Knežević, Sanja

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  • Knežević, Sanja (1)
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Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA

Ivanović, Marija; Knežević, Sanja; Radović, Ivona; Kljajević, Ljiljana; Mirković, Miljana; Nenadović, Miloš; Nenadović, Snežana

(MDPI, 2023)

TY  - JOUR
AU  - Ivanović, Marija
AU  - Knežević, Sanja
AU  - Radović, Ivona
AU  - Kljajević, Ljiljana
AU  - Mirković, Miljana
AU  - Nenadović, Miloš
AU  - Nenadović, Snežana
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6311
AB  - Geopolymers have excellent physical and mechanical properties, so they can be used as a substitute for ordinary polymers. Geopolymers are ceramic materials, which exhibit the property of brittleness, which can be a limitation in some structural applications. To overcome this shortcoming, a new group of materials (organic geopolymers) was developed. The aim of this work is the synthesis of organic (hybrid) geopolymers. A geopolymer based on metakaolin was synthesized as a reference sample, while polyvinyl alcohol was added as an organic phase for synthesizing a hybrid geopolymer. It was concluded that the systems follow the rule of behavior in liquid systems. The chemical composition of the samples was determined by X-ray fluorescence analysis (XRF). Structural and phase characterization of hybrid and reference materials were analyzed using X-ray diffraction (XRD)and Fourier-transform infrared spectroscopy (FTIR), which revealed new phases in the PVA-added samples. The results show that the content of added PVA in the reaction mixture affects the phase composition of the synthesized materials. To examine the possibility of adsorption of the samples, Ultraviolet-visible spectroscopy (UV/VIS) was used. The morphology was analyzed using a scanning electron microscope with energy dispersive spectroscopy (SEM/EDS), where efflorescence was observed and identified. After characterizing the geopolymer with the addition of PVA, we obtained a material that was far more porous than the basic sample, and we can conclude that we have synthesized a material that shows good mechanical properties.
PB  - MDPI
T2  - Sustainability (Switzerland)
T1  - Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA
IS  - 5
SP  - 4441
VL  - 15
DO  - 10.3390/su15054441
ER  - 
@article{
author = "Ivanović, Marija and Knežević, Sanja and Radović, Ivona and Kljajević, Ljiljana and Mirković, Miljana and Nenadović, Miloš and Nenadović, Snežana",
year = "2023",
abstract = "Geopolymers have excellent physical and mechanical properties, so they can be used as a substitute for ordinary polymers. Geopolymers are ceramic materials, which exhibit the property of brittleness, which can be a limitation in some structural applications. To overcome this shortcoming, a new group of materials (organic geopolymers) was developed. The aim of this work is the synthesis of organic (hybrid) geopolymers. A geopolymer based on metakaolin was synthesized as a reference sample, while polyvinyl alcohol was added as an organic phase for synthesizing a hybrid geopolymer. It was concluded that the systems follow the rule of behavior in liquid systems. The chemical composition of the samples was determined by X-ray fluorescence analysis (XRF). Structural and phase characterization of hybrid and reference materials were analyzed using X-ray diffraction (XRD)and Fourier-transform infrared spectroscopy (FTIR), which revealed new phases in the PVA-added samples. The results show that the content of added PVA in the reaction mixture affects the phase composition of the synthesized materials. To examine the possibility of adsorption of the samples, Ultraviolet-visible spectroscopy (UV/VIS) was used. The morphology was analyzed using a scanning electron microscope with energy dispersive spectroscopy (SEM/EDS), where efflorescence was observed and identified. After characterizing the geopolymer with the addition of PVA, we obtained a material that was far more porous than the basic sample, and we can conclude that we have synthesized a material that shows good mechanical properties.",
publisher = "MDPI",
journal = "Sustainability (Switzerland)",
title = "Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA",
number = "5",
pages = "4441",
volume = "15",
doi = "10.3390/su15054441"
}
Ivanović, M., Knežević, S., Radović, I., Kljajević, L., Mirković, M., Nenadović, M.,& Nenadović, S.. (2023). Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA. in Sustainability (Switzerland)
MDPI., 15(5), 4441.
https://doi.org/10.3390/su15054441
Ivanović M, Knežević S, Radović I, Kljajević L, Mirković M, Nenadović M, Nenadović S. Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA. in Sustainability (Switzerland). 2023;15(5):4441.
doi:10.3390/su15054441 .
Ivanović, Marija, Knežević, Sanja, Radović, Ivona, Kljajević, Ljiljana, Mirković, Miljana, Nenadović, Miloš, Nenadović, Snežana, "Preparation and Characterization of Geopolymers Based on Metakaolin with the Addition of Organic Phase PVA" in Sustainability (Switzerland), 15, no. 5 (2023):4441,
https://doi.org/10.3390/su15054441 . .