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Improvement to the Flynn-Wall method of determining apparent activation energies of the thermal degradation of polymers
(Amer Chemical Soc, Washington, 2003)
An improvement to the Flynn-Wall method of determining apparent activation energies of the thermal degradation of polymers is presented. The method involves the deconvolution of differential thermogravimetric (TG) curves ...
Correlation between apparent activation energy for hot working and temperature of no recrystallization in microalloyed steels
(Trans Tech Publications Ltd, Durnten-Zurich, 2003)
Two-stage linear ln[sinh(as)] vs 1/T plots, based on the stress data derived from either continuous or multipass flow curves generated by testing low carbon Nb/Ti microalloyed steel (Nb steel) and medium carbon V-microalloyed ...
Relationship between Mechanical Characteristics and Thermal Shock Behaviour of Alumina Based Refractories
(InterCeram: International Ceramic Review, 2003)
The thermal stability of the refractory material with the Al 2 O 3 content of 42 mass-% was investigated. Water quench tests (JUS.B.D8.319.) were carried out. The dynamic Young modulus of elasticity was calculated using ...
Crystallization behavior of alkoxy-derived cordierite gels
(Springer, New York, 2003)
Alkoxy-derived cordierite gels were synthesized from tetraethylorthosilicate (TEOS), aluminum isopropoxide (Al(OPri)(3)), and magnesium ethoxide (Mg(OEt)(2)). TEOS was partially hydrolyzed at molar ratios H2O/TEOS=1.2, in ...
Manganese-containing silica-based microporous molecular sieve MnS-1: Synthesis and characterization
(Amer Chemical Soc, Washington, 2003)
Manganese-containing silicalite-1 (MnS-1) was synthesized hydrothermally in the presence of the structure-directing agent (template) tetraethylammonium hydroxide (TEAOH) for the first time. The highly crystalline MnS-1 ...
New inorganic-organic hybrid: Synthesis and structural characterization of an alumino(oxalato)phosphate
(Amer Chemical Soc, Washington, 2003)
A new 3-D alumino(oxalato)phosphate, [H3NCH(CH3)CH2NH3](2)[Al4P6O20(OH)(4)(C2O4)(H2O)], consists of aluminophosphate layers which are pillared by oxalate anions. It contains a hybrid 12-membered channel where guest species, ...
Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent
(Pergamon-Elsevier Science Ltd, Oxford, 2003)
Colorless plate-like crystals (AIPO-1,2DAP) crystallize from a clear 'AlPO4-1,2-diaminopropane' reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH4+)(1,2-H(2)DAP ...
PZT ceramics obtained from mechanochemically synthesized powders
(Kluwer Academic Publ, Dordrecht, 2003)
PZT ceramics were obtained from the mechanochemically synthesized powders. Milling and sintering conditions were optimized based on results of density measurements, as well as on microstructural and electrical characterization. ...
The influence of heat treatment and finishing on the mechanical and dielectric properties of glass fabric-epoxy resin laminar composites
(Springer Netherlands, 2003)
The aim of this investigation was to define the optimum conditions of obtaining glass fabric - epoxy resin laminar composites with mechanical and dielectric properties that satisfy the quality needed for production of ...
Somebody get me a drill!
(Elsevier, 2003)