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42055

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Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine

Zabukovec-Logar, Nataša; Mali, Gregor; Rajić, Nevenka; Jevtić, Sanja; Rangus, Mojca; Golobić, Amalija; Kaučič, Venčeslav

(Academic Press Inc Elsevier Science, San Diego, 2010)

TY  - JOUR
AU  - Zabukovec-Logar, Nataša
AU  - Mali, Gregor
AU  - Rajić, Nevenka
AU  - Jevtić, Sanja
AU  - Rangus, Mojca
AU  - Golobić, Amalija
AU  - Kaučič, Venčeslav
PY  - 2010
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1699
AB  - A single-crystal X-ray diffraction analysis of an open-framework aluminophosphate ULM-3 Al prepared by 3-methylaminopropylamine (MAPA) as structure-directing agent revealed an orthorhombic Pcab symmetry (a=9.9949(4)angstrom, b=15.8229(7)angstrom, c=18.1963(5)angstrom, R=0.0648, Z=8, unit cell formula (Al24P24O96F16 center dot C32H112N16]). which differs from the Pbc2(1) symmetry of the structural analogue prepared in the presence of 1,4-diaminobutane. The Al-27, P-31, F-19, C-13 and H-1 NMR investigations, which were performed to study in detail MAPA arrangement inside the framework as well as the interactions of MAPA with the aluminophosphate host, confirmed the crystal symmetry and the proposed hydrogen bonding scheme between the template and the framework.
PB  - Academic Press Inc Elsevier Science, San Diego
T2  - Journal of Solid State Chemistry
T1  - Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine
EP  - 1062
IS  - 5
SP  - 1055
VL  - 183
DO  - 10.1016/j.jssc.2010.02.020
ER  - 
@article{
author = "Zabukovec-Logar, Nataša and Mali, Gregor and Rajić, Nevenka and Jevtić, Sanja and Rangus, Mojca and Golobić, Amalija and Kaučič, Venčeslav",
year = "2010",
abstract = "A single-crystal X-ray diffraction analysis of an open-framework aluminophosphate ULM-3 Al prepared by 3-methylaminopropylamine (MAPA) as structure-directing agent revealed an orthorhombic Pcab symmetry (a=9.9949(4)angstrom, b=15.8229(7)angstrom, c=18.1963(5)angstrom, R=0.0648, Z=8, unit cell formula (Al24P24O96F16 center dot C32H112N16]). which differs from the Pbc2(1) symmetry of the structural analogue prepared in the presence of 1,4-diaminobutane. The Al-27, P-31, F-19, C-13 and H-1 NMR investigations, which were performed to study in detail MAPA arrangement inside the framework as well as the interactions of MAPA with the aluminophosphate host, confirmed the crystal symmetry and the proposed hydrogen bonding scheme between the template and the framework.",
publisher = "Academic Press Inc Elsevier Science, San Diego",
journal = "Journal of Solid State Chemistry",
title = "Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine",
pages = "1062-1055",
number = "5",
volume = "183",
doi = "10.1016/j.jssc.2010.02.020"
}
Zabukovec-Logar, N., Mali, G., Rajić, N., Jevtić, S., Rangus, M., Golobić, A.,& Kaučič, V.. (2010). Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine. in Journal of Solid State Chemistry
Academic Press Inc Elsevier Science, San Diego., 183(5), 1055-1062.
https://doi.org/10.1016/j.jssc.2010.02.020
Zabukovec-Logar N, Mali G, Rajić N, Jevtić S, Rangus M, Golobić A, Kaučič V. Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine. in Journal of Solid State Chemistry. 2010;183(5):1055-1062.
doi:10.1016/j.jssc.2010.02.020 .
Zabukovec-Logar, Nataša, Mali, Gregor, Rajić, Nevenka, Jevtić, Sanja, Rangus, Mojca, Golobić, Amalija, Kaučič, Venčeslav, "Structure investigation of fluorinated aluminophosphate ULM-3 Al templated by 3-methylaminopropylamine" in Journal of Solid State Chemistry, 183, no. 5 (2010):1055-1062,
https://doi.org/10.1016/j.jssc.2010.02.020 . .
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