TY  - JOUR
AU  - Zabukovec-Logar, Nataša
AU  - Mali, Gregor
AU  - Rajić, Nevenka
AU  - Jevtić, Sanja
AU  - Rangus, Mojca
AU  - Golobić, Amalija
AU  - Kaučič, Venčeslav
PY  - 2010
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1699
AB  - A single-crystal X-ray diffraction analysis of an open-framework aluminophosphate ULM-3 Al prepared by 3-methylaminopropylamine (MAPA) as structure-directing agent revealed an orthorhombic Pcab symmetry (a=9.9949(4)angstrom, b=15.8229(7)angstrom, c=18.1963(5)angstrom, R=0.0648, Z=8, unit cell formula (Al24P24O96F16 center dot C32H112N16]). which differs from the Pbc2(1) symmetry of the structural analogue prepared in the presence of 1,4-diaminobutane. The Al-27, P-31, F-19, C-13 and H-1 NMR investigations, which were performed to study in detail MAPA arrangement inside the framework as well as the interactions of MAPA with the aluminophosphate host, confirmed the crystal symmetry and the proposed hydrogen bonding scheme between the template and the framework.
PB  - Academic Press Inc Elsevier Science, San Diego
T2  - Journal of Solid State Chemistry
T1  - Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine
EP  - 1062
IS  - 5
SP  - 1055
VL  - 183
DO  - 10.1016/j.jssc.2010.02.020
ER  - 

@article{
author = "Zabukovec-Logar, Nataša and Mali, Gregor and Rajić, Nevenka and Jevtić, Sanja and Rangus, Mojca and Golobić, Amalija and Kaučič, Venčeslav",
year = "2010",
abstract = "A single-crystal X-ray diffraction analysis of an open-framework aluminophosphate ULM-3 Al prepared by 3-methylaminopropylamine (MAPA) as structure-directing agent revealed an orthorhombic Pcab symmetry (a=9.9949(4)angstrom, b=15.8229(7)angstrom, c=18.1963(5)angstrom, R=0.0648, Z=8, unit cell formula (Al24P24O96F16 center dot C32H112N16]). which differs from the Pbc2(1) symmetry of the structural analogue prepared in the presence of 1,4-diaminobutane. The Al-27, P-31, F-19, C-13 and H-1 NMR investigations, which were performed to study in detail MAPA arrangement inside the framework as well as the interactions of MAPA with the aluminophosphate host, confirmed the crystal symmetry and the proposed hydrogen bonding scheme between the template and the framework.",
publisher = "Academic Press Inc Elsevier Science, San Diego",
journal = "Journal of Solid State Chemistry",
title = "Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine",
pages = "1062-1055",
number = "5",
volume = "183",
doi = "10.1016/j.jssc.2010.02.020"
}

Zabukovec-Logar, N., Mali, G., Rajić, N., Jevtić, S., Rangus, M., Golobić, A.,& Kaučič, V.. (2010). Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine. in Journal of Solid State Chemistry
Academic Press Inc Elsevier Science, San Diego., 183(5), 1055-1062.
https://doi.org/10.1016/j.jssc.2010.02.020

Zabukovec-Logar N, Mali G, Rajić N, Jevtić S, Rangus M, Golobić A, Kaučič V. Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine. in Journal of Solid State Chemistry. 2010;183(5):1055-1062.
doi:10.1016/j.jssc.2010.02.020 .

Zabukovec-Logar, Nataša, Mali, Gregor, Rajić, Nevenka, Jevtić, Sanja, Rangus, Mojca, Golobić, Amalija, Kaučič, Venčeslav, "Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine" in Journal of Solid State Chemistry, 183, no. 5 (2010):1055-1062,
https://doi.org/10.1016/j.jssc.2010.02.020 . .

TY  - JOUR
AU  - Zabukovec-Logar, Nataša
AU  - Rajić, Nevenka
AU  - Stojaković, D.
AU  - Golobić, Amalija
AU  - Kaučič, Venčeslav
PY  - 2005
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/726
AB  - A new 2D zinc phosphate [H3NCH(CH3)CH 2NH3]2+0.75[COOH(CH 2)COOH]0.25 (Zn3P3O 11OH)2-* 0.5NH4+ consists of zinc phosphate layers, which are intercalated by diprotonated 1,2-diaminopropane, malonic acid, and NH4+ ions. The inorganic layers are composed of alternating ZnO4 and PO4 (PO3OH) tetrahedra that form 8-membered ring apertures. The intercalated species strongly interact with the zinc phosphate layers through hydrogen bonds, which is a key factor in stabilizing the structure. Crystal data: monoclinic, P21/a, a = 8.3457(1) Å, b = 16.8953(3) Å, c = 10.1817(2) Å, β = 95.3121(8)°, Z = 4, R = 0.0423.
T2  - Pure and Applied Chemistry
T1  - Synthesis and single-crystal structure analysis of a new layered zinc phosphate
EP  - 1717
IS  - 10
SP  - 1707
VL  - 77
DO  - 10.1351/pac200577101707
ER  - 

@article{
author = "Zabukovec-Logar, Nataša and Rajić, Nevenka and Stojaković, D. and Golobić, Amalija and Kaučič, Venčeslav",
year = "2005",
abstract = "A new 2D zinc phosphate [H3NCH(CH3)CH 2NH3]2+0.75[COOH(CH 2)COOH]0.25 (Zn3P3O 11OH)2-* 0.5NH4+ consists of zinc phosphate layers, which are intercalated by diprotonated 1,2-diaminopropane, malonic acid, and NH4+ ions. The inorganic layers are composed of alternating ZnO4 and PO4 (PO3OH) tetrahedra that form 8-membered ring apertures. The intercalated species strongly interact with the zinc phosphate layers through hydrogen bonds, which is a key factor in stabilizing the structure. Crystal data: monoclinic, P21/a, a = 8.3457(1) Å, b = 16.8953(3) Å, c = 10.1817(2) Å, β = 95.3121(8)°, Z = 4, R = 0.0423.",
journal = "Pure and Applied Chemistry",
title = "Synthesis and single-crystal structure analysis of a new layered zinc phosphate",
pages = "1717-1707",
number = "10",
volume = "77",
doi = "10.1351/pac200577101707"
}

Zabukovec-Logar, N., Rajić, N., Stojaković, D., Golobić, A.,& Kaučič, V.. (2005). Synthesis and single-crystal structure analysis of a new layered zinc phosphate. in Pure and Applied Chemistry, 77(10), 1707-1717.
https://doi.org/10.1351/pac200577101707

Zabukovec-Logar N, Rajić N, Stojaković D, Golobić A, Kaučič V. Synthesis and single-crystal structure analysis of a new layered zinc phosphate. in Pure and Applied Chemistry. 2005;77(10):1707-1717.
doi:10.1351/pac200577101707 .

Zabukovec-Logar, Nataša, Rajić, Nevenka, Stojaković, D., Golobić, Amalija, Kaučič, Venčeslav, "Synthesis and single-crystal structure analysis of a new layered zinc phosphate" in Pure and Applied Chemistry, 77, no. 10 (2005):1707-1717,
https://doi.org/10.1351/pac200577101707 . .

TY  - JOUR
AU  - Zabukovec-Logar, Nataša
AU  - Rajić, Nevenka
AU  - Stojaković, D.
AU  - Sajić, Sanja
AU  - Golobić, Amalija
AU  - Kaučič, Venčeslav
PY  - 2005
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/784
AB  - The title compound, catena-poly[[N-methylpropane-1,3diaminium [mu-phosphato-(mu-hydrogen phosphato)(mu-dihydrogen phosphato) dizincate(II)]], {(C4H14N2)[Zn-2(PO4)(HPO4)(H2PO4)]}(n), consists of macroanionic [Zn-2(PO4)(HPO4)(H2PO4)](2-) layers and intercalated (C4H12N2)(2+) cations. The layers are built up from ZnO4 and PO4/HPO4/H2PO4 tetrahedra that result in small channels of approximate diameter 3.7 angstrom within the layers. Framework-to-framework O - H center dot center dot center dot O and template-to-framework N - H center dot center dot center dot O hydrogen bonds are important in stabilizing the structure.
PB  - Int Union Crystallography, Chester
T2  - Acta Crystallographica Section E-Crystallographic Communications
T1  - (C4H12N2)[Zn-2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalated N-methylpropane-1,3-diaminium cations
EP  - M1356
SP  - M1354
VL  - 61
DO  - 10.1107/S1600536805018908
ER  - 

@article{
author = "Zabukovec-Logar, Nataša and Rajić, Nevenka and Stojaković, D. and Sajić, Sanja and Golobić, Amalija and Kaučič, Venčeslav",
year = "2005",
abstract = "The title compound, catena-poly[[N-methylpropane-1,3diaminium [mu-phosphato-(mu-hydrogen phosphato)(mu-dihydrogen phosphato) dizincate(II)]], {(C4H14N2)[Zn-2(PO4)(HPO4)(H2PO4)]}(n), consists of macroanionic [Zn-2(PO4)(HPO4)(H2PO4)](2-) layers and intercalated (C4H12N2)(2+) cations. The layers are built up from ZnO4 and PO4/HPO4/H2PO4 tetrahedra that result in small channels of approximate diameter 3.7 angstrom within the layers. Framework-to-framework O - H center dot center dot center dot O and template-to-framework N - H center dot center dot center dot O hydrogen bonds are important in stabilizing the structure.",
publisher = "Int Union Crystallography, Chester",
journal = "Acta Crystallographica Section E-Crystallographic Communications",
title = "(C4H12N2)[Zn-2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalated N-methylpropane-1,3-diaminium cations",
pages = "M1356-M1354",
volume = "61",
doi = "10.1107/S1600536805018908"
}

Zabukovec-Logar, N., Rajić, N., Stojaković, D., Sajić, S., Golobić, A.,& Kaučič, V.. (2005). (C4H12N2)[Zn-2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalated N-methylpropane-1,3-diaminium cations. in Acta Crystallographica Section E-Crystallographic Communications
Int Union Crystallography, Chester., 61, M1354-M1356.
https://doi.org/10.1107/S1600536805018908

Zabukovec-Logar N, Rajić N, Stojaković D, Sajić S, Golobić A, Kaučič V. (C4H12N2)[Zn-2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalated N-methylpropane-1,3-diaminium cations. in Acta Crystallographica Section E-Crystallographic Communications. 2005;61:M1354-M1356.
doi:10.1107/S1600536805018908 .

Zabukovec-Logar, Nataša, Rajić, Nevenka, Stojaković, D., Sajić, Sanja, Golobić, Amalija, Kaučič, Venčeslav, "(C4H12N2)[Zn-2(PO4)(HPO4)(H2PO4)], a layered zinc phosphate with intercalated N-methylpropane-1,3-diaminium cations" in Acta Crystallographica Section E-Crystallographic Communications, 61 (2005):M1354-M1356,
https://doi.org/10.1107/S1600536805018908 . .

TY  - JOUR
AU  - Rajić, Nevenka
AU  - Zabukovec-Logar, Nataša
AU  - Golobić, Amalija
AU  - Kaučič, Venčeslav
PY  - 2003
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/517
AB  - Colorless plate-like crystals (AIPO-1,2DAP) crystallize from a clear 'AlPO4-1,2-diaminopropane' reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH4+)(1,2-H(2)DAP)(2+)(AlP2O8)(3-), confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150 K reveal the space group Pc2(1)n with a = 8.2788(2), b = 16.7882(3), c = 8.6608(2) Angstrom, and V = 1203.73(5) Angstrom(3). The AIPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH4+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.
PB  - Pergamon-Elsevier Science Ltd, Oxford
T2  - Journal of Physics and Chemistry of Solids
T1  - Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent
EP  - 1103
IS  - 7
SP  - 1097
VL  - 64
DO  - 10.1016/S0022-3697(03)00002-7
ER  - 

@article{
author = "Rajić, Nevenka and Zabukovec-Logar, Nataša and Golobić, Amalija and Kaučič, Venčeslav",
year = "2003",
abstract = "Colorless plate-like crystals (AIPO-1,2DAP) crystallize from a clear 'AlPO4-1,2-diaminopropane' reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH4+)(1,2-H(2)DAP)(2+)(AlP2O8)(3-), confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150 K reveal the space group Pc2(1)n with a = 8.2788(2), b = 16.7882(3), c = 8.6608(2) Angstrom, and V = 1203.73(5) Angstrom(3). The AIPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH4+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.",
publisher = "Pergamon-Elsevier Science Ltd, Oxford",
journal = "Journal of Physics and Chemistry of Solids",
title = "Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent",
pages = "1103-1097",
number = "7",
volume = "64",
doi = "10.1016/S0022-3697(03)00002-7"
}

Rajić, N., Zabukovec-Logar, N., Golobić, A.,& Kaučič, V.. (2003). Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent. in Journal of Physics and Chemistry of Solids
Pergamon-Elsevier Science Ltd, Oxford., 64(7), 1097-1103.
https://doi.org/10.1016/S0022-3697(03)00002-7

Rajić N, Zabukovec-Logar N, Golobić A, Kaučič V. Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent. in Journal of Physics and Chemistry of Solids. 2003;64(7):1097-1103.
doi:10.1016/S0022-3697(03)00002-7 .

Rajić, Nevenka, Zabukovec-Logar, Nataša, Golobić, Amalija, Kaučič, Venčeslav, "Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent" in Journal of Physics and Chemistry of Solids, 64, no. 7 (2003):1097-1103,
https://doi.org/10.1016/S0022-3697(03)00002-7 . .