Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition
Аутори
Mijatović, NevenkaTerzić, Anja
Pezo, Lato
Milicić, Ljiljana
Milosavljević, Aleksandra
Živojinović, Dragana
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to... prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method.
Кључне речи:
Analytical procedures / Building materials / Waste materials / Leaching / Analytical modelingИзвор:
Science of Sintering, 2019, 51, 4, 429-444Издавач:
- Međunarodni Institut za nauku o sinterovanju, Beograd
Финансирање / пројекти:
- Развој и примена мултифункционалних материјала на бази домаћих сировина модернизацијом традиционалних технологија (RS-45008)
- Усмерена синтеза, структура и својства мултифункционалних материјала (RS-172057)
DOI: 10.2298/SOS1904429M
ISSN: 0350-820X
WoS: 000509869400008
Scopus: 2-s2.0-85078854100
Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Mijatović, Nevenka AU - Terzić, Anja AU - Pezo, Lato AU - Milicić, Ljiljana AU - Milosavljević, Aleksandra AU - Živojinović, Dragana PY - 2019 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4137 AB - New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method. PB - Međunarodni Institut za nauku o sinterovanju, Beograd T2 - Science of Sintering T1 - Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition EP - 444 IS - 4 SP - 429 VL - 51 DO - 10.2298/SOS1904429M ER -
@article{ author = "Mijatović, Nevenka and Terzić, Anja and Pezo, Lato and Milicić, Ljiljana and Milosavljević, Aleksandra and Živojinović, Dragana", year = "2019", abstract = "New global tendencies for waste materials reusing in building materials are imposing the request for improved performances of chemical analysis methods and the improvements of matrices used. A new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) is developed and validated for the chemical analysis (35 elements: Al, Be, Cd, So, Cr, Cu, Fe, Mn, Mo, Ni, V, Mo, Zn, Pb , Bi, Si, Zr, W, As, Se, Sb, Sn, Ti, Ba, B, Ag, Mg, Ca, K, Na, S, P, Ga, In, Li) in leachate of fly ash. Validation performances and the uncertainty of measurement were resolved. Uncertainty of measurements were resolved by three routes: validation procedure, participation in proficiency testing (PT) schemes and standard method. The obtained method is a new simple and effective analyzing route for determination of undesired trace elements and their quantity comprised in leachates of fly ash, and leachates of building materials with addition of fly ash (cement binders and mortars). In order to prove its accuracy and precision, the developed method was employed on laboratory samples of cement binders and mortars. Results were compared with limit values provided in the standard. Multivariate analyses, i.e. cluster analysis and principal component analysis, were applied to establish interrelations between analyzed samples, and to certify the developed ICP-OES method.", publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd", journal = "Science of Sintering", title = "Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition", pages = "444-429", number = "4", volume = "51", doi = "10.2298/SOS1904429M" }
Mijatović, N., Terzić, A., Pezo, L., Milicić, L., Milosavljević, A.,& Živojinović, D.. (2019). Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition. in Science of Sintering Međunarodni Institut za nauku o sinterovanju, Beograd., 51(4), 429-444. https://doi.org/10.2298/SOS1904429M
Mijatović N, Terzić A, Pezo L, Milicić L, Milosavljević A, Živojinović D. Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition. in Science of Sintering. 2019;51(4):429-444. doi:10.2298/SOS1904429M .
Mijatović, Nevenka, Terzić, Anja, Pezo, Lato, Milicić, Ljiljana, Milosavljević, Aleksandra, Živojinović, Dragana, "Novel Approach for Determination of Potentially Toxic Elements via ICP-OES in Aqueous Solutions of Building Materials with Industrial Byproduct Addition" in Science of Sintering, 51, no. 4 (2019):429-444, https://doi.org/10.2298/SOS1904429M . .