Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization
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1998
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Metapodaci
Prikaz svih podataka o dokumentuApstrakt
Thin Fe-P alloy films (0.5 to 25.0 mu m thick) were electrodeposited from sulfate solutions. The influences of various deposition conditions (current density, time, pH and temperature) on the composition and structure of the deposited films were examined. These Fe-P films were first characterized by the ALSV. The voltammograms obtained show several current peaks, indicating the presence of several different phase structures in the deposit. Chemical composition of the phase structures in the film was determined by EDX analysis and the amorphous nature of the alloy was verified by XRD and DTA techniques. Chemical and phase structure compositions of the alloys (containing 15-50 at.% P in the form of phosphides FeP, Fe2P and/or Fe3P) were found to depend on deposition conditions. Appearance and morphology of the film alloys were also found to depend on deposition conditions, particularly current density, as illustrated by the SEM technique.
Ključne reči:
iron-phosphorous alloy / amorphous alloys / electrodeposition / thin filmsIzvor:
Journal of Electroanalytical Chemistry, 1998, 448, 2, 245-252Izdavač:
- Elsevier Science Sa, Lausanne
DOI: 10.1016/S0022-0728(97)00417-8
ISSN: 1572-6657
WoS: 000075475600012
Scopus: 2-s2.0-0032064068
Institucija/grupa
Tehnološko-metalurški fakultetTY - JOUR AU - Zečević, S.K. AU - Zotović, Jelena B. AU - Gojković, Snežana Lj. AU - Radmilović, V. PY - 1998 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/216 AB - Thin Fe-P alloy films (0.5 to 25.0 mu m thick) were electrodeposited from sulfate solutions. The influences of various deposition conditions (current density, time, pH and temperature) on the composition and structure of the deposited films were examined. These Fe-P films were first characterized by the ALSV. The voltammograms obtained show several current peaks, indicating the presence of several different phase structures in the deposit. Chemical composition of the phase structures in the film was determined by EDX analysis and the amorphous nature of the alloy was verified by XRD and DTA techniques. Chemical and phase structure compositions of the alloys (containing 15-50 at.% P in the form of phosphides FeP, Fe2P and/or Fe3P) were found to depend on deposition conditions. Appearance and morphology of the film alloys were also found to depend on deposition conditions, particularly current density, as illustrated by the SEM technique. PB - Elsevier Science Sa, Lausanne T2 - Journal of Electroanalytical Chemistry T1 - Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization EP - 252 IS - 2 SP - 245 VL - 448 DO - 10.1016/S0022-0728(97)00417-8 ER -
@article{ author = "Zečević, S.K. and Zotović, Jelena B. and Gojković, Snežana Lj. and Radmilović, V.", year = "1998", abstract = "Thin Fe-P alloy films (0.5 to 25.0 mu m thick) were electrodeposited from sulfate solutions. The influences of various deposition conditions (current density, time, pH and temperature) on the composition and structure of the deposited films were examined. These Fe-P films were first characterized by the ALSV. The voltammograms obtained show several current peaks, indicating the presence of several different phase structures in the deposit. Chemical composition of the phase structures in the film was determined by EDX analysis and the amorphous nature of the alloy was verified by XRD and DTA techniques. Chemical and phase structure compositions of the alloys (containing 15-50 at.% P in the form of phosphides FeP, Fe2P and/or Fe3P) were found to depend on deposition conditions. Appearance and morphology of the film alloys were also found to depend on deposition conditions, particularly current density, as illustrated by the SEM technique.", publisher = "Elsevier Science Sa, Lausanne", journal = "Journal of Electroanalytical Chemistry", title = "Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization", pages = "252-245", number = "2", volume = "448", doi = "10.1016/S0022-0728(97)00417-8" }
Zečević, S.K., Zotović, J. B., Gojković, S. Lj.,& Radmilović, V.. (1998). Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization. in Journal of Electroanalytical Chemistry Elsevier Science Sa, Lausanne., 448(2), 245-252. https://doi.org/10.1016/S0022-0728(97)00417-8
Zečević S, Zotović JB, Gojković SL, Radmilović V. Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization. in Journal of Electroanalytical Chemistry. 1998;448(2):245-252. doi:10.1016/S0022-0728(97)00417-8 .
Zečević, S.K., Zotović, Jelena B., Gojković, Snežana Lj., Radmilović, V., "Electrochemically deposited thin films of amorphous Fe-P alloy Part I. Chemical composition and phase structure characterization" in Journal of Electroanalytical Chemistry, 448, no. 2 (1998):245-252, https://doi.org/10.1016/S0022-0728(97)00417-8 . .