TY  - CONF
AU  - Vidak Vasić, Milica
AU  - Radovanović, Lidija
AU  - Radojević, Zagorka
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7357
AB  - The study makes a unique effort to characterize all the necessary characteristics of refractory clays and products fired at
temperatures between 1100 and 1300 °C on a laboratory level. For 19 composite samples from the recently opened
reservoir, thorough instrumental and ceramic-technological data are presented. The potential for using Serbian raw
refractory clays from the recently discovered deposit is investigated. The composites had a variety of qualities and varied
in composition, but they were majorly composed of kaolinite and illite and had a significant share of fluxes. The samples
had high quantities of clay minerals and organic matter, which is seen as the most intense mass loss in the 400–600 °C
range. Low-duty and high-duty refractories could be distinguished by their refractoriness over 1581 °C. This parameter
was mostly influenced by the content of alumina and kaolinite within the materials. Hydraulically-pressed ceramic tiles,
following the firing stage, showed water absorption was between 9.02–1.42 % and a modulus of rupture of 16.5 – 53.6
MPa. Color is determined by spectrophotometer and correlated to the composition of the initial clay and fired products.
For the lining of ceramic and glass furnaces, the majority of these clays can be used as natural refractory materials. Some
of the samples' organic content has a detrimental effect on the fast-firing procedure, since the occurrence of the entrapped
air (bloating).
PB  - Belgrade : Association of Metallurgical Engineers of Serbia (AMES)
C3  - Congress Proceedings / 5th Metallurgical & Materials Engineering Congress of South-East Europe MME SEE Congress 2023, Trebinje, Bosnia and Herzegovina 7-10th June 2023
T1  - Raw kaolinitic-illitic clays for the production of refractory ceramics
EP  - 22
SP  - 17
UR  - https://hdl.handle.net/21.15107/rcub_technorep_7357
ER  - 

@conference{
author = "Vidak Vasić, Milica and Radovanović, Lidija and Radojević, Zagorka",
year = "2023",
abstract = "The study makes a unique effort to characterize all the necessary characteristics of refractory clays and products fired at
temperatures between 1100 and 1300 °C on a laboratory level. For 19 composite samples from the recently opened
reservoir, thorough instrumental and ceramic-technological data are presented. The potential for using Serbian raw
refractory clays from the recently discovered deposit is investigated. The composites had a variety of qualities and varied
in composition, but they were majorly composed of kaolinite and illite and had a significant share of fluxes. The samples
had high quantities of clay minerals and organic matter, which is seen as the most intense mass loss in the 400–600 °C
range. Low-duty and high-duty refractories could be distinguished by their refractoriness over 1581 °C. This parameter
was mostly influenced by the content of alumina and kaolinite within the materials. Hydraulically-pressed ceramic tiles,
following the firing stage, showed water absorption was between 9.02–1.42 % and a modulus of rupture of 16.5 – 53.6
MPa. Color is determined by spectrophotometer and correlated to the composition of the initial clay and fired products.
For the lining of ceramic and glass furnaces, the majority of these clays can be used as natural refractory materials. Some
of the samples' organic content has a detrimental effect on the fast-firing procedure, since the occurrence of the entrapped
air (bloating).",
publisher = "Belgrade : Association of Metallurgical Engineers of Serbia (AMES)",
journal = "Congress Proceedings / 5th Metallurgical & Materials Engineering Congress of South-East Europe MME SEE Congress 2023, Trebinje, Bosnia and Herzegovina 7-10th June 2023",
title = "Raw kaolinitic-illitic clays for the production of refractory ceramics",
pages = "22-17",
url = "https://hdl.handle.net/21.15107/rcub_technorep_7357"
}

Vidak Vasić, M., Radovanović, L.,& Radojević, Z.. (2023). Raw kaolinitic-illitic clays for the production of refractory ceramics. in Congress Proceedings / 5th Metallurgical & Materials Engineering Congress of South-East Europe MME SEE Congress 2023, Trebinje, Bosnia and Herzegovina 7-10th June 2023
Belgrade : Association of Metallurgical Engineers of Serbia (AMES)., 17-22.
https://hdl.handle.net/21.15107/rcub_technorep_7357

Vidak Vasić M, Radovanović L, Radojević Z. Raw kaolinitic-illitic clays for the production of refractory ceramics. in Congress Proceedings / 5th Metallurgical & Materials Engineering Congress of South-East Europe MME SEE Congress 2023, Trebinje, Bosnia and Herzegovina 7-10th June 2023. 2023;:17-22.
https://hdl.handle.net/21.15107/rcub_technorep_7357 .

Vidak Vasić, Milica, Radovanović, Lidija, Radojević, Zagorka, "Raw kaolinitic-illitic clays for the production of refractory ceramics" in Congress Proceedings / 5th Metallurgical & Materials Engineering Congress of South-East Europe MME SEE Congress 2023, Trebinje, Bosnia and Herzegovina 7-10th June 2023 (2023):17-22,
https://hdl.handle.net/21.15107/rcub_technorep_7357 .

TY  - JOUR
AU  - Radovanović, Lidija
AU  - Radovanović, Željko
AU  - Simović, Bojana
AU  - Vasić, Milica V.
AU  - Balanč, Bojana
AU  - Dapčević, Aleksandra
AU  - Dramićanin, Miroslav D.
AU  - Rogan, Jelena
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5984
AB  - A biphasic [Mn(dipya)(H2O)4](tpht)/{[Zn(dipya)(tpht)]·H2O}n com­plex material, I (dipya = 2,2’-dipyridylamine, tpht2– = dianion of terephthalatic acid) was synthesized by ligand exchange reaction and characterized by XRPD and FTIR spectroscopy. A ZnO/ZnMn2O4 composite, II, has been prepared via thermal decomposition of I in an air atmosphere at 450 °C. XRPD, FTIR and FESEM analyses of II revealed the simultaneous presence of spherical nano­particles of wurtzite ZnO and elongated nanoparticles of spinel ZnMn2O4. The specific surface area of II was determined by the BET method, whereas the volume and average size of the mesopores were calculated in accordance with the BJH method. The measurements of the mean size, polydispersity index and zeta potential showed colloidal instability of II. Two band gap values of 2.4 and 3.3 eV were determined using UV–Vis diffuse reflectance spectroscopy, while the measurements of photoluminescence revealed that II is active in the blue region of the visible spectrum. Testing of composite II as a pigmentary material showed that it can be used for the colouring of a ceramic glaze.
AB  - Двофазни  [Mn(dipya)(H2O)4](tpht)/{[Zn(dipya)(tpht)]·H2O}n комплексни материјал, I,  (dipya  =  2,2’-дипиридиламин,  tpht2–  =  дианјон  1,4-бензендикарбоксилнекиселине) синтетисан је реакцијом измене лиганада и окарактерисан XRPD мeтoдоми FTIR спек-троскопијом. Композит ZnO/ZnMn2O4, II, добијен је термичком разградњом прекурcopa I у атмосфери ваздуха на  450  °C.  XRPD  мeтoдом,  FTIR  спектроскопијом и  FESEM  микроскопијом композита II утврђено је истовремено присуство сферних наночестица ZnO вирцитне структуре и издужених наночестица  ZnMn2O4 са структуром спинела. Специфична површина композита II одређена је BET методом, док су запремина и просечна величина мезопора израчунати у складу са  BJH  методом. Средња величина, индекс полидисперзије и цета потенцијал измерени су фотонском корелационом спектроскопијом и електрофоретским расејањем светлости и показали су нестабилност композита II. Вредности ширине забрањене зоне од  2,4  и  3,3  eV  одређене су  UV–Vis  дифузно-рефлексионом спектроскопијом, док су мерења фотолуминесценције показала да је композит II активан у плавој области видљивог дела спектра. Испитивање композита II као пигментног материјала показало је да се може користити за бојење керамичке глазуре.
PB  - Serbian Chemical Society
T2  - Journal of the Serbian Chemical Society
T1  - Structure and properties of ZnO/ZnMn2O4 composite obtained by thermal decomposition of terephthalate precursor
T1  - Структура и својства композита ZnO/ZnMn2O4 добијеног термичком разградњом терефталат-прекурсора
EP  - 325
IS  - 3
SP  - 313
VL  - 88
DO  - 10.2298/JSC221102090R
ER  - 

@article{
author = "Radovanović, Lidija and Radovanović, Željko and Simović, Bojana and Vasić, Milica V. and Balanč, Bojana and Dapčević, Aleksandra and Dramićanin, Miroslav D. and Rogan, Jelena",
year = "2023",
abstract = "A biphasic [Mn(dipya)(H2O)4](tpht)/{[Zn(dipya)(tpht)]·H2O}n com­plex material, I (dipya = 2,2’-dipyridylamine, tpht2– = dianion of terephthalatic acid) was synthesized by ligand exchange reaction and characterized by XRPD and FTIR spectroscopy. A ZnO/ZnMn2O4 composite, II, has been prepared via thermal decomposition of I in an air atmosphere at 450 °C. XRPD, FTIR and FESEM analyses of II revealed the simultaneous presence of spherical nano­particles of wurtzite ZnO and elongated nanoparticles of spinel ZnMn2O4. The specific surface area of II was determined by the BET method, whereas the volume and average size of the mesopores were calculated in accordance with the BJH method. The measurements of the mean size, polydispersity index and zeta potential showed colloidal instability of II. Two band gap values of 2.4 and 3.3 eV were determined using UV–Vis diffuse reflectance spectroscopy, while the measurements of photoluminescence revealed that II is active in the blue region of the visible spectrum. Testing of composite II as a pigmentary material showed that it can be used for the colouring of a ceramic glaze., Двофазни  [Mn(dipya)(H2O)4](tpht)/{[Zn(dipya)(tpht)]·H2O}n комплексни материјал, I,  (dipya  =  2,2’-дипиридиламин,  tpht2–  =  дианјон  1,4-бензендикарбоксилнекиселине) синтетисан је реакцијом измене лиганада и окарактерисан XRPD мeтoдоми FTIR спек-троскопијом. Композит ZnO/ZnMn2O4, II, добијен је термичком разградњом прекурcopa I у атмосфери ваздуха на  450  °C.  XRPD  мeтoдом,  FTIR  спектроскопијом и  FESEM  микроскопијом композита II утврђено је истовремено присуство сферних наночестица ZnO вирцитне структуре и издужених наночестица  ZnMn2O4 са структуром спинела. Специфична површина композита II одређена је BET методом, док су запремина и просечна величина мезопора израчунати у складу са  BJH  методом. Средња величина, индекс полидисперзије и цета потенцијал измерени су фотонском корелационом спектроскопијом и електрофоретским расејањем светлости и показали су нестабилност композита II. Вредности ширине забрањене зоне од  2,4  и  3,3  eV  одређене су  UV–Vis  дифузно-рефлексионом спектроскопијом, док су мерења фотолуминесценције показала да је композит II активан у плавој области видљивог дела спектра. Испитивање композита II као пигментног материјала показало је да се може користити за бојење керамичке глазуре.",
publisher = "Serbian Chemical Society",
journal = "Journal of the Serbian Chemical Society",
title = "Structure and properties of ZnO/ZnMn2O4 composite obtained by thermal decomposition of terephthalate precursor, Структура и својства композита ZnO/ZnMn2O4 добијеног термичком разградњом терефталат-прекурсора",
pages = "325-313",
number = "3",
volume = "88",
doi = "10.2298/JSC221102090R"
}

Radovanović, L., Radovanović, Ž., Simović, B., Vasić, M. V., Balanč, B., Dapčević, A., Dramićanin, M. D.,& Rogan, J.. (2023). Structure and properties of ZnO/ZnMn2O4 composite obtained by thermal decomposition of terephthalate precursor. in Journal of the Serbian Chemical Society
Serbian Chemical Society., 88(3), 313-325.
https://doi.org/10.2298/JSC221102090R

Radovanović L, Radovanović Ž, Simović B, Vasić MV, Balanč B, Dapčević A, Dramićanin MD, Rogan J. Structure and properties of ZnO/ZnMn2O4 composite obtained by thermal decomposition of terephthalate precursor. in Journal of the Serbian Chemical Society. 2023;88(3):313-325.
doi:10.2298/JSC221102090R .

Radovanović, Lidija, Radovanović, Željko, Simović, Bojana, Vasić, Milica V., Balanč, Bojana, Dapčević, Aleksandra, Dramićanin, Miroslav D., Rogan, Jelena, "Structure and properties of ZnO/ZnMn2O4 composite obtained by thermal decomposition of terephthalate precursor" in Journal of the Serbian Chemical Society, 88, no. 3 (2023):313-325,
https://doi.org/10.2298/JSC221102090R . .

TY  - JOUR
AU  - Mijatović, Nevenka
AU  - Vasić, Milica
AU  - Miličić, Ljiljana
AU  - Radomirović, Milena
AU  - Radojević, Zagorka
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5193
AB  - In this paper, the main subject concerns comparing different techniques to prepare raw clay samples for energy-dispersive X-ray fluorescence spectrometry (EDXRF). Three kinds of sample preparation procedures are examined, such as loose powder, pressed pellet, and fired pressed pellet. The fired pressed pellet approach was observed as a part of universal sample preparation for physic, mechanical, and instrumental analysis, which has not been previously tested as a solution in chemical analysis by the EDXRF method. The observed sample preparation techniques were compared by calculating the parameters of validation (recoveries, limit of detection - LOD, limit of quantification - LOQ, precision, and expanded uncertainties of measurements) of 11 elements (Si, Al, Fe, Ca, Mg, K, Na, Ti, P, Mn, and S) using 15 certified reference materials (CRMs). Calibration curves were created and evaluated using 30 reference materials (RM) for all three approaches. Results proved that the fired pressed pellet is the most practical and precise approach for sample preparation of raw clays.
PB  - Elsevier B.V.
T2  - Talanta
T1  - Fired pressed pellet as a sample preparation technique of choice for an energy dispersive X-ray fluorescence analysis of raw clays
SP  - 123844
VL  - 252
DO  - 10.1016/j.talanta.2022.123844
ER  - 

@article{
author = "Mijatović, Nevenka and Vasić, Milica and Miličić, Ljiljana and Radomirović, Milena and Radojević, Zagorka",
year = "2023",
abstract = "In this paper, the main subject concerns comparing different techniques to prepare raw clay samples for energy-dispersive X-ray fluorescence spectrometry (EDXRF). Three kinds of sample preparation procedures are examined, such as loose powder, pressed pellet, and fired pressed pellet. The fired pressed pellet approach was observed as a part of universal sample preparation for physic, mechanical, and instrumental analysis, which has not been previously tested as a solution in chemical analysis by the EDXRF method. The observed sample preparation techniques were compared by calculating the parameters of validation (recoveries, limit of detection - LOD, limit of quantification - LOQ, precision, and expanded uncertainties of measurements) of 11 elements (Si, Al, Fe, Ca, Mg, K, Na, Ti, P, Mn, and S) using 15 certified reference materials (CRMs). Calibration curves were created and evaluated using 30 reference materials (RM) for all three approaches. Results proved that the fired pressed pellet is the most practical and precise approach for sample preparation of raw clays.",
publisher = "Elsevier B.V.",
journal = "Talanta",
title = "Fired pressed pellet as a sample preparation technique of choice for an energy dispersive X-ray fluorescence analysis of raw clays",
pages = "123844",
volume = "252",
doi = "10.1016/j.talanta.2022.123844"
}

Mijatović, N., Vasić, M., Miličić, L., Radomirović, M.,& Radojević, Z.. (2023). Fired pressed pellet as a sample preparation technique of choice for an energy dispersive X-ray fluorescence analysis of raw clays. in Talanta
Elsevier B.V.., 252, 123844.
https://doi.org/10.1016/j.talanta.2022.123844

Mijatović N, Vasić M, Miličić L, Radomirović M, Radojević Z. Fired pressed pellet as a sample preparation technique of choice for an energy dispersive X-ray fluorescence analysis of raw clays. in Talanta. 2023;252:123844.
doi:10.1016/j.talanta.2022.123844 .

Mijatović, Nevenka, Vasić, Milica, Miličić, Ljiljana, Radomirović, Milena, Radojević, Zagorka, "Fired pressed pellet as a sample preparation technique of choice for an energy dispersive X-ray fluorescence analysis of raw clays" in Talanta, 252 (2023):123844,
https://doi.org/10.1016/j.talanta.2022.123844 . .

TY  - JOUR
AU  - Mijatović, Nevenka
AU  - Vasić, Milica
AU  - Terzić, Anja
AU  - Radomirović, Milena
AU  - Miličić, Ljiljana
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6634
AB  - The chemical compositions of refractory materials, such as high-alumina concrete, bricks, and putty, were analyzed using an energy-dispersive X-ray spectrometer (EDXRF). An improved methodology for investigating the effect of particle size on the outcomes of EDXRF chemical analysis is presented. Eight independent refractory samples (refractory concrete, brick, and putty) were pulverized utilizing seven milling times (30, 60, 120, 180, 240, 300, and 360 s) and compared to non-pulverized samples. Thus, sixty-four refractory samples were obtained and analyzed using EDXRF. The method for measuring the fundamental EDXRF characteristics was then tested with ten certified reference materials. The acquired data were compared using inductively coupled plasma atomic emission spectrometry (ICP-OES). Univariate and multivariate statistics are used to evaluate EDXRF data. The particle size of the tested samples affected the z-scores of SiO2, Al2O3, Fe2O3, TiO2, CaO, MgO, Na2O, K2O, and P2O5 concentration measurements. Grinding times for refractory concrete, brick, and putty samples were determined in order to validate the robustness of the EDXRF technique and provide reliable chemical analyses. The ideal milling times for the samples studied ranged from 180 to 360 s, depending on the type of refractory material.
PB  - Elsevier B.V.
T2  - Spectrochimica Acta - Part B Atomic Spectroscopy
T1  - An augmented approach for the determination of the particle size effect on energy dispersive X-ray fluorescence analysis outcomes for alumina-based refractory materials
SP  - 106796
VL  - 209
DO  - 10.1016/j.sab.2023.106796
ER  - 

@article{
author = "Mijatović, Nevenka and Vasić, Milica and Terzić, Anja and Radomirović, Milena and Miličić, Ljiljana",
year = "2023",
abstract = "The chemical compositions of refractory materials, such as high-alumina concrete, bricks, and putty, were analyzed using an energy-dispersive X-ray spectrometer (EDXRF). An improved methodology for investigating the effect of particle size on the outcomes of EDXRF chemical analysis is presented. Eight independent refractory samples (refractory concrete, brick, and putty) were pulverized utilizing seven milling times (30, 60, 120, 180, 240, 300, and 360 s) and compared to non-pulverized samples. Thus, sixty-four refractory samples were obtained and analyzed using EDXRF. The method for measuring the fundamental EDXRF characteristics was then tested with ten certified reference materials. The acquired data were compared using inductively coupled plasma atomic emission spectrometry (ICP-OES). Univariate and multivariate statistics are used to evaluate EDXRF data. The particle size of the tested samples affected the z-scores of SiO2, Al2O3, Fe2O3, TiO2, CaO, MgO, Na2O, K2O, and P2O5 concentration measurements. Grinding times for refractory concrete, brick, and putty samples were determined in order to validate the robustness of the EDXRF technique and provide reliable chemical analyses. The ideal milling times for the samples studied ranged from 180 to 360 s, depending on the type of refractory material.",
publisher = "Elsevier B.V.",
journal = "Spectrochimica Acta - Part B Atomic Spectroscopy",
title = "An augmented approach for the determination of the particle size effect on energy dispersive X-ray fluorescence analysis outcomes for alumina-based refractory materials",
pages = "106796",
volume = "209",
doi = "10.1016/j.sab.2023.106796"
}

Mijatović, N., Vasić, M., Terzić, A., Radomirović, M.,& Miličić, L.. (2023). An augmented approach for the determination of the particle size effect on energy dispersive X-ray fluorescence analysis outcomes for alumina-based refractory materials. in Spectrochimica Acta - Part B Atomic Spectroscopy
Elsevier B.V.., 209, 106796.
https://doi.org/10.1016/j.sab.2023.106796

Mijatović N, Vasić M, Terzić A, Radomirović M, Miličić L. An augmented approach for the determination of the particle size effect on energy dispersive X-ray fluorescence analysis outcomes for alumina-based refractory materials. in Spectrochimica Acta - Part B Atomic Spectroscopy. 2023;209:106796.
doi:10.1016/j.sab.2023.106796 .

Mijatović, Nevenka, Vasić, Milica, Terzić, Anja, Radomirović, Milena, Miličić, Ljiljana, "An augmented approach for the determination of the particle size effect on energy dispersive X-ray fluorescence analysis outcomes for alumina-based refractory materials" in Spectrochimica Acta - Part B Atomic Spectroscopy, 209 (2023):106796,
https://doi.org/10.1016/j.sab.2023.106796 . .

TY  - JOUR
AU  - Aleksić, Vujadin
AU  - Milović, Ljubica
AU  - Zečević, Bojana
AU  - Bulatović, Srđan
PY  - 2023
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5289
AB  - Fracture mechanics, as a scientific discipline dealing with the study of cracks in welded structures, has defined parameters and introduced new test methods in order to better determine the tendency to crack growth, critical conditions for rapid fracture development, material resistance to rapid crack propagation and better definition of other parameters for assessing the behaviour of the material and the safety of the structure in the presence of cracks. In this paper, the focus is on determination of the parameter of elastic-plastic mechanics of J-integral, more precisely, on examination of the critical value of J-integral (JIc) of the welded joint of HSLA steel. The position of the tip of the fatigue crack and the properties of the region where fracture propagation occurs are main indicators of influence of the heterogeneity of the NN-70 welded structure and mechanical properties. Resistance to cracking in the welded joint shows that the heterogeneity has a major impact on the resistance to crack initiation and propagation, in elastic as well as in the plastic region.
PB  - Strojarski Facultet
T2  - Tehnicki Vjesnik
T1  - Experimental Determination of the Critical Value of the J-Integral that Refers to the HSLA Steel Welded Joint
EP  - 152
IS  - 1
SP  - 148
VL  - 30
DO  - 10.17559/TV-20220419093052
ER  - 

@article{
author = "Aleksić, Vujadin and Milović, Ljubica and Zečević, Bojana and Bulatović, Srđan",
year = "2023",
abstract = "Fracture mechanics, as a scientific discipline dealing with the study of cracks in welded structures, has defined parameters and introduced new test methods in order to better determine the tendency to crack growth, critical conditions for rapid fracture development, material resistance to rapid crack propagation and better definition of other parameters for assessing the behaviour of the material and the safety of the structure in the presence of cracks. In this paper, the focus is on determination of the parameter of elastic-plastic mechanics of J-integral, more precisely, on examination of the critical value of J-integral (JIc) of the welded joint of HSLA steel. The position of the tip of the fatigue crack and the properties of the region where fracture propagation occurs are main indicators of influence of the heterogeneity of the NN-70 welded structure and mechanical properties. Resistance to cracking in the welded joint shows that the heterogeneity has a major impact on the resistance to crack initiation and propagation, in elastic as well as in the plastic region.",
publisher = "Strojarski Facultet",
journal = "Tehnicki Vjesnik",
title = "Experimental Determination of the Critical Value of the J-Integral that Refers to the HSLA Steel Welded Joint",
pages = "152-148",
number = "1",
volume = "30",
doi = "10.17559/TV-20220419093052"
}

Aleksić, V., Milović, L., Zečević, B.,& Bulatović, S.. (2023). Experimental Determination of the Critical Value of the J-Integral that Refers to the HSLA Steel Welded Joint. in Tehnicki Vjesnik
Strojarski Facultet., 30(1), 148-152.
https://doi.org/10.17559/TV-20220419093052

Aleksić V, Milović L, Zečević B, Bulatović S. Experimental Determination of the Critical Value of the J-Integral that Refers to the HSLA Steel Welded Joint. in Tehnicki Vjesnik. 2023;30(1):148-152.
doi:10.17559/TV-20220419093052 .

Aleksić, Vujadin, Milović, Ljubica, Zečević, Bojana, Bulatović, Srđan, "Experimental Determination of the Critical Value of the J-Integral that Refers to the HSLA Steel Welded Joint" in Tehnicki Vjesnik, 30, no. 1 (2023):148-152,
https://doi.org/10.17559/TV-20220419093052 . .

TY  - CONF
AU  - Aleksić, Vujadin
AU  - Milović, Ljubica
AU  - Bulatović, Srđan
AU  - Zečević, Bojana
AU  - Maksimović, Ana
PY  - 2022
UR  - http://rims.institutims.rs/handle/123456789/416
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5126
AB  - The behavior of steel in low-cycle fatigue (LCF) is tested experimentally, in accordance with ISO 12106:2017 (E) and/or ASTM E 606-04. For this purpose, smooth specimens which are exposed to low-cycle fatigue at several levels of regulated strains and/or loads at room, elevated or reduced temperatures are used. Stress–strain response at LCF has the shape of an ideal hysteresis loop. The strain range Δε corresponds to overall loop width, while the stress range Δσ corresponds to its overall height. The paper presents a method for determining the intersection of the idealized hysteresis loop and the positive part of the strain axis in order to determine the values of elastic, Δεe/2, and plastic, Δεp/2, components of the strain amplitude to characterize the behavior of steel under low cyclic fatigue. The values of elastic and plastic components of the strain amplitude are needed to determine the characteristic curves of low-cycle fatigue, which describe the behavior of steel under the loading of low-cycle fatigue.
PB  - Springer Science and Business Media B.V.
C3  - Mechanisms and Machine Science
T1  - Determination of LCF Plastic and Elastic Strain Components of Steel
EP  - 349
SP  - 341
VL  - 109
DO  - 10.1007/978-3-030-88465-9_32
ER  - 

@conference{
author = "Aleksić, Vujadin and Milović, Ljubica and Bulatović, Srđan and Zečević, Bojana and Maksimović, Ana",
year = "2022",
abstract = "The behavior of steel in low-cycle fatigue (LCF) is tested experimentally, in accordance with ISO 12106:2017 (E) and/or ASTM E 606-04. For this purpose, smooth specimens which are exposed to low-cycle fatigue at several levels of regulated strains and/or loads at room, elevated or reduced temperatures are used. Stress–strain response at LCF has the shape of an ideal hysteresis loop. The strain range Δε corresponds to overall loop width, while the stress range Δσ corresponds to its overall height. The paper presents a method for determining the intersection of the idealized hysteresis loop and the positive part of the strain axis in order to determine the values of elastic, Δεe/2, and plastic, Δεp/2, components of the strain amplitude to characterize the behavior of steel under low cyclic fatigue. The values of elastic and plastic components of the strain amplitude are needed to determine the characteristic curves of low-cycle fatigue, which describe the behavior of steel under the loading of low-cycle fatigue.",
publisher = "Springer Science and Business Media B.V.",
journal = "Mechanisms and Machine Science",
title = "Determination of LCF Plastic and Elastic Strain Components of Steel",
pages = "349-341",
volume = "109",
doi = "10.1007/978-3-030-88465-9_32"
}

Aleksić, V., Milović, L., Bulatović, S., Zečević, B.,& Maksimović, A.. (2022). Determination of LCF Plastic and Elastic Strain Components of Steel. in Mechanisms and Machine Science
Springer Science and Business Media B.V.., 109, 341-349.
https://doi.org/10.1007/978-3-030-88465-9_32

Aleksić V, Milović L, Bulatović S, Zečević B, Maksimović A. Determination of LCF Plastic and Elastic Strain Components of Steel. in Mechanisms and Machine Science. 2022;109:341-349.
doi:10.1007/978-3-030-88465-9_32 .

Aleksić, Vujadin, Milović, Ljubica, Bulatović, Srđan, Zečević, Bojana, Maksimović, Ana, "Determination of LCF Plastic and Elastic Strain Components of Steel" in Mechanisms and Machine Science, 109 (2022):341-349,
https://doi.org/10.1007/978-3-030-88465-9_32 . .

TY  - JOUR
AU  - Aleksić, Vujadin
AU  - Bulatović, Srđan
AU  - Zečević, Bojana
AU  - Maksimović, Ana
AU  - Milović, Ljubica
PY  - 2022
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5290
AB  - The design of mechanical components exposed to fatigue load, at a low number of cycles, requires knowledge of the behaviour of the material under the impact of variable load in conditions of controlled strain when cyclic plasticity is present. The aim of testing the quality of the material of the components exposed to low cycle fatigue (LCF) in many industries: Nuclear, aerospace, mechanical, civil engineering and shipbuilding. In order to ensure the reliability and consistency of the results from different laboratories, it is necessary to collect all test data using test and data processing methodologies that are in accordance with a number of key points of ISO 12106: 2017 and/or ASTM E 606-04 standards. This paper defines a new data processing methodology after the LCF testing of steel.
PB  - University of Zagreb Faculty of Mechanical Engineering and Naval Architecture
T2  - Transactions of Famena
T1  - Processing of Data Obtained by the Testing of Steel under Low Cyclic Fatigue (Part I)
EP  - 72
IS  - 4
SP  - 59
VL  - 46
DO  - 10.21278/TOF.464041622
ER  - 

@article{
author = "Aleksić, Vujadin and Bulatović, Srđan and Zečević, Bojana and Maksimović, Ana and Milović, Ljubica",
year = "2022",
abstract = "The design of mechanical components exposed to fatigue load, at a low number of cycles, requires knowledge of the behaviour of the material under the impact of variable load in conditions of controlled strain when cyclic plasticity is present. The aim of testing the quality of the material of the components exposed to low cycle fatigue (LCF) in many industries: Nuclear, aerospace, mechanical, civil engineering and shipbuilding. In order to ensure the reliability and consistency of the results from different laboratories, it is necessary to collect all test data using test and data processing methodologies that are in accordance with a number of key points of ISO 12106: 2017 and/or ASTM E 606-04 standards. This paper defines a new data processing methodology after the LCF testing of steel.",
publisher = "University of Zagreb Faculty of Mechanical Engineering and Naval Architecture",
journal = "Transactions of Famena",
title = "Processing of Data Obtained by the Testing of Steel under Low Cyclic Fatigue (Part I)",
pages = "72-59",
number = "4",
volume = "46",
doi = "10.21278/TOF.464041622"
}

Aleksić, V., Bulatović, S., Zečević, B., Maksimović, A.,& Milović, L.. (2022). Processing of Data Obtained by the Testing of Steel under Low Cyclic Fatigue (Part I). in Transactions of Famena
University of Zagreb Faculty of Mechanical Engineering and Naval Architecture., 46(4), 59-72.
https://doi.org/10.21278/TOF.464041622

Aleksić V, Bulatović S, Zečević B, Maksimović A, Milović L. Processing of Data Obtained by the Testing of Steel under Low Cyclic Fatigue (Part I). in Transactions of Famena. 2022;46(4):59-72.
doi:10.21278/TOF.464041622 .

Aleksić, Vujadin, Bulatović, Srđan, Zečević, Bojana, Maksimović, Ana, Milović, Ljubica, "Processing of Data Obtained by the Testing of Steel under Low Cyclic Fatigue (Part I)" in Transactions of Famena, 46, no. 4 (2022):59-72,
https://doi.org/10.21278/TOF.464041622 . .

TY  - JOUR
AU  - Bulatović, Srđan M.
AU  - Aleksić, Vujadin D.
AU  - Milović, Ljubica P.
AU  - Zečević, Bojana V.
PY  - 2022
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5011
AB  - The most important characteristics for service safety of welded joints are those describing crack initiation and growth caused by variable loading. Crack initiation and growth caused by variable loading is the subject of numerous investigations. This paper shows the determination of parameters of the fatigue crack for constituents of welded joints produced of high strength low alloyed steel. The crack growth law of Paris establishes the relation between the applied variable load quantity or the corresponding stress intensity factor range and crack growth per cycle. Results have shown that the position of the notch and crack initiation affect the values of the stress intensity range of fatigue threshold Delta Kth and parameters in the Paris' equation.
PB  - Faculty of Mechanical Engineering, Belgrade University
T2  - FME Transactions
T1  - Application of Paris' Law Under Variable Loading
EP  - 78
IS  - 1
SP  - 72
VL  - 50
DO  - 10.5937/fme2201072B
ER  - 

@article{
author = "Bulatović, Srđan M. and Aleksić, Vujadin D. and Milović, Ljubica P. and Zečević, Bojana V.",
year = "2022",
abstract = "The most important characteristics for service safety of welded joints are those describing crack initiation and growth caused by variable loading. Crack initiation and growth caused by variable loading is the subject of numerous investigations. This paper shows the determination of parameters of the fatigue crack for constituents of welded joints produced of high strength low alloyed steel. The crack growth law of Paris establishes the relation between the applied variable load quantity or the corresponding stress intensity factor range and crack growth per cycle. Results have shown that the position of the notch and crack initiation affect the values of the stress intensity range of fatigue threshold Delta Kth and parameters in the Paris' equation.",
publisher = "Faculty of Mechanical Engineering, Belgrade University",
journal = "FME Transactions",
title = "Application of Paris' Law Under Variable Loading",
pages = "78-72",
number = "1",
volume = "50",
doi = "10.5937/fme2201072B"
}

Bulatović, S. M., Aleksić, V. D., Milović, L. P.,& Zečević, B. V.. (2022). Application of Paris' Law Under Variable Loading. in FME Transactions
Faculty of Mechanical Engineering, Belgrade University., 50(1), 72-78.
https://doi.org/10.5937/fme2201072B

Bulatović SM, Aleksić VD, Milović LP, Zečević BV. Application of Paris' Law Under Variable Loading. in FME Transactions. 2022;50(1):72-78.
doi:10.5937/fme2201072B .

Bulatović, Srđan M., Aleksić, Vujadin D., Milović, Ljubica P., Zečević, Bojana V., "Application of Paris' Law Under Variable Loading" in FME Transactions, 50, no. 1 (2022):72-78,
https://doi.org/10.5937/fme2201072B . .

TY  - JOUR
AU  - Vidak Vasić, Milica
AU  - Terzić, Anja
AU  - Radovanović, Željko
AU  - Radojević, Zagorka
AU  - Warr, Laurence N.
PY  - 2022
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5301
AB  - Geopolymerization was investigated as an alternative to traditional ceramic products by developing a more sustainable approach that avoids thermal treatment. The study presents the first known alkali-activation of the raw clay and waste clay brick mixture using the solid to liquid ratios of 2.33 and 2.78. Several experimental sets were prepared to harden under varying conditions (2–4 days drying in 60 °C–70 °C and 3 h steam-curing). Non-activated and activated samples were analyzed for their physical and chemical properties after 14, 21, and 28 days. The tile-shaped specimens exhibited better initial drying behavior than the cubes and produced stronger materials with fewer cracks. Pre-curing in steam conditions induced higher flexural strength (13.7 MPa) and water absorption (13.13%) for the geopolymer tiles. The highest Si/Al molar ratio in the amorphous portion of 5.78 induced the best flexural strength. The geopolymerization process showed microstructural changes associated with the appearance of fibrous Na-zeolite nanocrystals. The degree of geopolymerization and zeolite formation was enhanced by steam-curing, but the microstructural stress and heterogeneity induced by the reactions resulted in higher water absorption. Ongoing reactions of amorphization in the bulk material and further crystallization at the surface are documented after 6 months of curing. This first detailed study reveals that the production of geopolymer ceramics from brick waste is possible, but further optimization of the activating solution and curing parameters is required.
PB  - Elsevier Ltd.
T2  - Applied Clay Science
T1  - Alkali-activated geopolymerization of a low illitic raw clay and waste brick mixture. An alternative to traditional ceramics
SP  - 106410
VL  - 218
DO  - 10.1016/j.clay.2022.106410
ER  - 

@article{
author = "Vidak Vasić, Milica and Terzić, Anja and Radovanović, Željko and Radojević, Zagorka and Warr, Laurence N.",
year = "2022",
abstract = "Geopolymerization was investigated as an alternative to traditional ceramic products by developing a more sustainable approach that avoids thermal treatment. The study presents the first known alkali-activation of the raw clay and waste clay brick mixture using the solid to liquid ratios of 2.33 and 2.78. Several experimental sets were prepared to harden under varying conditions (2–4 days drying in 60 °C–70 °C and 3 h steam-curing). Non-activated and activated samples were analyzed for their physical and chemical properties after 14, 21, and 28 days. The tile-shaped specimens exhibited better initial drying behavior than the cubes and produced stronger materials with fewer cracks. Pre-curing in steam conditions induced higher flexural strength (13.7 MPa) and water absorption (13.13%) for the geopolymer tiles. The highest Si/Al molar ratio in the amorphous portion of 5.78 induced the best flexural strength. The geopolymerization process showed microstructural changes associated with the appearance of fibrous Na-zeolite nanocrystals. The degree of geopolymerization and zeolite formation was enhanced by steam-curing, but the microstructural stress and heterogeneity induced by the reactions resulted in higher water absorption. Ongoing reactions of amorphization in the bulk material and further crystallization at the surface are documented after 6 months of curing. This first detailed study reveals that the production of geopolymer ceramics from brick waste is possible, but further optimization of the activating solution and curing parameters is required.",
publisher = "Elsevier Ltd.",
journal = "Applied Clay Science",
title = "Alkali-activated geopolymerization of a low illitic raw clay and waste brick mixture. An alternative to traditional ceramics",
pages = "106410",
volume = "218",
doi = "10.1016/j.clay.2022.106410"
}

Vidak Vasić, M., Terzić, A., Radovanović, Ž., Radojević, Z.,& Warr, L. N.. (2022). Alkali-activated geopolymerization of a low illitic raw clay and waste brick mixture. An alternative to traditional ceramics. in Applied Clay Science
Elsevier Ltd.., 218, 106410.
https://doi.org/10.1016/j.clay.2022.106410

Vidak Vasić M, Terzić A, Radovanović Ž, Radojević Z, Warr LN. Alkali-activated geopolymerization of a low illitic raw clay and waste brick mixture. An alternative to traditional ceramics. in Applied Clay Science. 2022;218:106410.
doi:10.1016/j.clay.2022.106410 .

Vidak Vasić, Milica, Terzić, Anja, Radovanović, Željko, Radojević, Zagorka, Warr, Laurence N., "Alkali-activated geopolymerization of a low illitic raw clay and waste brick mixture. An alternative to traditional ceramics" in Applied Clay Science, 218 (2022):106410,
https://doi.org/10.1016/j.clay.2022.106410 . .

TY  - JOUR
AU  - Vidak Vasić, Milica
AU  - Radovanović, Lidija
AU  - Pezo, Lato
AU  - Radojević, Zagorka
PY  - 2022
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5291
AB  - The usage possibility of 19 composites of raw refractory clays from Serbia containing approximately 53.29% of SiO2 and 26.73% of Al2O3 is presented. The sum of fluxing oxides was 57.74%, while these materials contained 32% of quartz, 29% of kaolinite and 26% of illite–mica. Dilatometry tests revealed a sudden shrinkage with the peak at approximately 1115 °C, owing to the formation of mullite. The refractoriness was in the range of 1581–1718 °C, which classifies the composites from low- to high-duty refractories. Based on correlation analysis, the refractoriness mostly depended on the content of alumina. The lightness of the fired test pieces was lower after firing when compared to the dry samples, and it decreased with the firing temperature from reddish to grayish. The study presents a novel attempt to define all the necessary properties of raw refractory clays and products fired at the 1100–1300 °C range on a laboratory level. Most of these clays can be used as natural refractory materials for ceramic and glass furnace lining. The organic matter in some of the samples influences negatively the fast-firing process.
PB  - Springer Science and Business Media B.V.
T2  - Journal of Thermal Analysis and Calorimetry
T1  - Raw kaolinitic–illitic clays as high-mechanical-performance hydraulically pressed refractories
EP  - 1803
IS  - 5
SP  - 1783
VL  - 148
DO  - 10.1007/s10973-022-11848-w
ER  - 

@article{
author = "Vidak Vasić, Milica and Radovanović, Lidija and Pezo, Lato and Radojević, Zagorka",
year = "2022",
abstract = "The usage possibility of 19 composites of raw refractory clays from Serbia containing approximately 53.29% of SiO2 and 26.73% of Al2O3 is presented. The sum of fluxing oxides was 57.74%, while these materials contained 32% of quartz, 29% of kaolinite and 26% of illite–mica. Dilatometry tests revealed a sudden shrinkage with the peak at approximately 1115 °C, owing to the formation of mullite. The refractoriness was in the range of 1581–1718 °C, which classifies the composites from low- to high-duty refractories. Based on correlation analysis, the refractoriness mostly depended on the content of alumina. The lightness of the fired test pieces was lower after firing when compared to the dry samples, and it decreased with the firing temperature from reddish to grayish. The study presents a novel attempt to define all the necessary properties of raw refractory clays and products fired at the 1100–1300 °C range on a laboratory level. Most of these clays can be used as natural refractory materials for ceramic and glass furnace lining. The organic matter in some of the samples influences negatively the fast-firing process.",
publisher = "Springer Science and Business Media B.V.",
journal = "Journal of Thermal Analysis and Calorimetry",
title = "Raw kaolinitic–illitic clays as high-mechanical-performance hydraulically pressed refractories",
pages = "1803-1783",
number = "5",
volume = "148",
doi = "10.1007/s10973-022-11848-w"
}

Vidak Vasić, M., Radovanović, L., Pezo, L.,& Radojević, Z.. (2022). Raw kaolinitic–illitic clays as high-mechanical-performance hydraulically pressed refractories. in Journal of Thermal Analysis and Calorimetry
Springer Science and Business Media B.V.., 148(5), 1783-1803.
https://doi.org/10.1007/s10973-022-11848-w

Vidak Vasić M, Radovanović L, Pezo L, Radojević Z. Raw kaolinitic–illitic clays as high-mechanical-performance hydraulically pressed refractories. in Journal of Thermal Analysis and Calorimetry. 2022;148(5):1783-1803.
doi:10.1007/s10973-022-11848-w .

Vidak Vasić, Milica, Radovanović, Lidija, Pezo, Lato, Radojević, Zagorka, "Raw kaolinitic–illitic clays as high-mechanical-performance hydraulically pressed refractories" in Journal of Thermal Analysis and Calorimetry, 148, no. 5 (2022):1783-1803,
https://doi.org/10.1007/s10973-022-11848-w . .

TY  - JOUR
AU  - Aleksić, Vujadin
AU  - Dojčinović, Marina
AU  - Milović, Ljubica
AU  - Zečević, Bojana
AU  - Maksimović, Ana
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5623
AB  - Polomljene epruvete za ispitivanje niskocikličnim zamorom čelika Nionikral 70 (NN-70) osnovnog materijala (OM) i simulirane zone pod uticajem toplote (SZUT) poslužile su NAM za izradu uzoraka za ispitivanje otpornosti na kavitaciju. Za ispitivanje u laboratorijskim uslovima primenjena je ultrazvučna vibraciona metoda kavitacije (metoda stacionarnog uzorka). Uslovi i procedura ispitivanja, priprema uzoraka kao i interpretacija rezultata definisani su standardom ASTM G32. Površine uzoraka čelika NN-70 OM i SZUT bile su izložene dejstvu kavitacije i praćenju oštećenja kroz određeno vreme. Merenje gubitka mase uzoraka na analitičkoj vagi posle određenog vremena omogućilo NAM je određivanje kavitacione brzine kao mere procene otpornosti materijala na dejstvo kavitacije. Za praćenje varijacija u morfologiji površine s promenom vremena ispitivanja primenjena je skenirajuća elektronska mikroskopija (SEM). Na osnovu rezultata ispitivanja otpornosti na kavitaciju u radu su analizirane morfologije oštećenja površina za različita vremena izlaganja dejstvu kavitacije uzoraka OM i SZUT čelika NN-70 kao i mehanizmi koji su doveli do oštećenja površina uzoraka.
AB  - Broken test tubes for low-cycle fatigue testing of Nionicral 70 (NN-70) parent material (PM) steel and simulated heat-affected zones (SHAZ) were used to produce samples for cavitation resistance testing. Ultrasonic vibrational cavitation method (stationary sample method) was applied for testing in laboratory conditions. The test conditions and procedure, sample preparation and interpretation of results are defined by ASTM G32. The surfaces of the NN-70 PM and SHAZ steel samples were exposed to cavitation and damage monitoring over time. Measuring the weight loss of samples on the analytical balance after a certain time allowed us to determine the cavitation velocity as a measure of the material's resistance to the effect of cavitation. Scanning electron microscopy (SEM) was applied to monitor variations in surface morphology with changing test time. On the basis of the results of the cavitation resistance test, the morphologies of the surface damage for different exposure times of the cavitation of PM and SHAZ steel NN-70 samples were analyzed, as well as the mechanisms that led to the damage of the sample surfaces.
PB  - Inženjersko društvo za koroziju, Beograd
T2  - Zaštita materijala
T1  - Mehanizmi i morfologije kavitacionog oštećenja čelika Nionikral 70
T1  - Mechanisms and morphologies of cavitation damage of NN 70 steel
EP  - 105
IS  - 2
SP  - 95
VL  - 2021
DO  - 10.5937/zasmat2102095A
ER  - 

@article{
author = "Aleksić, Vujadin and Dojčinović, Marina and Milović, Ljubica and Zečević, Bojana and Maksimović, Ana",
year = "2021",
abstract = "Polomljene epruvete za ispitivanje niskocikličnim zamorom čelika Nionikral 70 (NN-70) osnovnog materijala (OM) i simulirane zone pod uticajem toplote (SZUT) poslužile su NAM za izradu uzoraka za ispitivanje otpornosti na kavitaciju. Za ispitivanje u laboratorijskim uslovima primenjena je ultrazvučna vibraciona metoda kavitacije (metoda stacionarnog uzorka). Uslovi i procedura ispitivanja, priprema uzoraka kao i interpretacija rezultata definisani su standardom ASTM G32. Površine uzoraka čelika NN-70 OM i SZUT bile su izložene dejstvu kavitacije i praćenju oštećenja kroz određeno vreme. Merenje gubitka mase uzoraka na analitičkoj vagi posle određenog vremena omogućilo NAM je određivanje kavitacione brzine kao mere procene otpornosti materijala na dejstvo kavitacije. Za praćenje varijacija u morfologiji površine s promenom vremena ispitivanja primenjena je skenirajuća elektronska mikroskopija (SEM). Na osnovu rezultata ispitivanja otpornosti na kavitaciju u radu su analizirane morfologije oštećenja površina za različita vremena izlaganja dejstvu kavitacije uzoraka OM i SZUT čelika NN-70 kao i mehanizmi koji su doveli do oštećenja površina uzoraka., Broken test tubes for low-cycle fatigue testing of Nionicral 70 (NN-70) parent material (PM) steel and simulated heat-affected zones (SHAZ) were used to produce samples for cavitation resistance testing. Ultrasonic vibrational cavitation method (stationary sample method) was applied for testing in laboratory conditions. The test conditions and procedure, sample preparation and interpretation of results are defined by ASTM G32. The surfaces of the NN-70 PM and SHAZ steel samples were exposed to cavitation and damage monitoring over time. Measuring the weight loss of samples on the analytical balance after a certain time allowed us to determine the cavitation velocity as a measure of the material's resistance to the effect of cavitation. Scanning electron microscopy (SEM) was applied to monitor variations in surface morphology with changing test time. On the basis of the results of the cavitation resistance test, the morphologies of the surface damage for different exposure times of the cavitation of PM and SHAZ steel NN-70 samples were analyzed, as well as the mechanisms that led to the damage of the sample surfaces.",
publisher = "Inženjersko društvo za koroziju, Beograd",
journal = "Zaštita materijala",
title = "Mehanizmi i morfologije kavitacionog oštećenja čelika Nionikral 70, Mechanisms and morphologies of cavitation damage of NN 70 steel",
pages = "105-95",
number = "2",
volume = "2021",
doi = "10.5937/zasmat2102095A"
}

Aleksić, V., Dojčinović, M., Milović, L., Zečević, B.,& Maksimović, A.. (2021). Mehanizmi i morfologije kavitacionog oštećenja čelika Nionikral 70. in Zaštita materijala
Inženjersko društvo za koroziju, Beograd., 2021(2), 95-105.
https://doi.org/10.5937/zasmat2102095A

Aleksić V, Dojčinović M, Milović L, Zečević B, Maksimović A. Mehanizmi i morfologije kavitacionog oštećenja čelika Nionikral 70. in Zaštita materijala. 2021;2021(2):95-105.
doi:10.5937/zasmat2102095A .

Aleksić, Vujadin, Dojčinović, Marina, Milović, Ljubica, Zečević, Bojana, Maksimović, Ana, "Mehanizmi i morfologije kavitacionog oštećenja čelika Nionikral 70" in Zaštita materijala, 2021, no. 2 (2021):95-105,
https://doi.org/10.5937/zasmat2102095A . .

TY  - JOUR
AU  - Terzic, Anja
AU  - Dojčinović, Marina
AU  - Milicic, Ljiljana
AU  - Stojanovic, Jovica
AU  - Radojevic, Zagorka
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4958
AB  - Micro-silica is a highly efficient mineral additive whose role is reflected in improvements of microstructure packing, strength and durability of non-shaped composite building materials such as concrete and mortar. A comparative study of performances of rendering mortars with different quantities of micro silica was conducted. The experimental program included production of reference mortar based on Portland cement and quartz sand (CM) and three mortars with 5, 10, and 15 % addition of micro silica (SCM-5, SCM-10, and SCM-15). The effect that micro silica addition has on the thermal behavior and mechanical properties of mortars was discussed. Hydration mechanisms and thermally induced reactions were studied at temperatures ranging from ambient to 1100 degrees C by differential thermal analysis. The results were supported by X-ray diffraction analysis. The cementing efficiency of micro silica was assessed by cavitation erosion test. The changes in the morphology of mortar samples prior and upon cavitation testing were monitored by means of the scanning electron microscope imagining. It was found that 5 % of superfine micro silica (SCM-5 mortar) has positive effects on mechanical strengths (15 % increase in compressive strength) due to microstructure densification arising from the successive filling of voids by the micro silica. Addition of micro silica also improved the cavitation erosion resistance in comparison with reference cement mortar (SCM-5 showed cavitation velocity as low as 0.09 mg/min). This qualifies mortars with micro silica addition as building materials which can be safely employed in potential hydro-demolition environment.
T2  - Science of Sintering
T1  - Cavitation Properties of Rendering Mortars with Micro Silica Addition
EP  - 459
IS  - 4
SP  - 445
VL  - 53
DO  - 10.2298/SOS2104445T
ER  - 

@article{
author = "Terzic, Anja and Dojčinović, Marina and Milicic, Ljiljana and Stojanovic, Jovica and Radojevic, Zagorka",
year = "2021",
abstract = "Micro-silica is a highly efficient mineral additive whose role is reflected in improvements of microstructure packing, strength and durability of non-shaped composite building materials such as concrete and mortar. A comparative study of performances of rendering mortars with different quantities of micro silica was conducted. The experimental program included production of reference mortar based on Portland cement and quartz sand (CM) and three mortars with 5, 10, and 15 % addition of micro silica (SCM-5, SCM-10, and SCM-15). The effect that micro silica addition has on the thermal behavior and mechanical properties of mortars was discussed. Hydration mechanisms and thermally induced reactions were studied at temperatures ranging from ambient to 1100 degrees C by differential thermal analysis. The results were supported by X-ray diffraction analysis. The cementing efficiency of micro silica was assessed by cavitation erosion test. The changes in the morphology of mortar samples prior and upon cavitation testing were monitored by means of the scanning electron microscope imagining. It was found that 5 % of superfine micro silica (SCM-5 mortar) has positive effects on mechanical strengths (15 % increase in compressive strength) due to microstructure densification arising from the successive filling of voids by the micro silica. Addition of micro silica also improved the cavitation erosion resistance in comparison with reference cement mortar (SCM-5 showed cavitation velocity as low as 0.09 mg/min). This qualifies mortars with micro silica addition as building materials which can be safely employed in potential hydro-demolition environment.",
journal = "Science of Sintering",
title = "Cavitation Properties of Rendering Mortars with Micro Silica Addition",
pages = "459-445",
number = "4",
volume = "53",
doi = "10.2298/SOS2104445T"
}

Terzic, A., Dojčinović, M., Milicic, L., Stojanovic, J.,& Radojevic, Z.. (2021). Cavitation Properties of Rendering Mortars with Micro Silica Addition. in Science of Sintering, 53(4), 445-459.
https://doi.org/10.2298/SOS2104445T

Terzic A, Dojčinović M, Milicic L, Stojanovic J, Radojevic Z. Cavitation Properties of Rendering Mortars with Micro Silica Addition. in Science of Sintering. 2021;53(4):445-459.
doi:10.2298/SOS2104445T .

Terzic, Anja, Dojčinović, Marina, Milicic, Ljiljana, Stojanovic, Jovica, Radojevic, Zagorka, "Cavitation Properties of Rendering Mortars with Micro Silica Addition" in Science of Sintering, 53, no. 4 (2021):445-459,
https://doi.org/10.2298/SOS2104445T . .

TY  - JOUR
AU  - Radomirović, Milena
AU  - Mijatovic, Nevenka
AU  - Vasic, Milica
AU  - Tanaskovski, Bojan
AU  - Mandic, Milica
AU  - Pezo, Lato
AU  - Onjia, Antonije
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4937
AB  - Surface sediments collected from twelve stations in the Boka Kotorska Bay were analyzed for the level and distribution of twenty-six elements and ten oxides, grain sizes, organic matter, and carbonate content. Potentially toxic elements (Al, Fe, Mn, Cr, Zn, Ni, Cu, Pb, As, Co, U) were determined to assess the contamination status and potential environmental risk according to the single-element indices (enrichment factor (EF), geoaccumulation index (Igeo), contamination factor (CF)), and combined index (pollution load index (PLI)). The single-element indices EF and CF revealed that the surface marine sediment was moderately polluted with Pb, Cu, and Cr, while Igeo indicated moderate pollution with Ni > Cr > Zn > Cu > As and moderate to heavy pollution with Pb, as a result of the anthropogenic factors. The method of the combined effect of toxic elements, PLI, showed the highest pollution rate at the shipyard location in the Bay of Tivat. Pearson's correlation coefficient (r), principal component analysis (PCA), and cluster analysis (CA) were applied to highlight similarities and differences in the distribution of the investigated elements in the Bay, confirming the claim obtained by the pollution indices. The sediment contamination with most heavy metals, such as Cr, Zn, Ni, Cu, Pb, and As, has been identified in the Tivat Bay area.
T2  - Environmental Science and Pollution Research
T1  - The characterization and pollution status of the surface sediment in the Boka Kotorska Bay, Montenegro
EP  - 53652
IS  - 38
SP  - 53629
VL  - 28
DO  - 10.1007/s11356-021-14382-8
ER  - 

@article{
author = "Radomirović, Milena and Mijatovic, Nevenka and Vasic, Milica and Tanaskovski, Bojan and Mandic, Milica and Pezo, Lato and Onjia, Antonije",
year = "2021",
abstract = "Surface sediments collected from twelve stations in the Boka Kotorska Bay were analyzed for the level and distribution of twenty-six elements and ten oxides, grain sizes, organic matter, and carbonate content. Potentially toxic elements (Al, Fe, Mn, Cr, Zn, Ni, Cu, Pb, As, Co, U) were determined to assess the contamination status and potential environmental risk according to the single-element indices (enrichment factor (EF), geoaccumulation index (Igeo), contamination factor (CF)), and combined index (pollution load index (PLI)). The single-element indices EF and CF revealed that the surface marine sediment was moderately polluted with Pb, Cu, and Cr, while Igeo indicated moderate pollution with Ni > Cr > Zn > Cu > As and moderate to heavy pollution with Pb, as a result of the anthropogenic factors. The method of the combined effect of toxic elements, PLI, showed the highest pollution rate at the shipyard location in the Bay of Tivat. Pearson's correlation coefficient (r), principal component analysis (PCA), and cluster analysis (CA) were applied to highlight similarities and differences in the distribution of the investigated elements in the Bay, confirming the claim obtained by the pollution indices. The sediment contamination with most heavy metals, such as Cr, Zn, Ni, Cu, Pb, and As, has been identified in the Tivat Bay area.",
journal = "Environmental Science and Pollution Research",
title = "The characterization and pollution status of the surface sediment in the Boka Kotorska Bay, Montenegro",
pages = "53652-53629",
number = "38",
volume = "28",
doi = "10.1007/s11356-021-14382-8"
}

Radomirović, M., Mijatovic, N., Vasic, M., Tanaskovski, B., Mandic, M., Pezo, L.,& Onjia, A.. (2021). The characterization and pollution status of the surface sediment in the Boka Kotorska Bay, Montenegro. in Environmental Science and Pollution Research, 28(38), 53629-53652.
https://doi.org/10.1007/s11356-021-14382-8

Radomirović M, Mijatovic N, Vasic M, Tanaskovski B, Mandic M, Pezo L, Onjia A. The characterization and pollution status of the surface sediment in the Boka Kotorska Bay, Montenegro. in Environmental Science and Pollution Research. 2021;28(38):53629-53652.
doi:10.1007/s11356-021-14382-8 .

Radomirović, Milena, Mijatovic, Nevenka, Vasic, Milica, Tanaskovski, Bojan, Mandic, Milica, Pezo, Lato, Onjia, Antonije, "The characterization and pollution status of the surface sediment in the Boka Kotorska Bay, Montenegro" in Environmental Science and Pollution Research, 28, no. 38 (2021):53629-53652,
https://doi.org/10.1007/s11356-021-14382-8 . .

TY  - JOUR
AU  - Bulatović, Srđan
AU  - Aleksić, Vujadin
AU  - Milović, Ljubica
AU  - Zečević, Bojana
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4789
AB  - Brittle damages have been examined widely since welding became common practice when it comes to carrying out robust structures. Welded structure of the ship hull has to be continuous. Brittle damages that occur on hull structures have always been examined thoroughly. Cracks are most commonly initiated at locations where stress concentrators exist. These concentrators can originate due to flaws that occur during the design phase or due to mistakes that occur during the assembly of the structure. When it comes to failures and damages that occur at ship structures, it has been noticed that damages due to brittleness practically always happen at low temperatures. Impact test analysis is significant due to the fact that it replicates the ductile to brittle transition of steel in practically identical range of temperatures for all ship structures. Impact of ductile-brittle transition temperature is an important factor especially because there have been many ship failures and damages in history. In ship structures made of welded joints of high strength low-alloy (HSLA) steels with their segments (parent metal, weld metal and heat-affected- zone), the toughness test determines the tendency of steel to brittle fracture, respectively the tendency to increase brittleness during exploitation. Parameters obtained by testing the properties of plasticity are the fundamental for the composition of ship structures with the aim of realize strengths under tested load. The test results of high strength low-alloy steel toughness assessment at different test temperatures show that temperature significantly affects the impact toughness of steels and their alloys.
T2  - Brodogradnja
T1  - An analysis of impact testing of high strength low-alloy steels used in ship construction
EP  - 12
IS  - 3
SP  - 1
VL  - 72
DO  - 10.21278/brod72301
ER  - 

@article{
author = "Bulatović, Srđan and Aleksić, Vujadin and Milović, Ljubica and Zečević, Bojana",
year = "2021",
abstract = "Brittle damages have been examined widely since welding became common practice when it comes to carrying out robust structures. Welded structure of the ship hull has to be continuous. Brittle damages that occur on hull structures have always been examined thoroughly. Cracks are most commonly initiated at locations where stress concentrators exist. These concentrators can originate due to flaws that occur during the design phase or due to mistakes that occur during the assembly of the structure. When it comes to failures and damages that occur at ship structures, it has been noticed that damages due to brittleness practically always happen at low temperatures. Impact test analysis is significant due to the fact that it replicates the ductile to brittle transition of steel in practically identical range of temperatures for all ship structures. Impact of ductile-brittle transition temperature is an important factor especially because there have been many ship failures and damages in history. In ship structures made of welded joints of high strength low-alloy (HSLA) steels with their segments (parent metal, weld metal and heat-affected- zone), the toughness test determines the tendency of steel to brittle fracture, respectively the tendency to increase brittleness during exploitation. Parameters obtained by testing the properties of plasticity are the fundamental for the composition of ship structures with the aim of realize strengths under tested load. The test results of high strength low-alloy steel toughness assessment at different test temperatures show that temperature significantly affects the impact toughness of steels and their alloys.",
journal = "Brodogradnja",
title = "An analysis of impact testing of high strength low-alloy steels used in ship construction",
pages = "12-1",
number = "3",
volume = "72",
doi = "10.21278/brod72301"
}

Bulatović, S., Aleksić, V., Milović, L.,& Zečević, B.. (2021). An analysis of impact testing of high strength low-alloy steels used in ship construction. in Brodogradnja, 72(3), 1-12.
https://doi.org/10.21278/brod72301

Bulatović S, Aleksić V, Milović L, Zečević B. An analysis of impact testing of high strength low-alloy steels used in ship construction. in Brodogradnja. 2021;72(3):1-12.
doi:10.21278/brod72301 .

Bulatović, Srđan, Aleksić, Vujadin, Milović, Ljubica, Zečević, Bojana, "An analysis of impact testing of high strength low-alloy steels used in ship construction" in Brodogradnja, 72, no. 3 (2021):1-12,
https://doi.org/10.21278/brod72301 . .

TY  - JOUR
AU  - Bulatović, Srđan
AU  - Aleksić, Vujadin
AU  - Milović, Ljubica
AU  - Zečević, Bojana
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4787
AB  - The cycle loading of a material results in the modification of its properties and so in this paper is presented the behaviour of the fatigue life using low-cycle fatigue parameters. By applying the Coffin-Manson equation in fatigue loading of the tested specimens, the crack initiation has been computed. The stabilized hysteresis loop is a characteristic of all hystereses and it is used to determine all of the parameters for the low cycle fatigue (LCF) assessment. The experimental results have given us important information on the understanding of fatigue behaviour of high strength low-alloyed steel (HSLA) and its welded joints.
T2  - Structural Integrity and Life-Integritet I Vek Konstrukcija
T1  - Determination of the coffin-manson equation under low-cycle fatigue conditions
EP  - 228
IS  - 3
SP  - 225
VL  - 21
UR  - https://hdl.handle.net/21.15107/rcub_technorep_4787
ER  - 

@article{
author = "Bulatović, Srđan and Aleksić, Vujadin and Milović, Ljubica and Zečević, Bojana",
year = "2021",
abstract = "The cycle loading of a material results in the modification of its properties and so in this paper is presented the behaviour of the fatigue life using low-cycle fatigue parameters. By applying the Coffin-Manson equation in fatigue loading of the tested specimens, the crack initiation has been computed. The stabilized hysteresis loop is a characteristic of all hystereses and it is used to determine all of the parameters for the low cycle fatigue (LCF) assessment. The experimental results have given us important information on the understanding of fatigue behaviour of high strength low-alloyed steel (HSLA) and its welded joints.",
journal = "Structural Integrity and Life-Integritet I Vek Konstrukcija",
title = "Determination of the coffin-manson equation under low-cycle fatigue conditions",
pages = "228-225",
number = "3",
volume = "21",
url = "https://hdl.handle.net/21.15107/rcub_technorep_4787"
}

Bulatović, S., Aleksić, V., Milović, L.,& Zečević, B.. (2021). Determination of the coffin-manson equation under low-cycle fatigue conditions. in Structural Integrity and Life-Integritet I Vek Konstrukcija, 21(3), 225-228.
https://hdl.handle.net/21.15107/rcub_technorep_4787

Bulatović S, Aleksić V, Milović L, Zečević B. Determination of the coffin-manson equation under low-cycle fatigue conditions. in Structural Integrity and Life-Integritet I Vek Konstrukcija. 2021;21(3):225-228.
https://hdl.handle.net/21.15107/rcub_technorep_4787 .

Bulatović, Srđan, Aleksić, Vujadin, Milović, Ljubica, Zečević, Bojana, "Determination of the coffin-manson equation under low-cycle fatigue conditions" in Structural Integrity and Life-Integritet I Vek Konstrukcija, 21, no. 3 (2021):225-228,
https://hdl.handle.net/21.15107/rcub_technorep_4787 .

TY  - JOUR
AU  - Međo, Bojan
AU  - Arsić, Miodrag
AU  - Mladenović, Mladen
AU  - Savić, Zoran
AU  - Grabulov, Vencislav
AU  - Radosavljević, Zoran
AU  - Rakin, Marko
PY  - 2020
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4567
AB  - Topic of this work is the integrity assessment of the pipeline section from hydropower plant Pirot. Crack-like defect size, maximum depth, is determined based on non-destructive evaluation - the largest crack depth is taken as the initial value for load carrying capacity estimation. Also, the crack dimensions (both length and depth) are varied. Limit pressure values are determined from 3D and 2D models of pipes with axial cracks on external surface. The influence of tensile loading on the load carrying capacity of the pipes with circumferential cracks is also examined. Integrity of pipes with both types of defects (axial and circumferential) is assessed through application of FAD diagrams.
PB  - Society for Structural Integrity and Life, Institute for Material Testing
T2  - Structural Integrity and Life
T1  - Influence of defects on limit loads and integrity of the pipeline at hydropower plant 'Pirot'
EP  - 86
IS  - 1
SP  - 82
VL  - 20
UR  - https://hdl.handle.net/21.15107/rcub_technorep_4567
ER  - 

@article{
author = "Međo, Bojan and Arsić, Miodrag and Mladenović, Mladen and Savić, Zoran and Grabulov, Vencislav and Radosavljević, Zoran and Rakin, Marko",
year = "2020",
abstract = "Topic of this work is the integrity assessment of the pipeline section from hydropower plant Pirot. Crack-like defect size, maximum depth, is determined based on non-destructive evaluation - the largest crack depth is taken as the initial value for load carrying capacity estimation. Also, the crack dimensions (both length and depth) are varied. Limit pressure values are determined from 3D and 2D models of pipes with axial cracks on external surface. The influence of tensile loading on the load carrying capacity of the pipes with circumferential cracks is also examined. Integrity of pipes with both types of defects (axial and circumferential) is assessed through application of FAD diagrams.",
publisher = "Society for Structural Integrity and Life, Institute for Material Testing",
journal = "Structural Integrity and Life",
title = "Influence of defects on limit loads and integrity of the pipeline at hydropower plant 'Pirot'",
pages = "86-82",
number = "1",
volume = "20",
url = "https://hdl.handle.net/21.15107/rcub_technorep_4567"
}

Međo, B., Arsić, M., Mladenović, M., Savić, Z., Grabulov, V., Radosavljević, Z.,& Rakin, M.. (2020). Influence of defects on limit loads and integrity of the pipeline at hydropower plant 'Pirot'. in Structural Integrity and Life
Society for Structural Integrity and Life, Institute for Material Testing., 20(1), 82-86.
https://hdl.handle.net/21.15107/rcub_technorep_4567

Međo B, Arsić M, Mladenović M, Savić Z, Grabulov V, Radosavljević Z, Rakin M. Influence of defects on limit loads and integrity of the pipeline at hydropower plant 'Pirot'. in Structural Integrity and Life. 2020;20(1):82-86.
https://hdl.handle.net/21.15107/rcub_technorep_4567 .

Međo, Bojan, Arsić, Miodrag, Mladenović, Mladen, Savić, Zoran, Grabulov, Vencislav, Radosavljević, Zoran, Rakin, Marko, "Influence of defects on limit loads and integrity of the pipeline at hydropower plant 'Pirot'" in Structural Integrity and Life, 20, no. 1 (2020):82-86,
https://hdl.handle.net/21.15107/rcub_technorep_4567 .

TY  - JOUR
AU  - Mijatović, N.N.
AU  - Terzić, Anja
AU  - Pezo, Lato
AU  - Miličić, L.R.
AU  - Živojinović, Dragana
PY  - 2020
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4570
AB  - A modification of analytical procedure for energy-dispersive X-ray fluorescence (EDXRF) quantification of ten chemical elements (As, Ba, Cd, Co, Cr, Cu, Mo, Ni, Pb, Zn) in the leachates obtained from cement binders was developed. Twenty-nine testing samples were used in the experiment. All samples were based on Portland cement. Fly ash of different origin, zeolite and bentonite were employed as mineral additives in the cement binders. Distilled water was used as leachate. Validation of the modified EDXRF procedure was conducted in terms of limits of detection and quantification, working range, linearity, selectivity, precision, trueness, and robustness. Traceability of the procedure was established using certified reference materials. Uncertainty of measurement was confirmed via "in-house" laboratory validation approach. The expanded uncertainties for ten analysed elements were obtained for entire working range of EDXRF method. Robustness of the modified EDXRF procedure was assessed by means of chemometric in-house approach. The results obtained by modified X-ray fluorescence method were additionally correlated to those acquired by inductively coupled plasma optical emission spectrometry to confirm that EDXRF can be used as an effective and reliable alternative method for analysis of cement leachates.
PB  - Serbian Chemical Society, Belgrade
T2  - Journal of the Serbian Chemical Society
T1  - Improvement and modification of energy-dispersive X-ray fluorescence method for determination of metal elements in cement leachates-chemometric approach
EP  - 15
SP  - 1
VL  - 85
DO  - 10.2298/JSC200501067M
ER  - 

@article{
author = "Mijatović, N.N. and Terzić, Anja and Pezo, Lato and Miličić, L.R. and Živojinović, Dragana",
year = "2020",
abstract = "A modification of analytical procedure for energy-dispersive X-ray fluorescence (EDXRF) quantification of ten chemical elements (As, Ba, Cd, Co, Cr, Cu, Mo, Ni, Pb, Zn) in the leachates obtained from cement binders was developed. Twenty-nine testing samples were used in the experiment. All samples were based on Portland cement. Fly ash of different origin, zeolite and bentonite were employed as mineral additives in the cement binders. Distilled water was used as leachate. Validation of the modified EDXRF procedure was conducted in terms of limits of detection and quantification, working range, linearity, selectivity, precision, trueness, and robustness. Traceability of the procedure was established using certified reference materials. Uncertainty of measurement was confirmed via "in-house" laboratory validation approach. The expanded uncertainties for ten analysed elements were obtained for entire working range of EDXRF method. Robustness of the modified EDXRF procedure was assessed by means of chemometric in-house approach. The results obtained by modified X-ray fluorescence method were additionally correlated to those acquired by inductively coupled plasma optical emission spectrometry to confirm that EDXRF can be used as an effective and reliable alternative method for analysis of cement leachates.",
publisher = "Serbian Chemical Society, Belgrade",
journal = "Journal of the Serbian Chemical Society",
title = "Improvement and modification of energy-dispersive X-ray fluorescence method for determination of metal elements in cement leachates-chemometric approach",
pages = "15-1",
volume = "85",
doi = "10.2298/JSC200501067M"
}

Mijatović, N.N., Terzić, A., Pezo, L., Miličić, L.R.,& Živojinović, D.. (2020). Improvement and modification of energy-dispersive X-ray fluorescence method for determination of metal elements in cement leachates-chemometric approach. in Journal of the Serbian Chemical Society
Serbian Chemical Society, Belgrade., 85, 1-15.
https://doi.org/10.2298/JSC200501067M

Mijatović N, Terzić A, Pezo L, Miličić L, Živojinović D. Improvement and modification of energy-dispersive X-ray fluorescence method for determination of metal elements in cement leachates-chemometric approach. in Journal of the Serbian Chemical Society. 2020;85:1-15.
doi:10.2298/JSC200501067M .

Mijatović, N.N., Terzić, Anja, Pezo, Lato, Miličić, L.R., Živojinović, Dragana, "Improvement and modification of energy-dispersive X-ray fluorescence method for determination of metal elements in cement leachates-chemometric approach" in Journal of the Serbian Chemical Society, 85 (2020):1-15,
https://doi.org/10.2298/JSC200501067M . .

TY  - JOUR
AU  - Mijatovic, Nevenka N.
AU  - Terzic, Anja M.
AU  - Pezo, Lato L.
AU  - Milicic, Ljiljana R.
AU  - Živojinović, Dragana
PY  - 2020
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4747
AB  - A modification of an analytical procedure for the energy-dispersive X-ray fluorescence (EDXRF) quantification of ten chemical elements (As, Ba, Cd, Co, Cr, Cu, Mo, Ni, Pb and Zn) in the leachates obtained from cement binders was developed. Twenty-nine testing samples were used in the experiment. All samples were based on Portland cement. Fly ash of different origin, zeolite and bentonite were employed as mineral additives in the cement binders. Distilled water was used as the leachate. Validation of the modified EDXRF procedure was conducted in terms of limits of detection and quantification, working range, linearity, selectivity, precision, trueness, and robustness. Traceability of the procedure was established using certified reference materials. Uncertainty of measurement was confirmed via an "in-house" laboratory validation approach. The expanded uncertainties for the ten analysed elements were obtained for the entire working range of the EDXRF method. Robustness of the modified EDXRF procedure was assessed by means of a chemometric in-house approach. The results obtained by the modified X-ray fluorescence method were additionally correlated to those acquired by inductively coupled plasma optical emission spectrometry to confirm that EDXRF could be used as an effective and reliable alternative method for analysis of cement leachates.
T2  - Journal of the Serbian Chemical Society
T1  - Improvement and modification of the energy-dispersive X-ray fluorescence method for the determination of metal elements in cement leachates - A chemometric approach
EP  - 1619
IS  - 12
SP  - 1605
VL  - 85
DO  - 10.2298/JSC200501067M
ER  - 

@article{
author = "Mijatovic, Nevenka N. and Terzic, Anja M. and Pezo, Lato L. and Milicic, Ljiljana R. and Živojinović, Dragana",
year = "2020",
abstract = "A modification of an analytical procedure for the energy-dispersive X-ray fluorescence (EDXRF) quantification of ten chemical elements (As, Ba, Cd, Co, Cr, Cu, Mo, Ni, Pb and Zn) in the leachates obtained from cement binders was developed. Twenty-nine testing samples were used in the experiment. All samples were based on Portland cement. Fly ash of different origin, zeolite and bentonite were employed as mineral additives in the cement binders. Distilled water was used as the leachate. Validation of the modified EDXRF procedure was conducted in terms of limits of detection and quantification, working range, linearity, selectivity, precision, trueness, and robustness. Traceability of the procedure was established using certified reference materials. Uncertainty of measurement was confirmed via an "in-house" laboratory validation approach. The expanded uncertainties for the ten analysed elements were obtained for the entire working range of the EDXRF method. Robustness of the modified EDXRF procedure was assessed by means of a chemometric in-house approach. The results obtained by the modified X-ray fluorescence method were additionally correlated to those acquired by inductively coupled plasma optical emission spectrometry to confirm that EDXRF could be used as an effective and reliable alternative method for analysis of cement leachates.",
journal = "Journal of the Serbian Chemical Society",
title = "Improvement and modification of the energy-dispersive X-ray fluorescence method for the determination of metal elements in cement leachates - A chemometric approach",
pages = "1619-1605",
number = "12",
volume = "85",
doi = "10.2298/JSC200501067M"
}

Mijatovic, N. N., Terzic, A. M., Pezo, L. L., Milicic, L. R.,& Živojinović, D.. (2020). Improvement and modification of the energy-dispersive X-ray fluorescence method for the determination of metal elements in cement leachates - A chemometric approach. in Journal of the Serbian Chemical Society, 85(12), 1605-1619.
https://doi.org/10.2298/JSC200501067M

Mijatovic NN, Terzic AM, Pezo LL, Milicic LR, Živojinović D. Improvement and modification of the energy-dispersive X-ray fluorescence method for the determination of metal elements in cement leachates - A chemometric approach. in Journal of the Serbian Chemical Society. 2020;85(12):1605-1619.
doi:10.2298/JSC200501067M .

Mijatovic, Nevenka N., Terzic, Anja M., Pezo, Lato L., Milicic, Ljiljana R., Živojinović, Dragana, "Improvement and modification of the energy-dispersive X-ray fluorescence method for the determination of metal elements in cement leachates - A chemometric approach" in Journal of the Serbian Chemical Society, 85, no. 12 (2020):1605-1619,
https://doi.org/10.2298/JSC200501067M . .