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Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol

Authorized Users Only
2016
Authors
Ćosović, Aleksandar
Žák, Tomáš
Glišić, Sandra
Sokić, Miroslav
Lazarević, Slavica
Ćosović, Vladan
Orlović, Aleksandar
Article (Published version)
Metadata
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Abstract
Nano-crystalline nickel ferrite has a broad range of applications due to its favourable magnetic properties. Those characteristics can be significantly influenced by the synthesis pathway including methods conducted in the presence of supercritical alcohols. Nano-crystalline NiFe2O4 powders were obtained in the reaction under subcritical and supercritical conditions of ethanol. Both high pressure synthesis routes resulted in powders with smaller primary particles and higher mesoporosity than co-precipitation method. Upon the annealing treatment the average crystallite size increased while material structure remained uniform, resulting in significantly enhanced magnetic properties, such as coercivity and remanence. It was found that synthesis under supercritical conditions provides higher conversion but also material with larger average crystallite size upon annealing. The time and temperature of annealing stage significantly influenced the morphology and magnetic properties of the obta...ined powders.

Keywords:
Supercritical / Subcritical / Nano-crystalline powders / Nickel ferrite / Metal oxide / Magnetic properties
Source:
Journal of Supercritical Fluids, 2016, 113, 96-105
Publisher:
  • Elsevier Science Bv, Amsterdam
Funding / projects:
  • Developing technological processes for nonstandard copper concentrates processing with the aim to decrease pollutants emission (RS-34023)
  • European Regional Development Fund through CEITEC-Central European Institute of Technology [CZ.1.05/1.1.00/02.0068]

DOI: 10.1016/j.supflu.2016.03.014

ISSN: 0896-8446

WoS: 000375500000014

Scopus: 2-s2.0-84961926591
[ Google Scholar ]
10
9
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3262
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Ćosović, Aleksandar
AU  - Žák, Tomáš
AU  - Glišić, Sandra
AU  - Sokić, Miroslav
AU  - Lazarević, Slavica
AU  - Ćosović, Vladan
AU  - Orlović, Aleksandar
PY  - 2016
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3262
AB  - Nano-crystalline nickel ferrite has a broad range of applications due to its favourable magnetic properties. Those characteristics can be significantly influenced by the synthesis pathway including methods conducted in the presence of supercritical alcohols. Nano-crystalline NiFe2O4 powders were obtained in the reaction under subcritical and supercritical conditions of ethanol. Both high pressure synthesis routes resulted in powders with smaller primary particles and higher mesoporosity than co-precipitation method. Upon the annealing treatment the average crystallite size increased while material structure remained uniform, resulting in significantly enhanced magnetic properties, such as coercivity and remanence. It was found that synthesis under supercritical conditions provides higher conversion but also material with larger average crystallite size upon annealing. The time and temperature of annealing stage significantly influenced the morphology and magnetic properties of the obtained powders.
PB  - Elsevier Science Bv, Amsterdam
T2  - Journal of Supercritical Fluids
T1  - Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol
EP  - 105
SP  - 96
VL  - 113
DO  - 10.1016/j.supflu.2016.03.014
UR  - conv_4999
ER  - 
@article{
author = "Ćosović, Aleksandar and Žák, Tomáš and Glišić, Sandra and Sokić, Miroslav and Lazarević, Slavica and Ćosović, Vladan and Orlović, Aleksandar",
year = "2016",
abstract = "Nano-crystalline nickel ferrite has a broad range of applications due to its favourable magnetic properties. Those characteristics can be significantly influenced by the synthesis pathway including methods conducted in the presence of supercritical alcohols. Nano-crystalline NiFe2O4 powders were obtained in the reaction under subcritical and supercritical conditions of ethanol. Both high pressure synthesis routes resulted in powders with smaller primary particles and higher mesoporosity than co-precipitation method. Upon the annealing treatment the average crystallite size increased while material structure remained uniform, resulting in significantly enhanced magnetic properties, such as coercivity and remanence. It was found that synthesis under supercritical conditions provides higher conversion but also material with larger average crystallite size upon annealing. The time and temperature of annealing stage significantly influenced the morphology and magnetic properties of the obtained powders.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Journal of Supercritical Fluids",
title = "Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol",
pages = "105-96",
volume = "113",
doi = "10.1016/j.supflu.2016.03.014",
url = "conv_4999"
}
Ćosović, A., Žák, T., Glišić, S., Sokić, M., Lazarević, S., Ćosović, V.,& Orlović, A.. (2016). Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol. in Journal of Supercritical Fluids
Elsevier Science Bv, Amsterdam., 113, 96-105.
https://doi.org/10.1016/j.supflu.2016.03.014
conv_4999
Ćosović A, Žák T, Glišić S, Sokić M, Lazarević S, Ćosović V, Orlović A. Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol. in Journal of Supercritical Fluids. 2016;113:96-105.
doi:10.1016/j.supflu.2016.03.014
conv_4999 .
Ćosović, Aleksandar, Žák, Tomáš, Glišić, Sandra, Sokić, Miroslav, Lazarević, Slavica, Ćosović, Vladan, Orlović, Aleksandar, "Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol" in Journal of Supercritical Fluids, 113 (2016):96-105,
https://doi.org/10.1016/j.supflu.2016.03.014 .,
conv_4999 .

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