Simultaneous Crystallization Testing in a Laboratory Furnace
Апстракт
The cooler allows easy regulation of simultaneous crystallization tests of different crystallization parameters and substances, with the purpose of obtaining crystals from a family of newly synthesized compounds with a layered crystal structure. The procedure involves first increasing the voltage until the substances are completely melted. Then, while a constant furnace voltage is maintained, a small amount of airflow is introduced into the cooler. As a result, crystallization starts on the surface of the melts for the lower row and at the bottom of the melts for the upper row. The crystallization rate interval in each Tamman test tube is regulated by the cross-section of the airflow. Different temperature gradients in the crucibles can be tested simultaneously using an inclined cooler. Tamman test tubes and plugs of various shapes and dimensions can be mounted and thus tested at the same time. Several coolers or a planar air cooler with several columns of plugs can be installed in a c...hamber furnace (crystallization board).
Извор:
American Laboratory, 2011, 43, 7, 18-19Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Čabrić, Branislav AU - Danilović, Nebojša AU - Janićijević, Aco PY - 2011 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1750 AB - The cooler allows easy regulation of simultaneous crystallization tests of different crystallization parameters and substances, with the purpose of obtaining crystals from a family of newly synthesized compounds with a layered crystal structure. The procedure involves first increasing the voltage until the substances are completely melted. Then, while a constant furnace voltage is maintained, a small amount of airflow is introduced into the cooler. As a result, crystallization starts on the surface of the melts for the lower row and at the bottom of the melts for the upper row. The crystallization rate interval in each Tamman test tube is regulated by the cross-section of the airflow. Different temperature gradients in the crucibles can be tested simultaneously using an inclined cooler. Tamman test tubes and plugs of various shapes and dimensions can be mounted and thus tested at the same time. Several coolers or a planar air cooler with several columns of plugs can be installed in a chamber furnace (crystallization board). T2 - American Laboratory T1 - Simultaneous Crystallization Testing in a Laboratory Furnace EP - 19 IS - 7 SP - 18 VL - 43 UR - https://hdl.handle.net/21.15107/rcub_technorep_1750 ER -
@article{ author = "Čabrić, Branislav and Danilović, Nebojša and Janićijević, Aco", year = "2011", abstract = "The cooler allows easy regulation of simultaneous crystallization tests of different crystallization parameters and substances, with the purpose of obtaining crystals from a family of newly synthesized compounds with a layered crystal structure. The procedure involves first increasing the voltage until the substances are completely melted. Then, while a constant furnace voltage is maintained, a small amount of airflow is introduced into the cooler. As a result, crystallization starts on the surface of the melts for the lower row and at the bottom of the melts for the upper row. The crystallization rate interval in each Tamman test tube is regulated by the cross-section of the airflow. Different temperature gradients in the crucibles can be tested simultaneously using an inclined cooler. Tamman test tubes and plugs of various shapes and dimensions can be mounted and thus tested at the same time. Several coolers or a planar air cooler with several columns of plugs can be installed in a chamber furnace (crystallization board).", journal = "American Laboratory", title = "Simultaneous Crystallization Testing in a Laboratory Furnace", pages = "19-18", number = "7", volume = "43", url = "https://hdl.handle.net/21.15107/rcub_technorep_1750" }
Čabrić, B., Danilović, N.,& Janićijević, A.. (2011). Simultaneous Crystallization Testing in a Laboratory Furnace. in American Laboratory, 43(7), 18-19. https://hdl.handle.net/21.15107/rcub_technorep_1750
Čabrić B, Danilović N, Janićijević A. Simultaneous Crystallization Testing in a Laboratory Furnace. in American Laboratory. 2011;43(7):18-19. https://hdl.handle.net/21.15107/rcub_technorep_1750 .
Čabrić, Branislav, Danilović, Nebojša, Janićijević, Aco, "Simultaneous Crystallization Testing in a Laboratory Furnace" in American Laboratory, 43, no. 7 (2011):18-19, https://hdl.handle.net/21.15107/rcub_technorep_1750 .