 (2009):3338-3343,
https://doi.org/10.1016/j.matdes.2008.11.017 . .
12
12
17

Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock

Pošarac, Milica B.; Dimitrijević, M.; Volkov-Husović, Tatjana; Egelja, Adela; Devečerski, Aleksandar; Matović, Branko

(Natl Inst Optoelectronics, Bucharest-Magurele, 2008)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Volkov-Husović, Tatjana
AU  - Egelja, Adela
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
PY  - 2008
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1313
AB  - In this paper composite material made from silicium carbide and cordierite was used in experiments. Behavior of the material in conditions of rapid temperature changes was investigated. Modified water quench test was applied to determine thermal stability behavior of the samples. Image analysis was used to monitored level of surface deterioration before and during quenching. Ultrasonic measurements were used for determination of dynamic Young modulus of elasticity and strength degradation during quenching. Obtained results are used for analysis of the behavior of the samples in conditions of rapid temperature changes and method for the improvement of the thermal stability behavior.
PB  - Natl Inst Optoelectronics, Bucharest-Magurele
T2  - Journal of Optoelectronics and Advanced Materials
T1  - Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock
EP  - 886
IS  - 4
SP  - 883
VL  - 10
UR  - https://hdl.handle.net/21.15107/rcub_vinar_6750
ER  - 
@article{
author = "Pošarac, Milica B. and Dimitrijević, M. and Volkov-Husović, Tatjana and Egelja, Adela and Devečerski, Aleksandar and Matović, Branko",
year = "2008",
abstract = "In this paper composite material made from silicium carbide and cordierite was used in experiments. Behavior of the material in conditions of rapid temperature changes was investigated. Modified water quench test was applied to determine thermal stability behavior of the samples. Image analysis was used to monitored level of surface deterioration before and during quenching. Ultrasonic measurements were used for determination of dynamic Young modulus of elasticity and strength degradation during quenching. Obtained results are used for analysis of the behavior of the samples in conditions of rapid temperature changes and method for the improvement of the thermal stability behavior.",
publisher = "Natl Inst Optoelectronics, Bucharest-Magurele",
journal = "Journal of Optoelectronics and Advanced Materials",
title = "Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock",
pages = "886-883",
number = "4",
volume = "10",
url = "https://hdl.handle.net/21.15107/rcub_vinar_6750"
}
Pošarac, M. B., Dimitrijević, M., Volkov-Husović, T., Egelja, A., Devečerski, A.,& Matović, B.. (2008). Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock. in Journal of Optoelectronics and Advanced Materials
Natl Inst Optoelectronics, Bucharest-Magurele., 10(4), 883-886.
https://hdl.handle.net/21.15107/rcub_vinar_6750
Pošarac MB, Dimitrijević M, Volkov-Husović T, Egelja A, Devečerski A, Matović B. Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock. in Journal of Optoelectronics and Advanced Materials. 2008;10(4):883-886.
https://hdl.handle.net/21.15107/rcub_vinar_6750 .
Pošarac, Milica B., Dimitrijević, M., Volkov-Husović, Tatjana, Egelja, Adela, Devečerski, Aleksandar, Matović, Branko, "Thermal stability of cordierite/silicon carbide composites after cyclic thermal shock" in Journal of Optoelectronics and Advanced Materials, 10, no. 4 (2008):883-886,
https://hdl.handle.net/21.15107/rcub_vinar_6750 .
3

Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods

Pošarac, Milica B.; Dimitrijević, M.; Volkov-Husović, Tatjana; Devečerski, Aleksandar; Matović, Branko

(Elsevier Sci Ltd, Oxford, 2008)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Volkov-Husović, Tatjana
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
PY  - 2008
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1308
AB  - In the present work Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 30:70 and 50:50. Behavior of composite ceramics after thermal shock treatments was investigated. Thermal shock of the samples was measured using standard laboratory procedure, water quench test (JUS.B.D8.319.). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as nondestructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of ultrasonic velocity technique and image analysis for simple, and reliable nondestructive methods of characterization are presented in this investigation. It was found that both composite materials exhibit good thermal shock resistance.
PB  - Elsevier Sci Ltd, Oxford
T2  - Journal of the European Ceramic Society
T1  - Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods
EP  - 1278
IS  - 6
SP  - 1275
VL  - 28
DO  - 10.1016/j.jeurceramsoc.2007.09.038
ER  - 
@article{
author = "Pošarac, Milica B. and Dimitrijević, M. and Volkov-Husović, Tatjana and Devečerski, Aleksandar and Matović, Branko",
year = "2008",
abstract = "In the present work Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 30:70 and 50:50. Behavior of composite ceramics after thermal shock treatments was investigated. Thermal shock of the samples was measured using standard laboratory procedure, water quench test (JUS.B.D8.319.). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as nondestructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of ultrasonic velocity technique and image analysis for simple, and reliable nondestructive methods of characterization are presented in this investigation. It was found that both composite materials exhibit good thermal shock resistance.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Journal of the European Ceramic Society",
title = "Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods",
pages = "1278-1275",
number = "6",
volume = "28",
doi = "10.1016/j.jeurceramsoc.2007.09.038"
}
Pošarac, M. B., Dimitrijević, M., Volkov-Husović, T., Devečerski, A.,& Matović, B.. (2008). Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods. in Journal of the European Ceramic Society
Elsevier Sci Ltd, Oxford., 28(6), 1275-1278.
https://doi.org/10.1016/j.jeurceramsoc.2007.09.038
Pošarac MB, Dimitrijević M, Volkov-Husović T, Devečerski A, Matović B. Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods. in Journal of the European Ceramic Society. 2008;28(6):1275-1278.
doi:10.1016/j.jeurceramsoc.2007.09.038 .
Pošarac, Milica B., Dimitrijević, M., Volkov-Husović, Tatjana, Devečerski, Aleksandar, Matović, Branko, "Determination of thermal shock resistance of silicon carbide/cordierite composite material using nondestructive test methods" in Journal of the European Ceramic Society, 28, no. 6 (2008):1275-1278,
https://doi.org/10.1016/j.jeurceramsoc.2007.09.038 . .
27
28
33

Thermal shock damage characterization of high temperature ceramics by non destructive test methods

Dimitrijević, Marija; Pošarac, Milica B.; Majstorović, Jelena; Volkov-Husović, Tatjana; Devečerski, Aleksandar; Matović, Branko

(University of Chemistry and Technology, Prague, 2008)

TY  - JOUR
AU  - Dimitrijević, Marija
AU  - Pošarac, Milica B.
AU  - Majstorović, Jelena
AU  - Volkov-Husović, Tatjana
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
PY  - 2008
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1211
AB  - In the present work a mixture of commercially available spinel, quartz (SiO2) and alumina (Al2O3) corresponding to cordierite stoichiometry was used as starting material for obtaining cordierite/SiC composite ceramics with weight ratio 30:70 and 50:50. Cordierite and silicon carbide are ceramic materials suitable for high temperature application with superior thermal shock resistance, low thermal expansion coefficient and good chemical resistance. The composite material could exhibit advantages of its constituents when the components have optimized properties and they are mixed in the proper ratio. Behavior of composite ceramics after thermal shock treatments was investigated. Thermal shock of quenching was monitored by image analysis. Ultrasonic measurements were used as non-destrusctive before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements.
PB  - University of Chemistry and Technology, Prague
T2  - Ceramics - Silikaty
T1  - Thermal shock damage characterization of high temperature ceramics by non destructive test methods
EP  - 119
IS  - 2
SP  - 115
VL  - 52
UR  - https://hdl.handle.net/21.15107/rcub_vinar_3522
ER  - 
@article{
author = "Dimitrijević, Marija and Pošarac, Milica B. and Majstorović, Jelena and Volkov-Husović, Tatjana and Devečerski, Aleksandar and Matović, Branko",
year = "2008",
abstract = "In the present work a mixture of commercially available spinel, quartz (SiO2) and alumina (Al2O3) corresponding to cordierite stoichiometry was used as starting material for obtaining cordierite/SiC composite ceramics with weight ratio 30:70 and 50:50. Cordierite and silicon carbide are ceramic materials suitable for high temperature application with superior thermal shock resistance, low thermal expansion coefficient and good chemical resistance. The composite material could exhibit advantages of its constituents when the components have optimized properties and they are mixed in the proper ratio. Behavior of composite ceramics after thermal shock treatments was investigated. Thermal shock of quenching was monitored by image analysis. Ultrasonic measurements were used as non-destrusctive before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements.",
publisher = "University of Chemistry and Technology, Prague",
journal = "Ceramics - Silikaty",
title = "Thermal shock damage characterization of high temperature ceramics by non destructive test methods",
pages = "119-115",
number = "2",
volume = "52",
url = "https://hdl.handle.net/21.15107/rcub_vinar_3522"
}
Dimitrijević, M., Pošarac, M. B., Majstorović, J., Volkov-Husović, T., Devečerski, A.,& Matović, B.. (2008). Thermal shock damage characterization of high temperature ceramics by non destructive test methods. in Ceramics - Silikaty
University of Chemistry and Technology, Prague., 52(2), 115-119.
https://hdl.handle.net/21.15107/rcub_vinar_3522
Dimitrijević M, Pošarac MB, Majstorović J, Volkov-Husović T, Devečerski A, Matović B. Thermal shock damage characterization of high temperature ceramics by non destructive test methods. in Ceramics - Silikaty. 2008;52(2):115-119.
https://hdl.handle.net/21.15107/rcub_vinar_3522 .
Dimitrijević, Marija, Pošarac, Milica B., Majstorović, Jelena, Volkov-Husović, Tatjana, Devečerski, Aleksandar, Matović, Branko, "Thermal shock damage characterization of high temperature ceramics by non destructive test methods" in Ceramics - Silikaty, 52, no. 2 (2008):115-119,
https://hdl.handle.net/21.15107/rcub_vinar_3522 .
9
16

An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material

Pošarac, Milica B.; Dimitrijević, M.; Majstorović, Jelena; Volkov-Husović, Tatjana; Devečerski, Aleksandar; Matović, Branko

(Savez inženjera metalurgije Srbije, Beograd, 2007)

TY  - JOUR
AU  - Pošarac, Milica B.
AU  - Dimitrijević, M.
AU  - Majstorović, Jelena
AU  - Volkov-Husović, Tatjana
AU  - Devečerski, Aleksandar
AU  - Matović, Branko
PY  - 2007
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1043
AB  - In the present work Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 50:50. Samples were exposed to the water quench test from 950°C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of non-destructive test methods such are: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive methods of characterization were presented in this investigation.
PB  - Savez inženjera metalurgije Srbije, Beograd
T2  - Metalurgija
T1  - An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material
EP  - 211
IS  - 3
SP  - 203
VL  - 13
UR  - https://hdl.handle.net/21.15107/rcub_technorep_1043
ER  - 
@article{
author = "Pošarac, Milica B. and Dimitrijević, M. and Majstorović, Jelena and Volkov-Husović, Tatjana and Devečerski, Aleksandar and Matović, Branko",
year = "2007",
abstract = "In the present work Mg-exchanged zeolit and silicon carbide were used as starting materials for obtaining cordierite/SiC composite ceramics with weight ratio 50:50. Samples were exposed to the water quench test from 950°C, applying various number of thermal cycles (shocks). Level of surface deterioration before and during quenching was monitored by image analysis. Ultrasonic measurements were used as non-destructive quantification of thermal shock damage in refractory specimens. When refractory samples are subjected to the rapid temperature changes crack nucleation and propagation occurs resulting in loss of strength and materials degradation. The formation of cracks decreases the density and elastic properties of material. Therefore measuring these properties can directly monitor the development of thermal shock damage level. Dynamic Young modulus of elasticity and strength degradation were calculated using measured values of ultrasonic velocities obtained by ultrasonic measurements. Level of degradation of the samples was monitored before and during testing using Image Pro Plus program for image analysis. The capability of non-destructive test methods such are: ultrasonic velocity technique and image analysis for simple, and reliable non-destructive methods of characterization were presented in this investigation.",
publisher = "Savez inženjera metalurgije Srbije, Beograd",
journal = "Metalurgija",
title = "An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material",
pages = "211-203",
number = "3",
volume = "13",
url = "https://hdl.handle.net/21.15107/rcub_technorep_1043"
}
Pošarac, M. B., Dimitrijević, M., Majstorović, J., Volkov-Husović, T., Devečerski, A.,& Matović, B.. (2007). An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material. in Metalurgija
Savez inženjera metalurgije Srbije, Beograd., 13(3), 203-211.
https://hdl.handle.net/21.15107/rcub_technorep_1043
Pošarac MB, Dimitrijević M, Majstorović J, Volkov-Husović T, Devečerski A, Matović B. An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material. in Metalurgija. 2007;13(3):203-211.
https://hdl.handle.net/21.15107/rcub_technorep_1043 .
Pošarac, Milica B., Dimitrijević, M., Majstorović, Jelena, Volkov-Husović, Tatjana, Devečerski, Aleksandar, Matović, Branko, "An improved method for thermal stability behavior characterization of silicon carbide/cordierite composite material" in Metalurgija, 13, no. 3 (2007):203-211,
https://hdl.handle.net/21.15107/rcub_technorep_1043 .