Laušević, Mila

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Authority KeyName Variants
57ee31aa-fa03-4e36-9a61-c3103e781cc2
  • Laušević, Mila (7)
  • Laušević, Mila D. (4)
  • Lausevic, Mila (2)

Author's Bibliography

Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata

Maletić, Marina; Vukčević, Marija; Kalijadis, Ana; Lausevic, Mila

(VISOKA ŠKOLA STRUKOVNIH STUDIJA BEOGRADSKA POLITEHNIKA, 2017)

TY  - CONF
AU  - Maletić, Marina
AU  - Vukčević, Marija
AU  - Kalijadis, Ana
AU  - Lausevic, Mila
PY  - 2017
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6309
AB  - Poslednjih godina velika pažnja se poklanja prečišćavanju otpadnih voda, koje u vodene
ekosisteme unose niz različitih zagađujućih materija. Za uklanjanje organskih zagađujućih materija
standardno se koriste različite fizičko-hemijske i biološke metode, kao što su filtracija, koagulacija,
flokulacija, jonska izmena i fotokatalitička razgradnja. Međutim, efikasnost ovih metoda je često
nezadovoljavajuća usled njihove visoke cene kao i velike količine toksičnih i kancerogenih
nusprodukata koji njihovom primenom mogu nastati. Jedna od najekonomičnijih, najpouzdanijih i
najefikasnijih metoda je adsorpcija. U ovom radu korišćeni su kompozitni ugljenični materijali
dobijeni hidrotermalnom karbonizacijom, polazeći od glukoze, titan izopropoksida i melamina, kao
izvora ugljenika, titana i azota. Variranjem količine melamina u reakcionoj smeši, dobijeni su
kompozitni materijali različitih karakteristika. Ispitan je uticaj količine melamina na specifičnu
površinu materijala, prisustvo površinskih funkcionlanih grupa i adsorpcione karakteristike.
Adsorpcione karakteristike dobijenih materijala ispitane su adsorpcijom metilensko-plavog, kao
modela organske zagađujuće materije. Dobijeni rezultati pokazuju da adsorpcioni proces prati
kinetiku pseudo-drugog reda i može se opisati Lengmirovom adsorpcionom izotermom. Takođe,
količina melamina dodata u reakcionu smešu utiče na adsorpcione karakteristike u smislu da
najmanja količina dodatog melamina daje materijal sa najboljim adsorpcionim kapacitetom.
PB  - VISOKA ŠKOLA STRUKOVNIH STUDIJA BEOGRADSKA POLITEHNIKA
C3  - Četvrti naučno-stručni skup Politehnika, Zbornik radova
T1  - Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata
EP  - 230
SP  - 225
UR  - https://hdl.handle.net/21.15107/rcub_technorep_6309
ER  - 
@conference{
author = "Maletić, Marina and Vukčević, Marija and Kalijadis, Ana and Lausevic, Mila",
year = "2017",
abstract = "Poslednjih godina velika pažnja se poklanja prečišćavanju otpadnih voda, koje u vodene
ekosisteme unose niz različitih zagađujućih materija. Za uklanjanje organskih zagađujućih materija
standardno se koriste različite fizičko-hemijske i biološke metode, kao što su filtracija, koagulacija,
flokulacija, jonska izmena i fotokatalitička razgradnja. Međutim, efikasnost ovih metoda je često
nezadovoljavajuća usled njihove visoke cene kao i velike količine toksičnih i kancerogenih
nusprodukata koji njihovom primenom mogu nastati. Jedna od najekonomičnijih, najpouzdanijih i
najefikasnijih metoda je adsorpcija. U ovom radu korišćeni su kompozitni ugljenični materijali
dobijeni hidrotermalnom karbonizacijom, polazeći od glukoze, titan izopropoksida i melamina, kao
izvora ugljenika, titana i azota. Variranjem količine melamina u reakcionoj smeši, dobijeni su
kompozitni materijali različitih karakteristika. Ispitan je uticaj količine melamina na specifičnu
površinu materijala, prisustvo površinskih funkcionlanih grupa i adsorpcione karakteristike.
Adsorpcione karakteristike dobijenih materijala ispitane su adsorpcijom metilensko-plavog, kao
modela organske zagađujuće materije. Dobijeni rezultati pokazuju da adsorpcioni proces prati
kinetiku pseudo-drugog reda i može se opisati Lengmirovom adsorpcionom izotermom. Takođe,
količina melamina dodata u reakcionu smešu utiče na adsorpcione karakteristike u smislu da
najmanja količina dodatog melamina daje materijal sa najboljim adsorpcionim kapacitetom.",
publisher = "VISOKA ŠKOLA STRUKOVNIH STUDIJA BEOGRADSKA POLITEHNIKA",
journal = "Četvrti naučno-stručni skup Politehnika, Zbornik radova",
title = "Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata",
pages = "230-225",
url = "https://hdl.handle.net/21.15107/rcub_technorep_6309"
}
Maletić, M., Vukčević, M., Kalijadis, A.,& Lausevic, M.. (2017). Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata. in Četvrti naučno-stručni skup Politehnika, Zbornik radova
VISOKA ŠKOLA STRUKOVNIH STUDIJA BEOGRADSKA POLITEHNIKA., 225-230.
https://hdl.handle.net/21.15107/rcub_technorep_6309
Maletić M, Vukčević M, Kalijadis A, Lausevic M. Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata. in Četvrti naučno-stručni skup Politehnika, Zbornik radova. 2017;:225-230.
https://hdl.handle.net/21.15107/rcub_technorep_6309 .
Maletić, Marina, Vukčević, Marija, Kalijadis, Ana, Lausevic, Mila, "Uklanjanje organskih boja primenom kompozitnih ugljeničnih materijala kao adsorbenata" in Četvrti naučno-stručni skup Politehnika, Zbornik radova (2017):225-230,
https://hdl.handle.net/21.15107/rcub_technorep_6309 .

Identification of methomyl photocatalytic degradation products

Radišić, Marina; Tomašević, Anđelka; Mijin, Dušan; Marinković, Aleksandar; Tolić, Ljiljana; Laušević, Mila

(Belgrade : Society of Physical Chemists of Serbia, 2016)

TY  - CONF
AU  - Radišić, Marina
AU  - Tomašević, Anđelka
AU  - Mijin, Dušan
AU  - Marinković, Aleksandar
AU  - Tolić, Ljiljana
AU  - Laušević, Mila
PY  - 2016
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7247
AB  - Photocatalytic degradation of the methomyl pesticide in aqueous suspension
of TiO2 using an Osram ultra-vitalux® lamp (315-400 nm) was investigated.
The effect of parameters such as initial concentration of catalyst, initial
methomyl concentration, and pH were studied. Complete removal of
methomyl was achieved but mineralization of organic carbon was
incomplete indicating the formation of methomyl degradation products.
Liquid chromatography tandem mass spectrometry technique was used in
order to identify the methomyl degradation products and three major
degradation products have been identified.
PB  - Belgrade : Society of Physical Chemists of Serbia
C3  - Physical Chemistry 2016 : proceedings / 13th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Belgrade, 26-30 September 2016
T1  - Identification of methomyl photocatalytic degradation products
EP  - 234
SP  - 231
VL  - 1
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7247
ER  - 
@conference{
author = "Radišić, Marina and Tomašević, Anđelka and Mijin, Dušan and Marinković, Aleksandar and Tolić, Ljiljana and Laušević, Mila",
year = "2016",
abstract = "Photocatalytic degradation of the methomyl pesticide in aqueous suspension
of TiO2 using an Osram ultra-vitalux® lamp (315-400 nm) was investigated.
The effect of parameters such as initial concentration of catalyst, initial
methomyl concentration, and pH were studied. Complete removal of
methomyl was achieved but mineralization of organic carbon was
incomplete indicating the formation of methomyl degradation products.
Liquid chromatography tandem mass spectrometry technique was used in
order to identify the methomyl degradation products and three major
degradation products have been identified.",
publisher = "Belgrade : Society of Physical Chemists of Serbia",
journal = "Physical Chemistry 2016 : proceedings / 13th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Belgrade, 26-30 September 2016",
title = "Identification of methomyl photocatalytic degradation products",
pages = "234-231",
volume = "1",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7247"
}
Radišić, M., Tomašević, A., Mijin, D., Marinković, A., Tolić, L.,& Laušević, M.. (2016). Identification of methomyl photocatalytic degradation products. in Physical Chemistry 2016 : proceedings / 13th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Belgrade, 26-30 September 2016
Belgrade : Society of Physical Chemists of Serbia., 1, 231-234.
https://hdl.handle.net/21.15107/rcub_technorep_7247
Radišić M, Tomašević A, Mijin D, Marinković A, Tolić L, Laušević M. Identification of methomyl photocatalytic degradation products. in Physical Chemistry 2016 : proceedings / 13th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Belgrade, 26-30 September 2016. 2016;1:231-234.
https://hdl.handle.net/21.15107/rcub_technorep_7247 .
Radišić, Marina, Tomašević, Anđelka, Mijin, Dušan, Marinković, Aleksandar, Tolić, Ljiljana, Laušević, Mila, "Identification of methomyl photocatalytic degradation products" in Physical Chemistry 2016 : proceedings / 13th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Belgrade, 26-30 September 2016, 1 (2016):231-234,
https://hdl.handle.net/21.15107/rcub_technorep_7247 .

Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima

Vukčević, Marija; Lalović, Bojana; Kalijadis, Ana; Tolić, Ljiljana; Laušević, Zoran; Đurkić, Tatjana; Laušević, Mila

(Beograd : Srpsko hemijsko društvo = Serbian Chemical Society, 2015)

TY  - CONF
AU  - Vukčević, Marija
AU  - Lalović, Bojana
AU  - Kalijadis, Ana
AU  - Tolić, Ljiljana
AU  - Laušević, Zoran
AU  - Đurkić, Tatjana
AU  - Laušević, Mila
PY  - 2015
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7254
AB  - Predmet ovog rada bio je ispitivanje mogućnosti primene višeslojnih ugljeničnih nanocevi kao sorbenta u metodi ekstrakcije na čvrstoj fazi (eng. solid phase extraction SPE) pri analizi ostataka lekova iz vode. U cilju dobijanja SPE sorbenata različitih karakteristika, izvršeno je hemijsko modifikovanje ugljeničnih nanocevi korišćenjem 4 M KOH, 5 M HNO3 i 1 M HCl. Lekovi odabrani za analizu (metoprolol, sulfametaksazol, azitromicin, bisoprolol, enalapril, eritromicin, karbamazepin, lorazepam, klopidogrel, diklofenak, simvastatin i cilazapril) pripadaju grupama antibiotika, kardiovaskularnih lekova, analgoantipiretika i lekova za lečenje nervnog sistema, a to su istovremeneno najčešće korišćeni lekovi u Republici Srbiji. Pored lekova odabrana su i dva metabolita metamizola (4-AAA i 4-FAA), koji su u prethodnim istraživanjima često detektovani u uzorcima površinskih i podzemnih voda [2]. Za identifikaciju i kvantitativno određivanje analita korišćena je tečna hromatografija visoke performanse u sprezi sa tandem masenom spektrometrijom.
PB  - Beograd : Srpsko hemijsko društvo = Serbian Chemical Society
C3  - Knjiga izvoda = Book of Abstracts / 7. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem = 7th Symposium Chemistry and Environmental Protection with International Participation, Palić, Srbija, 09-12. jun 2015
T1  - Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima
T1  - Extraction of selected pharmaceuticals on multiwalled carbon nanotubes
EP  - 238
SP  - 237
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7254
ER  - 
@conference{
author = "Vukčević, Marija and Lalović, Bojana and Kalijadis, Ana and Tolić, Ljiljana and Laušević, Zoran and Đurkić, Tatjana and Laušević, Mila",
year = "2015",
abstract = "Predmet ovog rada bio je ispitivanje mogućnosti primene višeslojnih ugljeničnih nanocevi kao sorbenta u metodi ekstrakcije na čvrstoj fazi (eng. solid phase extraction SPE) pri analizi ostataka lekova iz vode. U cilju dobijanja SPE sorbenata različitih karakteristika, izvršeno je hemijsko modifikovanje ugljeničnih nanocevi korišćenjem 4 M KOH, 5 M HNO3 i 1 M HCl. Lekovi odabrani za analizu (metoprolol, sulfametaksazol, azitromicin, bisoprolol, enalapril, eritromicin, karbamazepin, lorazepam, klopidogrel, diklofenak, simvastatin i cilazapril) pripadaju grupama antibiotika, kardiovaskularnih lekova, analgoantipiretika i lekova za lečenje nervnog sistema, a to su istovremeneno najčešće korišćeni lekovi u Republici Srbiji. Pored lekova odabrana su i dva metabolita metamizola (4-AAA i 4-FAA), koji su u prethodnim istraživanjima često detektovani u uzorcima površinskih i podzemnih voda [2]. Za identifikaciju i kvantitativno određivanje analita korišćena je tečna hromatografija visoke performanse u sprezi sa tandem masenom spektrometrijom.",
publisher = "Beograd : Srpsko hemijsko društvo = Serbian Chemical Society",
journal = "Knjiga izvoda = Book of Abstracts / 7. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem = 7th Symposium Chemistry and Environmental Protection with International Participation, Palić, Srbija, 09-12. jun 2015",
title = "Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima, Extraction of selected pharmaceuticals on multiwalled carbon nanotubes",
pages = "238-237",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7254"
}
Vukčević, M., Lalović, B., Kalijadis, A., Tolić, L., Laušević, Z., Đurkić, T.,& Laušević, M.. (2015). Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima. in Knjiga izvoda = Book of Abstracts / 7. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem = 7th Symposium Chemistry and Environmental Protection with International Participation, Palić, Srbija, 09-12. jun 2015
Beograd : Srpsko hemijsko društvo = Serbian Chemical Society., 237-238.
https://hdl.handle.net/21.15107/rcub_technorep_7254
Vukčević M, Lalović B, Kalijadis A, Tolić L, Laušević Z, Đurkić T, Laušević M. Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima. in Knjiga izvoda = Book of Abstracts / 7. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem = 7th Symposium Chemistry and Environmental Protection with International Participation, Palić, Srbija, 09-12. jun 2015. 2015;:237-238.
https://hdl.handle.net/21.15107/rcub_technorep_7254 .
Vukčević, Marija, Lalović, Bojana, Kalijadis, Ana, Tolić, Ljiljana, Laušević, Zoran, Đurkić, Tatjana, Laušević, Mila, "Ekstrakcija odabranih lekova na višeslojnim ugljeničnim nanocevima" in Knjiga izvoda = Book of Abstracts / 7. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem = 7th Symposium Chemistry and Environmental Protection with International Participation, Palić, Srbija, 09-12. jun 2015 (2015):237-238,
https://hdl.handle.net/21.15107/rcub_technorep_7254 .

Raspodela odabranih lekova i pesticida u sistemu voda-sediment

Matić, Ivana V.; Tolić, Ljiljana M.; Grujić, Svetlana D.; Laušević, Mila D.

(Beograd : Srpsko hemijsko društvo, 2015)

TY  - CONF
AU  - Matić, Ivana V.
AU  - Tolić, Ljiljana M.
AU  - Grujić, Svetlana D.
AU  - Laušević, Mila D.
PY  - 2015
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7242
AB  - Cilj ovog rada bio je ispitivanje načina adsorpcije i raspodele odabranih lekova i pesticida između vodene faze i sedimenta, kao i određivanje stepena adsorpcije i desorpcije na sedimentu reke Dunav. Rezultati adsorpcije leka karbamazepina i pesticida atrazina, karbendazima i karbofurana pokazuju najbolje slaganje sa Frojndlihovom izotermom, što ukazuje na reverzibilnu adsorpciju. Zbog visokog procenta desorpcije karbamazepina, atrazina i karbendazima, njihovo prisustvo u sistemu voda-sediment je očekivano, dok se karbofuran očekuje u manjoj koncentraciji u vodi, zbog nižeg procenta desorpcije. Lengmirov model opisuje monoslojnu adsorpciju pesticida dimetoata. Ovaj pesticid pokazuje i mali stepen desorpcije, što ukazuje na to da se može akumulirati u sedimentima u visokoj koncentraciji. Adsorpcija lekova trimetoprima, metoprolola i lorazepama se može opisati linearnim modelom. Ovi analiti pokazuju veliki afinitet adsorpcije i mogu se vezati za sediment u koncentracijama većim od ispitivanih. Za razliku od metoprolola i lorazepama, trimetoprim se u velikom procentu desorbuje sa sedimenta, pa se ovaj analit očekuje u vodi. Lekovi bromazepam, eritromicin i amlodipin su pokazali skoro potpunu adsorpciju na sedimentu i veoma mali stepen desorpcije, pa je njihova akumulacija u sedimentima očekivana.
AB  - The aim of this study was investigation of the adsorption and distribution of the selected
pharmaceuticals and pesticides between water phase and sediment, as well as determination
of the adsorption and desorption extent using sediment of the Danube River. Adsorption
data of the drug carbamazepine and pesticides atrazine, carbendazim and carbofuran fit well
to Freundlich isotherm, implying reversible adsorption. Due to high desorption extent of
carbamazepine, atrazine and carbendazim, their presence in water-sediment system is
expected, whereas lower desorption level of carbofuran indicates lower expected
concentration of this pesticide in water. Langmuir model describes monolayer adsorption of
pesticide dimethoate. This pesticide also shows low desorption extent, indicating its high
accumulation in sediments. Adsorption data of pharmaceuticals trimethoprim, metoprolol
and lorazepam fit fine to the linear model. These analytes show high adsorption affinity and
can be adsorbed onto sediment at concentrations higher than tested. Unlike metoprolol and
lorazepam, trimethoprim exhibits higher desorption level, so it is expected in water.
Pharmaceuticals bromazepam, erythromycin and amlodipine displayed almost complete
adsorption onto sediment and extremely low desorption rate, so their accumulation in
sediments is expected.
PB  - Beograd : Srpsko hemijsko društvo
C3  - Knjiga radova / 52. savetovanje Srpskog hemijskog društva, Novi Sad, 29. i 30. maj 2015
T1  - Raspodela odabranih lekova i pesticida u sistemu voda-sediment
T1  - Distribution of selected pharmaceuticals and pesticides in water-sediment system
EP  - 62
SP  - 59
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7242
ER  - 
@conference{
author = "Matić, Ivana V. and Tolić, Ljiljana M. and Grujić, Svetlana D. and Laušević, Mila D.",
year = "2015",
abstract = "Cilj ovog rada bio je ispitivanje načina adsorpcije i raspodele odabranih lekova i pesticida između vodene faze i sedimenta, kao i određivanje stepena adsorpcije i desorpcije na sedimentu reke Dunav. Rezultati adsorpcije leka karbamazepina i pesticida atrazina, karbendazima i karbofurana pokazuju najbolje slaganje sa Frojndlihovom izotermom, što ukazuje na reverzibilnu adsorpciju. Zbog visokog procenta desorpcije karbamazepina, atrazina i karbendazima, njihovo prisustvo u sistemu voda-sediment je očekivano, dok se karbofuran očekuje u manjoj koncentraciji u vodi, zbog nižeg procenta desorpcije. Lengmirov model opisuje monoslojnu adsorpciju pesticida dimetoata. Ovaj pesticid pokazuje i mali stepen desorpcije, što ukazuje na to da se može akumulirati u sedimentima u visokoj koncentraciji. Adsorpcija lekova trimetoprima, metoprolola i lorazepama se može opisati linearnim modelom. Ovi analiti pokazuju veliki afinitet adsorpcije i mogu se vezati za sediment u koncentracijama većim od ispitivanih. Za razliku od metoprolola i lorazepama, trimetoprim se u velikom procentu desorbuje sa sedimenta, pa se ovaj analit očekuje u vodi. Lekovi bromazepam, eritromicin i amlodipin su pokazali skoro potpunu adsorpciju na sedimentu i veoma mali stepen desorpcije, pa je njihova akumulacija u sedimentima očekivana., The aim of this study was investigation of the adsorption and distribution of the selected
pharmaceuticals and pesticides between water phase and sediment, as well as determination
of the adsorption and desorption extent using sediment of the Danube River. Adsorption
data of the drug carbamazepine and pesticides atrazine, carbendazim and carbofuran fit well
to Freundlich isotherm, implying reversible adsorption. Due to high desorption extent of
carbamazepine, atrazine and carbendazim, their presence in water-sediment system is
expected, whereas lower desorption level of carbofuran indicates lower expected
concentration of this pesticide in water. Langmuir model describes monolayer adsorption of
pesticide dimethoate. This pesticide also shows low desorption extent, indicating its high
accumulation in sediments. Adsorption data of pharmaceuticals trimethoprim, metoprolol
and lorazepam fit fine to the linear model. These analytes show high adsorption affinity and
can be adsorbed onto sediment at concentrations higher than tested. Unlike metoprolol and
lorazepam, trimethoprim exhibits higher desorption level, so it is expected in water.
Pharmaceuticals bromazepam, erythromycin and amlodipine displayed almost complete
adsorption onto sediment and extremely low desorption rate, so their accumulation in
sediments is expected.",
publisher = "Beograd : Srpsko hemijsko društvo",
journal = "Knjiga radova / 52. savetovanje Srpskog hemijskog društva, Novi Sad, 29. i 30. maj 2015",
title = "Raspodela odabranih lekova i pesticida u sistemu voda-sediment, Distribution of selected pharmaceuticals and pesticides in water-sediment system",
pages = "62-59",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7242"
}
Matić, I. V., Tolić, L. M., Grujić, S. D.,& Laušević, M. D.. (2015). Raspodela odabranih lekova i pesticida u sistemu voda-sediment. in Knjiga radova / 52. savetovanje Srpskog hemijskog društva, Novi Sad, 29. i 30. maj 2015
Beograd : Srpsko hemijsko društvo., 59-62.
https://hdl.handle.net/21.15107/rcub_technorep_7242
Matić IV, Tolić LM, Grujić SD, Laušević MD. Raspodela odabranih lekova i pesticida u sistemu voda-sediment. in Knjiga radova / 52. savetovanje Srpskog hemijskog društva, Novi Sad, 29. i 30. maj 2015. 2015;:59-62.
https://hdl.handle.net/21.15107/rcub_technorep_7242 .
Matić, Ivana V., Tolić, Ljiljana M., Grujić, Svetlana D., Laušević, Mila D., "Raspodela odabranih lekova i pesticida u sistemu voda-sediment" in Knjiga radova / 52. savetovanje Srpskog hemijskog društva, Novi Sad, 29. i 30. maj 2015 (2015):59-62,
https://hdl.handle.net/21.15107/rcub_technorep_7242 .

Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry

Tolić, Ljiljana M.; Grujić, Svetlana D.; Lubec, Gert; Laušević, Mila D.

(Beograd : Srpsko hemijsko društvo, 2014)

TY  - CONF
AU  - Tolić, Ljiljana M.
AU  - Grujić, Svetlana D.
AU  - Lubec, Gert
AU  - Laušević, Mila D.
PY  - 2014
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7241
AB  - The aim of this work was development of sensitive analytical method for determination of drug anisomycin in different tissue samples. The optimized extraction procedure included methanol as extraction solvent and Oasis HLB as extract clean up cartridge. In the method validation, ani-somycin was efficiently extracted from most of tissues, such as heart, brain, spleen, kidney and li-ver, whereas lower recoveries were obtained for fat tissue. Low limits of detection (0.6–3.8 ng g–1) and quantification (2.4–11.8 ng g–1) indicate that developed method is suitable for determination of anisomycin trace levels. The method was linear (R2 > 0.975) in the tested concentration range (50–2500 ng g–1). Significant matrix effect was eliminated using matrix-matched standards. It was finally determined that the developed method is sensitive and reliable for determination of drug anisomycin in various tissue samples using liquid chromatography–tandem mass spectrometry.
AB  - Cilj ovog rada bio je razvoj osetljive analitičke metode za određivanje leka anizomicina u različitim tkivima. U
optimizovanoj proceduri ekstrakcije, metanol je odabran kao rastvarač za ekstrakciju, a Oasis HLB kao
kertridž za prečišćavanje ekstrakta. Prilikom validacije razvijene metode, anizomicin je efikasno ekstrahovan
iz većine tkiva, kao što su srce, mozak, slezina, bubrezi i jetra, dok su za masno tkivo dobijeni niži prinosi.
Niske granice detekcije (0,6–3,8 ng g
–1
) i kvantifikacije (2,4–11,8 ng g–1
) ukazuju da je razvijena metoda
pogodna za određivanje tragova anizomicina. U ispitivanom opsegu koncentracija (50–2500 ng g–1
) metoda je
linearna (R2
> 0,975). Značajan uticaj matrice eliminisan je upotrebom standarda koji odgovaraju matrici
uzorka. Na osnovu rezultata validacije utvrđeno je da je razvijena metoda osetljiva i pouzdana za određivanje
leka anizomicina u različitim tkivima korišćenjem tečne hromatografije sa tandem masenom spektrometrijom.
PB  - Beograd : Srpsko hemijsko društvo
C3  - Knjiga radova / 51. savetovanje Srpskog hemijskog društva i 2. konferencija mladih hemičara Srbije, Niš, 5-7. juni 2014
T1  - Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry
T1  - Određivanje antibiotika anizomicina u tkivima metodom tečne hromatografije sa tandem masenom spektrometrijom
EP  - 10
SP  - 7
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7241
ER  - 
@conference{
author = "Tolić, Ljiljana M. and Grujić, Svetlana D. and Lubec, Gert and Laušević, Mila D.",
year = "2014",
abstract = "The aim of this work was development of sensitive analytical method for determination of drug anisomycin in different tissue samples. The optimized extraction procedure included methanol as extraction solvent and Oasis HLB as extract clean up cartridge. In the method validation, ani-somycin was efficiently extracted from most of tissues, such as heart, brain, spleen, kidney and li-ver, whereas lower recoveries were obtained for fat tissue. Low limits of detection (0.6–3.8 ng g–1) and quantification (2.4–11.8 ng g–1) indicate that developed method is suitable for determination of anisomycin trace levels. The method was linear (R2 > 0.975) in the tested concentration range (50–2500 ng g–1). Significant matrix effect was eliminated using matrix-matched standards. It was finally determined that the developed method is sensitive and reliable for determination of drug anisomycin in various tissue samples using liquid chromatography–tandem mass spectrometry., Cilj ovog rada bio je razvoj osetljive analitičke metode za određivanje leka anizomicina u različitim tkivima. U
optimizovanoj proceduri ekstrakcije, metanol je odabran kao rastvarač za ekstrakciju, a Oasis HLB kao
kertridž za prečišćavanje ekstrakta. Prilikom validacije razvijene metode, anizomicin je efikasno ekstrahovan
iz većine tkiva, kao što su srce, mozak, slezina, bubrezi i jetra, dok su za masno tkivo dobijeni niži prinosi.
Niske granice detekcije (0,6–3,8 ng g
–1
) i kvantifikacije (2,4–11,8 ng g–1
) ukazuju da je razvijena metoda
pogodna za određivanje tragova anizomicina. U ispitivanom opsegu koncentracija (50–2500 ng g–1
) metoda je
linearna (R2
> 0,975). Značajan uticaj matrice eliminisan je upotrebom standarda koji odgovaraju matrici
uzorka. Na osnovu rezultata validacije utvrđeno je da je razvijena metoda osetljiva i pouzdana za određivanje
leka anizomicina u različitim tkivima korišćenjem tečne hromatografije sa tandem masenom spektrometrijom.",
publisher = "Beograd : Srpsko hemijsko društvo",
journal = "Knjiga radova / 51. savetovanje Srpskog hemijskog društva i 2. konferencija mladih hemičara Srbije, Niš, 5-7. juni 2014",
title = "Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry, Određivanje antibiotika anizomicina u tkivima metodom tečne hromatografije sa tandem masenom spektrometrijom",
pages = "10-7",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7241"
}
Tolić, L. M., Grujić, S. D., Lubec, G.,& Laušević, M. D.. (2014). Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry. in Knjiga radova / 51. savetovanje Srpskog hemijskog društva i 2. konferencija mladih hemičara Srbije, Niš, 5-7. juni 2014
Beograd : Srpsko hemijsko društvo., 7-10.
https://hdl.handle.net/21.15107/rcub_technorep_7241
Tolić LM, Grujić SD, Lubec G, Laušević MD. Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry. in Knjiga radova / 51. savetovanje Srpskog hemijskog društva i 2. konferencija mladih hemičara Srbije, Niš, 5-7. juni 2014. 2014;:7-10.
https://hdl.handle.net/21.15107/rcub_technorep_7241 .
Tolić, Ljiljana M., Grujić, Svetlana D., Lubec, Gert, Laušević, Mila D., "Determination of antibiotic anisomycin in tissue samples by liquid chromatography–tandem mass spectrometry" in Knjiga radova / 51. savetovanje Srpskog hemijskog društva i 2. konferencija mladih hemičara Srbije, Niš, 5-7. juni 2014 (2014):7-10,
https://hdl.handle.net/21.15107/rcub_technorep_7241 .

Određivanje anizomicina u životinjskim tkivima

Tolić, Ljiljana; Antić, Nikolina; Grujić, Svetlana; Bačić, Goran; Laušević, Mila D.

(Beograd : Srpsko hemijsko društvo, 2013)

TY  - CONF
AU  - Tolić, Ljiljana
AU  - Antić, Nikolina
AU  - Grujić, Svetlana
AU  - Bačić, Goran
AU  - Laušević, Mila D.
PY  - 2013
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7243
AB  - Anizomicin je antibiotik izolovan iz bakterijske vrste Streptomyces griseolus za koji je nekoliko studija pokazalo da je citotoksičan prema ćelijama malignog tu-mora, tj. da može suzbiti njihov rast. Cilj ovog rada bio je razvoj i optimizacija metode  ekstrakcije  ovog  antibiotika  iz  životinjskih  tkiva,  kao  što  su  srce  i  jetra.  Ispitivani  su  različiti  rastvarači  za  ekstrakciju,  kao  i  metode  prečišćavanja  dobijenog ekstrakta. Ekstrakt je analiziran metodom tečne hromatografije sa tandem masenom  spektrometrijom  (LC–MS/MS,  engl.  liquid  chromatography–tandem  mass spectrometry).
PB  - Beograd : Srpsko hemijsko društvo
C3  - Knjiga izvoda / 6. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem, Vršac, 21-24. maj 2013
T1  - Određivanje anizomicina u životinjskim tkivima
EP  - 209
SP  - 208
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7243
ER  - 
@conference{
author = "Tolić, Ljiljana and Antić, Nikolina and Grujić, Svetlana and Bačić, Goran and Laušević, Mila D.",
year = "2013",
abstract = "Anizomicin je antibiotik izolovan iz bakterijske vrste Streptomyces griseolus za koji je nekoliko studija pokazalo da je citotoksičan prema ćelijama malignog tu-mora, tj. da može suzbiti njihov rast. Cilj ovog rada bio je razvoj i optimizacija metode  ekstrakcije  ovog  antibiotika  iz  životinjskih  tkiva,  kao  što  su  srce  i  jetra.  Ispitivani  su  različiti  rastvarači  za  ekstrakciju,  kao  i  metode  prečišćavanja  dobijenog ekstrakta. Ekstrakt je analiziran metodom tečne hromatografije sa tandem masenom  spektrometrijom  (LC–MS/MS,  engl.  liquid  chromatography–tandem  mass spectrometry).",
publisher = "Beograd : Srpsko hemijsko društvo",
journal = "Knjiga izvoda / 6. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem, Vršac, 21-24. maj 2013",
title = "Određivanje anizomicina u životinjskim tkivima",
pages = "209-208",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7243"
}
Tolić, L., Antić, N., Grujić, S., Bačić, G.,& Laušević, M. D.. (2013). Određivanje anizomicina u životinjskim tkivima. in Knjiga izvoda / 6. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem, Vršac, 21-24. maj 2013
Beograd : Srpsko hemijsko društvo., 208-209.
https://hdl.handle.net/21.15107/rcub_technorep_7243
Tolić L, Antić N, Grujić S, Bačić G, Laušević MD. Određivanje anizomicina u životinjskim tkivima. in Knjiga izvoda / 6. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem, Vršac, 21-24. maj 2013. 2013;:208-209.
https://hdl.handle.net/21.15107/rcub_technorep_7243 .
Tolić, Ljiljana, Antić, Nikolina, Grujić, Svetlana, Bačić, Goran, Laušević, Mila D., "Određivanje anizomicina u životinjskim tkivima" in Knjiga izvoda / 6. simpozijum Hemija i zaštita životne sredine sa međunarodnim učešćem, Vršac, 21-24. maj 2013 (2013):208-209,
https://hdl.handle.net/21.15107/rcub_technorep_7243 .

Modification of glassy carbon properties under low energy proton irradiation

Jovanovic, Zoran; Kalijadis, Ana; Vasiljević-Radović, Dana; Eric, Marko; Lausevic, Mila; Mentus, Slavko; Laušević, Zoran

(Oxford : Pergamon-Elsevier Science Ltd, 2011)

TY  - JOUR
AU  - Jovanovic, Zoran
AU  - Kalijadis, Ana
AU  - Vasiljević-Radović, Dana
AU  - Eric, Marko
AU  - Lausevic, Mila
AU  - Mentus, Slavko
AU  - Laušević, Zoran
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5639
AB  - Glassy carbon plates were irradiated with 15 key H(+) ion-beam in the fluence range of 1 x 10(16)-3 x 10(18) ion cm(-2). The influence of ion irradiation on surface morphology and topology was examined by scanning electron and atomic force microscopy. Structural changes were monitored by Raman spectrometry, while changes of wettability and the content of surface oxygen complexes were examined by contact angle measurements and temperature programmed desorption. Elastic recoil detection analysis was applied for determination of hydrogen concentration profiles in irradiated samples. Cyclic voltammetry was used for the assessment of the electrochemical properties of modified glassy carbon electrodes. It was concluded that there is critical fluence range (2 x 10(17)-5 x 10(17) ion cm(-2)) inside of which significant changes of glassy carbon properties occur.
PB  - Oxford : Pergamon-Elsevier Science Ltd
T2  - Carbon
T1  - Modification of glassy carbon properties under low energy proton irradiation
EP  - 3746
IS  - 12
SP  - 3737
VL  - 49
DO  - 10.1016/j.carbon.2011.05.006
ER  - 
@article{
author = "Jovanovic, Zoran and Kalijadis, Ana and Vasiljević-Radović, Dana and Eric, Marko and Lausevic, Mila and Mentus, Slavko and Laušević, Zoran",
year = "2011",
abstract = "Glassy carbon plates were irradiated with 15 key H(+) ion-beam in the fluence range of 1 x 10(16)-3 x 10(18) ion cm(-2). The influence of ion irradiation on surface morphology and topology was examined by scanning electron and atomic force microscopy. Structural changes were monitored by Raman spectrometry, while changes of wettability and the content of surface oxygen complexes were examined by contact angle measurements and temperature programmed desorption. Elastic recoil detection analysis was applied for determination of hydrogen concentration profiles in irradiated samples. Cyclic voltammetry was used for the assessment of the electrochemical properties of modified glassy carbon electrodes. It was concluded that there is critical fluence range (2 x 10(17)-5 x 10(17) ion cm(-2)) inside of which significant changes of glassy carbon properties occur.",
publisher = "Oxford : Pergamon-Elsevier Science Ltd",
journal = "Carbon",
title = "Modification of glassy carbon properties under low energy proton irradiation",
pages = "3746-3737",
number = "12",
volume = "49",
doi = "10.1016/j.carbon.2011.05.006"
}
Jovanovic, Z., Kalijadis, A., Vasiljević-Radović, D., Eric, M., Lausevic, M., Mentus, S.,& Laušević, Z.. (2011). Modification of glassy carbon properties under low energy proton irradiation. in Carbon
Oxford : Pergamon-Elsevier Science Ltd., 49(12), 3737-3746.
https://doi.org/10.1016/j.carbon.2011.05.006
Jovanovic Z, Kalijadis A, Vasiljević-Radović D, Eric M, Lausevic M, Mentus S, Laušević Z. Modification of glassy carbon properties under low energy proton irradiation. in Carbon. 2011;49(12):3737-3746.
doi:10.1016/j.carbon.2011.05.006 .
Jovanovic, Zoran, Kalijadis, Ana, Vasiljević-Radović, Dana, Eric, Marko, Lausevic, Mila, Mentus, Slavko, Laušević, Zoran, "Modification of glassy carbon properties under low energy proton irradiation" in Carbon, 49, no. 12 (2011):3737-3746,
https://doi.org/10.1016/j.carbon.2011.05.006 . .
8
7
8

The effect of boron incorporation on the structure and properties of glassy carbon

Kalijadis, Ana; Jovanović, Zoran M.; Laušević, Mila; Laušević, Zoran

(Elsevier Ltd., 2011)

TY  - JOUR
AU  - Kalijadis, Ana
AU  - Jovanović, Zoran M.
AU  - Laušević, Mila
AU  - Laušević, Zoran
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5660
AB  - Boron was introduced into glassy carbon by chemical modification and by irradiating the precursor polymer with boron ions. Using chemical modification, a polymer with uniform distribution of boron in the bulk was obtained, whereas irradiation with B3+ produced a polymer with boron located in a narrow region under the surface. Following modification with boron, the samples were carbonized at 1273 K and examined using X-ray diffraction, Raman spectroscopy, temperature programmed desorption (TPD) and by hardness measurements. Structural analysis results suggest that boron is mostly substitutionally bonded in the glassy carbon structure regardless of the method used to introduce boron into the polymer precursor. Formation of crosslinks between glassy carbon ribbons during carbonization as a consequence of the recombination of ion beam induced changes in the polymer structure and a high concentration of boron in the subsurface layer is proposed to account for an increase of glassy carbon hardness. An increase in the total amount of surface oxygen groups was observed in the TPD spectra of both boron-modified samples due to an increase in the number of active sites. Results show that the nature of these sites is influenced by the initial distribution of boron in the polymer precursor. (C) 2011 Elsevier Ltd. All rights reserved.
PB  - Elsevier Ltd.
T2  - Carbon
T1  - The effect of boron incorporation on the structure and properties of glassy carbon
EP  - 2678
IS  - 8
SP  - 2671
VL  - 49
DO  - 10.1016/j.carbon.2011.02.054
ER  - 
@article{
author = "Kalijadis, Ana and Jovanović, Zoran M. and Laušević, Mila and Laušević, Zoran",
year = "2011",
abstract = "Boron was introduced into glassy carbon by chemical modification and by irradiating the precursor polymer with boron ions. Using chemical modification, a polymer with uniform distribution of boron in the bulk was obtained, whereas irradiation with B3+ produced a polymer with boron located in a narrow region under the surface. Following modification with boron, the samples were carbonized at 1273 K and examined using X-ray diffraction, Raman spectroscopy, temperature programmed desorption (TPD) and by hardness measurements. Structural analysis results suggest that boron is mostly substitutionally bonded in the glassy carbon structure regardless of the method used to introduce boron into the polymer precursor. Formation of crosslinks between glassy carbon ribbons during carbonization as a consequence of the recombination of ion beam induced changes in the polymer structure and a high concentration of boron in the subsurface layer is proposed to account for an increase of glassy carbon hardness. An increase in the total amount of surface oxygen groups was observed in the TPD spectra of both boron-modified samples due to an increase in the number of active sites. Results show that the nature of these sites is influenced by the initial distribution of boron in the polymer precursor. (C) 2011 Elsevier Ltd. All rights reserved.",
publisher = "Elsevier Ltd.",
journal = "Carbon",
title = "The effect of boron incorporation on the structure and properties of glassy carbon",
pages = "2678-2671",
number = "8",
volume = "49",
doi = "10.1016/j.carbon.2011.02.054"
}
Kalijadis, A., Jovanović, Z. M., Laušević, M.,& Laušević, Z.. (2011). The effect of boron incorporation on the structure and properties of glassy carbon. in Carbon
Elsevier Ltd.., 49(8), 2671-2678.
https://doi.org/10.1016/j.carbon.2011.02.054
Kalijadis A, Jovanović ZM, Laušević M, Laušević Z. The effect of boron incorporation on the structure and properties of glassy carbon. in Carbon. 2011;49(8):2671-2678.
doi:10.1016/j.carbon.2011.02.054 .
Kalijadis, Ana, Jovanović, Zoran M., Laušević, Mila, Laušević, Zoran, "The effect of boron incorporation on the structure and properties of glassy carbon" in Carbon, 49, no. 8 (2011):2671-2678,
https://doi.org/10.1016/j.carbon.2011.02.054 . .
3
30
26
31

The evolution of hydrogen from proton irradiated glassy carbon

Jovanović, Zoran M.; Kalijadis, Ana; Laušević, Mila; Laušević, Zoran

(Elsevier B.V., 2011)

TY  - JOUR
AU  - Jovanović, Zoran M.
AU  - Kalijadis, Ana
AU  - Laušević, Mila
AU  - Laušević, Zoran
PY  - 2011
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5661
AB  - Glassy carbon was irradiated with 15 key H(+) ion beam. It was observed that the implanted hydrogen is unstable in material and evolves as H, H(2) and H(2)O. Post-irradiation evolution of H, H(2) and H(2)O from proton irradiated glassy carbon was monitored by temperature programmed desorption (TPD) in the period of 30 days. In between irradiation and TPD measurements the irradiated samples were stored in air. The evolution of the molecular hydrogen, although the protons are implanted deeply below the surface of the disordered glassy carbon, proceeds over the same mechanism as in the case of low-energy H-atoms chemisorbed on the very surface of an ideal graphite structure. (C) 2011 Elsevier B.V. All rights reserved.
PB  - Elsevier B.V.
T2  - Nuclear Instruments and Methods in Physics Research. Section B: Beam Interactions with Materials and Atoms
T1  - The evolution of hydrogen from proton irradiated glassy carbon
EP  - 2583
IS  - 21
SP  - 2578
VL  - 269
DO  - 10.1016/j.nimb.2011.07.014
ER  - 
@article{
author = "Jovanović, Zoran M. and Kalijadis, Ana and Laušević, Mila and Laušević, Zoran",
year = "2011",
abstract = "Glassy carbon was irradiated with 15 key H(+) ion beam. It was observed that the implanted hydrogen is unstable in material and evolves as H, H(2) and H(2)O. Post-irradiation evolution of H, H(2) and H(2)O from proton irradiated glassy carbon was monitored by temperature programmed desorption (TPD) in the period of 30 days. In between irradiation and TPD measurements the irradiated samples were stored in air. The evolution of the molecular hydrogen, although the protons are implanted deeply below the surface of the disordered glassy carbon, proceeds over the same mechanism as in the case of low-energy H-atoms chemisorbed on the very surface of an ideal graphite structure. (C) 2011 Elsevier B.V. All rights reserved.",
publisher = "Elsevier B.V.",
journal = "Nuclear Instruments and Methods in Physics Research. Section B: Beam Interactions with Materials and Atoms",
title = "The evolution of hydrogen from proton irradiated glassy carbon",
pages = "2583-2578",
number = "21",
volume = "269",
doi = "10.1016/j.nimb.2011.07.014"
}
Jovanović, Z. M., Kalijadis, A., Laušević, M.,& Laušević, Z.. (2011). The evolution of hydrogen from proton irradiated glassy carbon. in Nuclear Instruments and Methods in Physics Research. Section B: Beam Interactions with Materials and Atoms
Elsevier B.V.., 269(21), 2578-2583.
https://doi.org/10.1016/j.nimb.2011.07.014
Jovanović ZM, Kalijadis A, Laušević M, Laušević Z. The evolution of hydrogen from proton irradiated glassy carbon. in Nuclear Instruments and Methods in Physics Research. Section B: Beam Interactions with Materials and Atoms. 2011;269(21):2578-2583.
doi:10.1016/j.nimb.2011.07.014 .
Jovanović, Zoran M., Kalijadis, Ana, Laušević, Mila, Laušević, Zoran, "The evolution of hydrogen from proton irradiated glassy carbon" in Nuclear Instruments and Methods in Physics Research. Section B: Beam Interactions with Materials and Atoms, 269, no. 21 (2011):2578-2583,
https://doi.org/10.1016/j.nimb.2011.07.014 . .
3
2
3

Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry

Trtić-Petrović, Tatjana M.; Đorđević, Jelena S.; Dujaković, Nikolina; Kumrić, Ksenija; Vasiljević, Tatjana; Laušević, Mila

(2010)

TY  - JOUR
AU  - Trtić-Petrović, Tatjana M.
AU  - Đorđević, Jelena S.
AU  - Dujaković, Nikolina
AU  - Kumrić, Ksenija
AU  - Vasiljević, Tatjana
AU  - Laušević, Mila
PY  - 2010
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5590
AB  - An optimised extraction and cleanup method for the analysis of pesticide in natural water samples is presented. Sixteen pesticides of different polarity and from the different chemical classes (organophosphates, triazines, benzimidazoles, carbamates, carbamides, neonicotinoides, methylureas, phenylureas and benzohydrazides), most frequently used in Serbia, were selected for the analysis. Liquid-phase microextraction in a single hollow fibre (HF-LPME) has been applied for sample preparation. The concentrations of pesticides were determined using HPLC-MS/MS method with electrospray ionisation. The extraction behaviour and selection of the experimental conditions was predicted based on log D and pK (a) values of targeted pesticides, which were calculated applying the computer software ACD/Labs PhysChem Suite v12. The influence of the donor pH and concentration of pesticides, organic phase composition as well as the extraction time on the extraction efficiency was investigated. Optimum extraction conditions were evaluated with respect to the investigated parameters of the extraction. The extraction method was validated for 10 out of 16 studied pesticides. Linear range of the pesticides was 0.1-5 A mu g L(-1) with the correlation coefficient from 0.991 to 0.9998, and the relative standard deviation for three standard measurements was between 0.2 and 11.8%. The limits of detections ranged from 0.026 to 0.237 A mu g L(-1) and the limits of quantifications from 0.094 to 0.793 A mu g L(-1). The optimised two-phase HF-LPME method was successfully applied for determination of moderately polar as well low-polar pesticides in the environmental water samples.
T2  - Analytical and Bioanalytical Chemistry
T1  - Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry
EP  - 2243
IS  - 6
SP  - 2233
VL  - 397
DO  - 10.1007/s00216-010-3725-5
ER  - 
@article{
author = "Trtić-Petrović, Tatjana M. and Đorđević, Jelena S. and Dujaković, Nikolina and Kumrić, Ksenija and Vasiljević, Tatjana and Laušević, Mila",
year = "2010",
abstract = "An optimised extraction and cleanup method for the analysis of pesticide in natural water samples is presented. Sixteen pesticides of different polarity and from the different chemical classes (organophosphates, triazines, benzimidazoles, carbamates, carbamides, neonicotinoides, methylureas, phenylureas and benzohydrazides), most frequently used in Serbia, were selected for the analysis. Liquid-phase microextraction in a single hollow fibre (HF-LPME) has been applied for sample preparation. The concentrations of pesticides were determined using HPLC-MS/MS method with electrospray ionisation. The extraction behaviour and selection of the experimental conditions was predicted based on log D and pK (a) values of targeted pesticides, which were calculated applying the computer software ACD/Labs PhysChem Suite v12. The influence of the donor pH and concentration of pesticides, organic phase composition as well as the extraction time on the extraction efficiency was investigated. Optimum extraction conditions were evaluated with respect to the investigated parameters of the extraction. The extraction method was validated for 10 out of 16 studied pesticides. Linear range of the pesticides was 0.1-5 A mu g L(-1) with the correlation coefficient from 0.991 to 0.9998, and the relative standard deviation for three standard measurements was between 0.2 and 11.8%. The limits of detections ranged from 0.026 to 0.237 A mu g L(-1) and the limits of quantifications from 0.094 to 0.793 A mu g L(-1). The optimised two-phase HF-LPME method was successfully applied for determination of moderately polar as well low-polar pesticides in the environmental water samples.",
journal = "Analytical and Bioanalytical Chemistry",
title = "Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry",
pages = "2243-2233",
number = "6",
volume = "397",
doi = "10.1007/s00216-010-3725-5"
}
Trtić-Petrović, T. M., Đorđević, J. S., Dujaković, N., Kumrić, K., Vasiljević, T.,& Laušević, M.. (2010). Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry. in Analytical and Bioanalytical Chemistry, 397(6), 2233-2243.
https://doi.org/10.1007/s00216-010-3725-5
Trtić-Petrović TM, Đorđević JS, Dujaković N, Kumrić K, Vasiljević T, Laušević M. Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry. in Analytical and Bioanalytical Chemistry. 2010;397(6):2233-2243.
doi:10.1007/s00216-010-3725-5 .
Trtić-Petrović, Tatjana M., Đorđević, Jelena S., Dujaković, Nikolina, Kumrić, Ksenija, Vasiljević, Tatjana, Laušević, Mila, "Determination of selected pesticides in environmental water by employing liquid-phase microextraction and liquid chromatography-tandem mass spectrometry" in Analytical and Bioanalytical Chemistry, 397, no. 6 (2010):2233-2243,
https://doi.org/10.1007/s00216-010-3725-5 . .
52
41
49

Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester

Kaluđerović, Goran N.; Vasiljević, Tanja M.; Laušević, Mila D.; Gaballa, Akmal S.; Sabo, Tibor

(Springer Wien, Wien, 2009)

TY  - JOUR
AU  - Kaluđerović, Goran N.
AU  - Vasiljević, Tanja M.
AU  - Laušević, Mila D.
AU  - Gaballa, Akmal S.
AU  - Sabo, Tibor
PY  - 2009
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5526
AB  - The electrospray mass spectrometric (ESI-MS) behavior of the complexes trans-dichloro(ethylenediamine-N, N'-di-3-propionato) platinum(IV), trans-dibromo(ethylenediamine-N, N'-di-3-propionato) platinum( IV), dichloro (ethylenediamine-N,N'-di-3-propionic acid) platinum(II), tetrachloro(O,O'-di-n-butyl-ethylenediamine-N,N'-di-3-propanoate) platinum(IV), chlorotribromo(O,O'-di-n-butylethylenediamine-N,N'-di-3-propanoate) platinum(IV), and dichloro(O,O'-di-n-butyl-ethylenediamine-N,N'-di-3-propanoate) platinum( II), with the formulae trans-[PtCl(2) (eddp)] (1), trans-[PtBr(2)(eddp)] (2), [PtCl(2)(H(2)eddp)] (3), [PtCl(4)(Bu(2)eddp)] (4), [PtBr(3)Cl(Bu(2)eddp)] (5), and [PtCl(2)(Bu(2)eddp)]center dot H(2)O (6), is reported. The deprotonated molecular ions or halide adducts are usually observed. ESI-MS data demonstrate the usefulness of the method for efficient characterization of metal complexes in solution.
PB  - Springer Wien, Wien
T2  - Monatshefte Fur Chemie
T1  - Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester
EP  - 557
IS  - 5
SP  - 553
VL  - 140
DO  - 10.1007/s00706-008-0088-0
ER  - 
@article{
author = "Kaluđerović, Goran N. and Vasiljević, Tanja M. and Laušević, Mila D. and Gaballa, Akmal S. and Sabo, Tibor",
year = "2009",
abstract = "The electrospray mass spectrometric (ESI-MS) behavior of the complexes trans-dichloro(ethylenediamine-N, N'-di-3-propionato) platinum(IV), trans-dibromo(ethylenediamine-N, N'-di-3-propionato) platinum( IV), dichloro (ethylenediamine-N,N'-di-3-propionic acid) platinum(II), tetrachloro(O,O'-di-n-butyl-ethylenediamine-N,N'-di-3-propanoate) platinum(IV), chlorotribromo(O,O'-di-n-butylethylenediamine-N,N'-di-3-propanoate) platinum(IV), and dichloro(O,O'-di-n-butyl-ethylenediamine-N,N'-di-3-propanoate) platinum( II), with the formulae trans-[PtCl(2) (eddp)] (1), trans-[PtBr(2)(eddp)] (2), [PtCl(2)(H(2)eddp)] (3), [PtCl(4)(Bu(2)eddp)] (4), [PtBr(3)Cl(Bu(2)eddp)] (5), and [PtCl(2)(Bu(2)eddp)]center dot H(2)O (6), is reported. The deprotonated molecular ions or halide adducts are usually observed. ESI-MS data demonstrate the usefulness of the method for efficient characterization of metal complexes in solution.",
publisher = "Springer Wien, Wien",
journal = "Monatshefte Fur Chemie",
title = "Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester",
pages = "557-553",
number = "5",
volume = "140",
doi = "10.1007/s00706-008-0088-0"
}
Kaluđerović, G. N., Vasiljević, T. M., Laušević, M. D., Gaballa, A. S.,& Sabo, T.. (2009). Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester. in Monatshefte Fur Chemie
Springer Wien, Wien., 140(5), 553-557.
https://doi.org/10.1007/s00706-008-0088-0
Kaluđerović GN, Vasiljević TM, Laušević MD, Gaballa AS, Sabo T. Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester. in Monatshefte Fur Chemie. 2009;140(5):553-557.
doi:10.1007/s00706-008-0088-0 .
Kaluđerović, Goran N., Vasiljević, Tanja M., Laušević, Mila D., Gaballa, Akmal S., Sabo, Tibor, "Electrospray mass spectrometric studies of a potential antitumor drug and its analogous platinum(II) and platinum(IV) complexes with the ethylenediamine-N,N '-di-3-propanoato ligand and its dibutyl ester" in Monatshefte Fur Chemie, 140, no. 5 (2009):553-557,
https://doi.org/10.1007/s00706-008-0088-0 . .
6
6
6

Surface composition and adsorption properties of activated carbon cloth

Vasiljević, Tatjana; Baćić, Marija; Laušević, Mila; Onjia, Antonije

(Belgrade : Institute of Technical Sciences of SASA, 2003)

TY  - CONF
AU  - Vasiljević, Tatjana
AU  - Baćić, Marija
AU  - Laušević, Mila
AU  - Onjia, Antonije
PY  - 2003
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7127
AB  - Surface properties of activated carbons have shown to play an important role in
adsorption process. The presence of various functional groups (such as phenolic, carbonyl,
carboxylic) on the carbon surface depends on the nature of its base component and the activation
technique employed in the manufacturing process.
The aim of this work is to gain a better fundamental understanding of the nature of
surface oxide sites present on activated carbon cloth surface (ACC), and their role in the
adsorption process. BET surface areas of ACC were measured by means of benzene adsorption
isotherms. The amount and the type of surface oxygen groups were determined by
thermogravimetric analysis and classical titration following Boehm’s method. Batch adsorption
tests were used to evaluate equilibrium adsorption isotherms of phenol on ACC.
It was shown that both surface area and surface groups composition had impact on adsorption
properties of ACC against phenol.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Programme and The Book of Abstracts / Fifth Annual Conference YUCOMAT 2003, Herceg Novi, September 15-19, 2003
T1  - Surface composition and adsorption properties of activated carbon cloth
SP  - 90
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7127
ER  - 
@conference{
author = "Vasiljević, Tatjana and Baćić, Marija and Laušević, Mila and Onjia, Antonije",
year = "2003",
abstract = "Surface properties of activated carbons have shown to play an important role in
adsorption process. The presence of various functional groups (such as phenolic, carbonyl,
carboxylic) on the carbon surface depends on the nature of its base component and the activation
technique employed in the manufacturing process.
The aim of this work is to gain a better fundamental understanding of the nature of
surface oxide sites present on activated carbon cloth surface (ACC), and their role in the
adsorption process. BET surface areas of ACC were measured by means of benzene adsorption
isotherms. The amount and the type of surface oxygen groups were determined by
thermogravimetric analysis and classical titration following Boehm’s method. Batch adsorption
tests were used to evaluate equilibrium adsorption isotherms of phenol on ACC.
It was shown that both surface area and surface groups composition had impact on adsorption
properties of ACC against phenol.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Programme and The Book of Abstracts / Fifth Annual Conference YUCOMAT 2003, Herceg Novi, September 15-19, 2003",
title = "Surface composition and adsorption properties of activated carbon cloth",
pages = "90",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7127"
}
Vasiljević, T., Baćić, M., Laušević, M.,& Onjia, A.. (2003). Surface composition and adsorption properties of activated carbon cloth. in Programme and The Book of Abstracts / Fifth Annual Conference YUCOMAT 2003, Herceg Novi, September 15-19, 2003
Belgrade : Institute of Technical Sciences of SASA., 90.
https://hdl.handle.net/21.15107/rcub_technorep_7127
Vasiljević T, Baćić M, Laušević M, Onjia A. Surface composition and adsorption properties of activated carbon cloth. in Programme and The Book of Abstracts / Fifth Annual Conference YUCOMAT 2003, Herceg Novi, September 15-19, 2003. 2003;:90.
https://hdl.handle.net/21.15107/rcub_technorep_7127 .
Vasiljević, Tatjana, Baćić, Marija, Laušević, Mila, Onjia, Antonije, "Surface composition and adsorption properties of activated carbon cloth" in Programme and The Book of Abstracts / Fifth Annual Conference YUCOMAT 2003, Herceg Novi, September 15-19, 2003 (2003):90,
https://hdl.handle.net/21.15107/rcub_technorep_7127 .

Mikrokapilarni reaktor za konverziju CO u CO2

Onjia, Antonije; Laušević, Mila; Laušević, Zoran; Mitrović, Milan

(Srpsko hemijsko društvo, 1993)

TY  - CONF
AU  - Onjia, Antonije
AU  - Laušević, Mila
AU  - Laušević, Zoran
AU  - Mitrović, Milan
PY  - 1993
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6543
AB  - The alcrocapillary carbon supporting carposite platinum catalyst rOd distributed. Palls pores has been Installed into inside chefurnace and tested as oxidation of reactor F6=carbon sonoxide catalytic inlet of the rod was connected carboa sloxide. The valve and outlet was connected-o a tuse supplyinz co-o2 the to she ras. Las chromatogrash tases reselting E=o= chein orde detect product COg has been detested cacalycie Feaocion. The 200-556 0. in with 95% yield the temperature range.
PB  - Srpsko hemijsko društvo
C3  - 2. Simpozijum Hemija i zaštita životne sredine, Vrnjačka Banja
T1  - Mikrokapilarni reaktor za konverziju CO u CO2
EP  - 458
SP  - 457
UR  - https://hdl.handle.net/21.15107/rcub_technorep_6543
ER  - 
@conference{
author = "Onjia, Antonije and Laušević, Mila and Laušević, Zoran and Mitrović, Milan",
year = "1993",
abstract = "The alcrocapillary carbon supporting carposite platinum catalyst rOd distributed. Palls pores has been Installed into inside chefurnace and tested as oxidation of reactor F6=carbon sonoxide catalytic inlet of the rod was connected carboa sloxide. The valve and outlet was connected-o a tuse supplyinz co-o2 the to she ras. Las chromatogrash tases reselting E=o= chein orde detect product COg has been detested cacalycie Feaocion. The 200-556 0. in with 95% yield the temperature range.",
publisher = "Srpsko hemijsko društvo",
journal = "2. Simpozijum Hemija i zaštita životne sredine, Vrnjačka Banja",
title = "Mikrokapilarni reaktor za konverziju CO u CO2",
pages = "458-457",
url = "https://hdl.handle.net/21.15107/rcub_technorep_6543"
}
Onjia, A., Laušević, M., Laušević, Z.,& Mitrović, M.. (1993). Mikrokapilarni reaktor za konverziju CO u CO2. in 2. Simpozijum Hemija i zaštita životne sredine, Vrnjačka Banja
Srpsko hemijsko društvo., 457-458.
https://hdl.handle.net/21.15107/rcub_technorep_6543
Onjia A, Laušević M, Laušević Z, Mitrović M. Mikrokapilarni reaktor za konverziju CO u CO2. in 2. Simpozijum Hemija i zaštita životne sredine, Vrnjačka Banja. 1993;:457-458.
https://hdl.handle.net/21.15107/rcub_technorep_6543 .
Onjia, Antonije, Laušević, Mila, Laušević, Zoran, Mitrović, Milan, "Mikrokapilarni reaktor za konverziju CO u CO2" in 2. Simpozijum Hemija i zaštita životne sredine, Vrnjačka Banja (1993):457-458,
https://hdl.handle.net/21.15107/rcub_technorep_6543 .