Stopic, Srecko

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  • Stopic, Srecko (2)
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Author's Bibliography

Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method

Stopic, Srecko; Wenz, Felix; Volkov-Husović, Tatjana; Friedrich, Bernd

(2021)

TY  - JOUR
AU  - Stopic, Srecko
AU  - Wenz, Felix
AU  - Volkov-Husović, Tatjana
AU  - Friedrich, Bernd
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4902
AB  - Silica has sparked strong interest in hydrometallurgy, catalysis, the cement industry, and paper coating. The synthesis of silica particles was performed at 900 degrees C using the ultrasonic spray pyrolysis (USP) method. Ideally, spherical particles are obtained in one horizontal reactor from an aerosol. The controlled synthesis of submicron particles of silica was reached by changing the concentration of precursor solution. The experimentally obtained particles were compared with theoretically calculated values of silica particles. The characterization was performed using a scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS). X-ray diffraction, frequently abbreviated as XRD, was used to analyze the structure of obtained materials. The obtained silica by ultrasonic spray pyrolysis had an amorphous structure. In comparison to other methods such as sol-gel, acidic treatment, thermal decomposition, stirred bead milling, and high-pressure carbonation, the advantage of the ultrasonic spray method for preparation of nanosized silica controlled morphology is the simplicity of setting up individual process segments and changing their configuration, one-step continuous synthesis, and the possibility of synthesizing nanoparticles from various precursors.
T2  - Metals
T1  - Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method
IS  - 3
VL  - 11
DO  - 10.3390/met11030463
ER  - 
@article{
author = "Stopic, Srecko and Wenz, Felix and Volkov-Husović, Tatjana and Friedrich, Bernd",
year = "2021",
abstract = "Silica has sparked strong interest in hydrometallurgy, catalysis, the cement industry, and paper coating. The synthesis of silica particles was performed at 900 degrees C using the ultrasonic spray pyrolysis (USP) method. Ideally, spherical particles are obtained in one horizontal reactor from an aerosol. The controlled synthesis of submicron particles of silica was reached by changing the concentration of precursor solution. The experimentally obtained particles were compared with theoretically calculated values of silica particles. The characterization was performed using a scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS). X-ray diffraction, frequently abbreviated as XRD, was used to analyze the structure of obtained materials. The obtained silica by ultrasonic spray pyrolysis had an amorphous structure. In comparison to other methods such as sol-gel, acidic treatment, thermal decomposition, stirred bead milling, and high-pressure carbonation, the advantage of the ultrasonic spray method for preparation of nanosized silica controlled morphology is the simplicity of setting up individual process segments and changing their configuration, one-step continuous synthesis, and the possibility of synthesizing nanoparticles from various precursors.",
journal = "Metals",
title = "Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method",
number = "3",
volume = "11",
doi = "10.3390/met11030463"
}
Stopic, S., Wenz, F., Volkov-Husović, T.,& Friedrich, B.. (2021). Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method. in Metals, 11(3).
https://doi.org/10.3390/met11030463
Stopic S, Wenz F, Volkov-Husović T, Friedrich B. Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method. in Metals. 2021;11(3).
doi:10.3390/met11030463 .
Stopic, Srecko, Wenz, Felix, Volkov-Husović, Tatjana, Friedrich, Bernd, "Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method" in Metals, 11, no. 3 (2021),
https://doi.org/10.3390/met11030463 . .
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Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy

Volkov-Husović, Tatjana; Ivanic, Ivana; Kozuh, Stjepan; Stevanovic, Sanja; Vlahovic, Milica; Martinovic, Sanja; Stopic, Srecko; Gojic, Mirko

(2021)

TY  - JOUR
AU  - Volkov-Husović, Tatjana
AU  - Ivanic, Ivana
AU  - Kozuh, Stjepan
AU  - Stevanovic, Sanja
AU  - Vlahovic, Milica
AU  - Martinovic, Sanja
AU  - Stopic, Srecko
AU  - Gojic, Mirko
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4862
AB  - Microstructural and cavitation erosion testing was carried out on Cu-12.8Al-4.1Ni (wt. %) shape memory alloy (SMA) samples produced by continuous casting followed by heat treatment consisting of solution annealing at 885 degrees C for 60 min and, later, water quenching. Cavitation resistance testing was applied using a standard ultrasonic vibratory cavitation set up with stationary specimen. Surface changes during the cavitation were monitored by metallographic analysis using an optical microscope (OM), atomic force microscope (AFM), and scanning electron microscope (SEM) as well as by weight measurements. The results revealed a martensite microstructure after both casting and quenching. Microhardness value was higher after water quenching than in the as-cast state. After 420 min of cavitation exposure, a negligible mass loss was noticed for both samples. Based on the obtained results, both samples showed excellent cavitation resistance. Mass loss and morphological analysis of the formed pits indicated better cavitation resistance for the as-cast state (L).
T2  - Metals
T1  - Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy
IS  - 7
VL  - 11
DO  - 10.3390/met11070997
ER  - 
@article{
author = "Volkov-Husović, Tatjana and Ivanic, Ivana and Kozuh, Stjepan and Stevanovic, Sanja and Vlahovic, Milica and Martinovic, Sanja and Stopic, Srecko and Gojic, Mirko",
year = "2021",
abstract = "Microstructural and cavitation erosion testing was carried out on Cu-12.8Al-4.1Ni (wt. %) shape memory alloy (SMA) samples produced by continuous casting followed by heat treatment consisting of solution annealing at 885 degrees C for 60 min and, later, water quenching. Cavitation resistance testing was applied using a standard ultrasonic vibratory cavitation set up with stationary specimen. Surface changes during the cavitation were monitored by metallographic analysis using an optical microscope (OM), atomic force microscope (AFM), and scanning electron microscope (SEM) as well as by weight measurements. The results revealed a martensite microstructure after both casting and quenching. Microhardness value was higher after water quenching than in the as-cast state. After 420 min of cavitation exposure, a negligible mass loss was noticed for both samples. Based on the obtained results, both samples showed excellent cavitation resistance. Mass loss and morphological analysis of the formed pits indicated better cavitation resistance for the as-cast state (L).",
journal = "Metals",
title = "Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy",
number = "7",
volume = "11",
doi = "10.3390/met11070997"
}
Volkov-Husović, T., Ivanic, I., Kozuh, S., Stevanovic, S., Vlahovic, M., Martinovic, S., Stopic, S.,& Gojic, M.. (2021). Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy. in Metals, 11(7).
https://doi.org/10.3390/met11070997
Volkov-Husović T, Ivanic I, Kozuh S, Stevanovic S, Vlahovic M, Martinovic S, Stopic S, Gojic M. Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy. in Metals. 2021;11(7).
doi:10.3390/met11070997 .
Volkov-Husović, Tatjana, Ivanic, Ivana, Kozuh, Stjepan, Stevanovic, Sanja, Vlahovic, Milica, Martinovic, Sanja, Stopic, Srecko, Gojic, Mirko, "Microstructural and Cavitation Erosion Behavior of the CuAlNi Shape Memory Alloy" in Metals, 11, no. 7 (2021),
https://doi.org/10.3390/met11070997 . .
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