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Forced periodic operations of a chemical reactor for methanol synthesis - The search for the best scenario based on Nonlinear Frequency Response Method. Part I Single input modulations
(Chemical Engineering Science, 2022)
In this two-part paper a comprehensive study of the potential to improve performance criteria of a methanol synthesis reactor through forced periodical operations is presented. The study uses the Nonlinear Frequency Response ...
Transesterification of used cooking sunflower oil catalyzed by hazelnut shell ash
(Renewable Energy, 2022)
Hazelnut shell ash was investigated as a new base catalyst for the transesterification of used cooking sunflower oil to biodiesel. To understand its catalytic properties, the prepared ash was characterized by EDX, XRD, ...
Extraction of lyophilized olive mill wastewater using supercritical CO2 processes
(Alexandria Engineering Journal, 2022)
The olive growing in Tunisia has an economic dominance and agricultural importance. However, the huge extraction of olive oil generates a large quantity of olive mill wastewater (OMW), which is discharged to the surroundings. ...
Dispersive Solid–Liquid Microextraction Based on the Poly(HDDA)/Graphene Sorbent Followed by ICP-MS for the Determination of Rare Earth Elements in Coal Fly Ash Leachate
(MDPI, 2022)
A dispersive solid-phase microextraction (DSPME) sorbent consisting of poly(1,6-hexanedi-ol diacrylate)-based polymer microspheres, with embedded graphene microparticles (poly(HDDA)/g-raphene), was synthesized by microfluidic ...
Green manufacturing of high-value extracts from milk thistle seeds: Parameters that affect the supercritical CO2extraction process
(Elsevier Ltd, 2022)
The aim of this study was to provide insights into parameters that affect the oil extraction from an industrially valuable raw material (milk thistle) using green solvent supercritical CO2. The effect of plant origin, ...
Unravelling conformational and crystal packing preferences of cyclohexane-5-spirohydantoin derivatives incorporating a halogenated benzoyl group
(Royal Society of Chemistry, 2022)
Two spirohydantoin derivatives, 3-(4-chlorobenzoyl)-1,3-diazaspiro[4.5]decane-2,4-dione (1) and 3-(4-bromobenzoyl)-1,3-diazaspiro[4.5]decane-2,4-dione (2), were synthesized and analyzed by single crystal X-ray diffraction, ...
Polyphenol extraction in microwave reactor using by-product of Thymus serpyllum L. and biological potential of the extract
(Elsevier GmbH, 2022)
In the present study, polyphenol extraction from Thymus serpyllum by-product (herbal dust) in microwave reactor was optimized through varying extraction time, ethanol concentration and solid-to-solvent ratiovia determination ...
Improvement of theoretical UV–Vis spectra calculations by empirical solvatochromic parameters: Case study of 5-arylazo-3-cyano-1-ethyl-6-hydroxy-4-methyl-2-pyridones
(Elsevier B.V., 2022)
In order to improve the performance of theoretical UV–Vis spectra predictions, a theoretical and experimental study of solvatochromic properties of ten azo pyridone dyes has been performed. For quantitative estimation of ...
Development of a New AuCuZnGe Alloy and Determination of Its Corrosion Properties
(MDPI, 2022)
In this paper, we present the idea and development of a new gold-copper-zinc-germanium (AuCuZnGe) alloy, which is related to the method of production and research of its key properties, so that the new Au alloy could be ...
Bioactive Interpenetrating Hydrogel Networks Based on 2-Hydroxyethyl Methacrylate and Gelatin Intertwined with Alginate and Dopped with Apatite as Scaffolding Biomaterials
(MDPI, 2022)
Our goal was to create bioimitated scaffolding materials for biomedical purposes. The guiding idea was that we used an interpenetrating structural hierarchy of natural extracellular matrix as a “pattern” to design hydrogel ...