Omerašević, Mia

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Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting

Omerašević, Mia; Krsmanović, Miomir; Radovanović, Željko; Bučevac, Dušan

(Elsevier Ltd., 2024)

TY  - JOUR
AU  - Omerašević, Mia
AU  - Krsmanović, Miomir
AU  - Radovanović, Željko
AU  - Bučevac, Dušan
PY  - 2024
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6991
AB  - Anorthite ceramics (CaAl2Si2O8) was obtained by slip casting of water suspension of kaolin (Al2O3·2SiO2·2H2O) and CaCO3 as a source of CaO. A relative density of 87 % of the theoretical density was achieved after a 3-h-long sintering of green samples at 1200 °C. It was found that slip casting allows the fabrication of anorthite with relatively small pores (<8 μm) which was beneficial for achieving a high fracture strength of 129 MPa and good thermal shock resistance. For a quantitative measurement of thermal shock resistance, a critical temperature interval (ΔTc) was determined by a reduction in the mean fracture strength of at least 30 %. The experimentally determined ΔTc of 300 °C was higher than the value calculated by the equation assuming that the thermal stress created during quenching causes the fracture. It was found that the discrepancy between experimental and calculated values of ΔTc could be explained by an introduction of cracks of various sizes by indentation method and careful observation of crack growth initiation after quenching from various temperatures. It is believed that the reason for the discrepancy lies in the different nature of stress that was used in the theoretical calculation and the stress that acts during sample quenching.
PB  - Elsevier Ltd.
T2  - Ceramics International
T1  - Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting
EP  - 5795
IS  - 3
SP  - 5787
VL  - 50
DO  - 10.1016/j.ceramint.2023.11.381
ER  - 
@article{
author = "Omerašević, Mia and Krsmanović, Miomir and Radovanović, Željko and Bučevac, Dušan",
year = "2024",
abstract = "Anorthite ceramics (CaAl2Si2O8) was obtained by slip casting of water suspension of kaolin (Al2O3·2SiO2·2H2O) and CaCO3 as a source of CaO. A relative density of 87 % of the theoretical density was achieved after a 3-h-long sintering of green samples at 1200 °C. It was found that slip casting allows the fabrication of anorthite with relatively small pores (<8 μm) which was beneficial for achieving a high fracture strength of 129 MPa and good thermal shock resistance. For a quantitative measurement of thermal shock resistance, a critical temperature interval (ΔTc) was determined by a reduction in the mean fracture strength of at least 30 %. The experimentally determined ΔTc of 300 °C was higher than the value calculated by the equation assuming that the thermal stress created during quenching causes the fracture. It was found that the discrepancy between experimental and calculated values of ΔTc could be explained by an introduction of cracks of various sizes by indentation method and careful observation of crack growth initiation after quenching from various temperatures. It is believed that the reason for the discrepancy lies in the different nature of stress that was used in the theoretical calculation and the stress that acts during sample quenching.",
publisher = "Elsevier Ltd.",
journal = "Ceramics International",
title = "Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting",
pages = "5795-5787",
number = "3",
volume = "50",
doi = "10.1016/j.ceramint.2023.11.381"
}
Omerašević, M., Krsmanović, M., Radovanović, Ž.,& Bučevac, D.. (2024). Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting. in Ceramics International
Elsevier Ltd.., 50(3), 5787-5795.
https://doi.org/10.1016/j.ceramint.2023.11.381
Omerašević M, Krsmanović M, Radovanović Ž, Bučevac D. Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting. in Ceramics International. 2024;50(3):5787-5795.
doi:10.1016/j.ceramint.2023.11.381 .
Omerašević, Mia, Krsmanović, Miomir, Radovanović, Željko, Bučevac, Dušan, "Mechanical properties and thermal shock resistance of anorthite ceramics obtained by slip casting" in Ceramics International, 50, no. 3 (2024):5787-5795,
https://doi.org/10.1016/j.ceramint.2023.11.381 . .
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