The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics
Само за регистроване кориснике
2014
Аутори
Veljović, ĐorđeRadovanović, Željko
Dindune, Antonija
Palcevskis, Eriks
Krumina, Aija
Petrović, Rada
Janaćković, Đorđe
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The aims of this study were to investigate the effects of Sr- and Mn-doped ions on the sintering behaviors, microstructure and mechanical properties of the bioceramics processed by single- and two-step microwave sintering (MWSSS and MWTSS). Nano-sized calcium hydroxyapatite powders doped with Sr and Mn ions, obtained by modified precipitation synthesis, were isostatically pressed at 400 MPa and processed by MWSSS and MWTSS at different temperatures. In all cases during the sintering, the doped HAP powders turned into biphasic mixtures of HAP and TCP, but the amount of TCP was certainly lower in the case of MWTSS. It was shown that the doped ions significantly affected: density, microstructure, grain size, porosity, hardness, and fracture toughness of the processed bioceramics. Two-step microwave sintering was successfully applied for the processing of HAP/TCP bioceramics doped with strontium and manganese ions. Both two-step microwave sintered doped bioceramics had similar and high har...dness values, but the strontium-substituted bioceramic material certainly had higher fracture toughness (1.54 MPam(1/2)), with an average grain size of 195 nm. Based on the results presented in this paper, it was concluded that the two-step microwave sintered strontium-doped bioceramics could be suitable materials in the bone regenerative field.
Извор:
Journal of Materials Science, 2014, 49, 19, 6793-6802Издавач:
- Springer, New York
Финансирање / пројекти:
- Синтеза, развој технологија добијања и примена наноструктурних мултифункционалних материјала дефинисаних својстава (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45019)
- Reinforcing of Nanotechnology and Functional Materials Centre (EU-FP7-245916)
- Reinforcing of Nanotechnology and Functional Materials Centre (EU-FP7-245916)
DOI: 10.1007/s10853-014-8380-3
ISSN: 0022-2461
WoS: 000339337600035
Scopus: 2-s2.0-84904724385
Колекције
Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Veljović, Đorđe AU - Radovanović, Željko AU - Dindune, Antonija AU - Palcevskis, Eriks AU - Krumina, Aija AU - Petrović, Rada AU - Janaćković, Đorđe PY - 2014 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/2682 AB - The aims of this study were to investigate the effects of Sr- and Mn-doped ions on the sintering behaviors, microstructure and mechanical properties of the bioceramics processed by single- and two-step microwave sintering (MWSSS and MWTSS). Nano-sized calcium hydroxyapatite powders doped with Sr and Mn ions, obtained by modified precipitation synthesis, were isostatically pressed at 400 MPa and processed by MWSSS and MWTSS at different temperatures. In all cases during the sintering, the doped HAP powders turned into biphasic mixtures of HAP and TCP, but the amount of TCP was certainly lower in the case of MWTSS. It was shown that the doped ions significantly affected: density, microstructure, grain size, porosity, hardness, and fracture toughness of the processed bioceramics. Two-step microwave sintering was successfully applied for the processing of HAP/TCP bioceramics doped with strontium and manganese ions. Both two-step microwave sintered doped bioceramics had similar and high hardness values, but the strontium-substituted bioceramic material certainly had higher fracture toughness (1.54 MPam(1/2)), with an average grain size of 195 nm. Based on the results presented in this paper, it was concluded that the two-step microwave sintered strontium-doped bioceramics could be suitable materials in the bone regenerative field. PB - Springer, New York T2 - Journal of Materials Science T1 - The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics EP - 6802 IS - 19 SP - 6793 VL - 49 DO - 10.1007/s10853-014-8380-3 ER -
@article{ author = "Veljović, Đorđe and Radovanović, Željko and Dindune, Antonija and Palcevskis, Eriks and Krumina, Aija and Petrović, Rada and Janaćković, Đorđe", year = "2014", abstract = "The aims of this study were to investigate the effects of Sr- and Mn-doped ions on the sintering behaviors, microstructure and mechanical properties of the bioceramics processed by single- and two-step microwave sintering (MWSSS and MWTSS). Nano-sized calcium hydroxyapatite powders doped with Sr and Mn ions, obtained by modified precipitation synthesis, were isostatically pressed at 400 MPa and processed by MWSSS and MWTSS at different temperatures. In all cases during the sintering, the doped HAP powders turned into biphasic mixtures of HAP and TCP, but the amount of TCP was certainly lower in the case of MWTSS. It was shown that the doped ions significantly affected: density, microstructure, grain size, porosity, hardness, and fracture toughness of the processed bioceramics. Two-step microwave sintering was successfully applied for the processing of HAP/TCP bioceramics doped with strontium and manganese ions. Both two-step microwave sintered doped bioceramics had similar and high hardness values, but the strontium-substituted bioceramic material certainly had higher fracture toughness (1.54 MPam(1/2)), with an average grain size of 195 nm. Based on the results presented in this paper, it was concluded that the two-step microwave sintered strontium-doped bioceramics could be suitable materials in the bone regenerative field.", publisher = "Springer, New York", journal = "Journal of Materials Science", title = "The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics", pages = "6802-6793", number = "19", volume = "49", doi = "10.1007/s10853-014-8380-3" }
Veljović, Đ., Radovanović, Ž., Dindune, A., Palcevskis, E., Krumina, A., Petrović, R.,& Janaćković, Đ.. (2014). The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics. in Journal of Materials Science Springer, New York., 49(19), 6793-6802. https://doi.org/10.1007/s10853-014-8380-3
Veljović Đ, Radovanović Ž, Dindune A, Palcevskis E, Krumina A, Petrović R, Janaćković Đ. The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics. in Journal of Materials Science. 2014;49(19):6793-6802. doi:10.1007/s10853-014-8380-3 .
Veljović, Đorđe, Radovanović, Željko, Dindune, Antonija, Palcevskis, Eriks, Krumina, Aija, Petrović, Rada, Janaćković, Đorđe, "The influence of Sr and Mn incorporated ions on the properties of microwave single- and two-step sintered biphasic HAP/TCP bioceramics" in Journal of Materials Science, 49, no. 19 (2014):6793-6802, https://doi.org/10.1007/s10853-014-8380-3 . .