Investigation of the dynamics of fluidized bed granulation process
Ispitivanje dinamike granulacije praškastih materijala u fluidizovanom sloju
Апстракт
In this paper, experimental investigation of the dynamics of the process of fluidized bed granulation was performed, in order to find optimal process conditions and binder concentration to achieve the desired granules development. The experiments were performed in batch system using corn flour as starting material. Ten experiments were performed in which sucrose solution of different concentrations (20, 30, 35 and 40 %) was used as binder. The temperature of the system was kept constant during the granulation process and amounted to 40-50°C. Samples were taken from the fluidized bed at time intervals of 3 min. The dynamics of granulation was examined by determining three different factors (bulk density, moisure content and particle size distribution) for each of the samples. It has been found that bulk density continuously decreases during the granulation process, while in the drying phase it remains constant. Particle size distribution has shown that the average diameter of the projec...ted surface increases uniformly during the process. By comparing all of the three investigated factors, it was shown that the best quality of granules is achieved using 35 % sucrose solution .
U ovom radu izvršeno je eksperimentalno ispitivanje procesa mokre granulacije u fluidizovanom sloju u cilju pronalaženja optimalnih uslova izvođenja procesa i sastava veziva kojim će se ostvariti željena dinamika razvoja granula. Ispitivanje je izvršeno u šaržnom sistemu, a korišćeno je kukuruzno brašno kao polazni materijal. Izvršeno je 10 eksperimenata u kojima je kao vezivno sredstvo korišćen rastvor saharoze različitih koncentracija: 20, 30, 35 i 40 %. Temperatura je održavana konstantnom tokom procesa granulacije i iznosila je 40-50C. Uzorci su iz sloja uzimani u jednakim vremenskim intervalima od 3 min. Dinamika granulacije ispitivana je određivanjem tri različita faktora (nasipne gustina, vlažnosti i raspodele veličine čestica) za svaki od uzoraka. Utvrđeno je da nasipna gustina kontinualno opada tokom izvođenja procesa granulacije, dok u fazi sušenja ostaje konstantna. Raspodela veličina čestica je pokazala da srednji prečnik projektovane površine ravnomerno raste tokom proces...a. Poređenjem sva tri ispitivana faktora pokazano je da se najbolji kvalitet granula postiže korišćenjem 35 % rastvora saharoze kao vezivnog sredstva.
Кључне речи:
fluidized bed granulation / granules / dynamics of granulation / Particle size distributionИзвор:
56th Meeting of the Serbian chemical Society - Proceedings, 2019, 55-59Издавач:
- Serbian Chemical Society, Belgrade
Финансирање / пројекти:
- Развој ефикаснијих хемијско-инжењерских процеса заснован на истраживањима феномена преноса и принципима интензификације процеса (RS-MESTD-Basic Research (BR or ON)-172022)
Институција/група
Tehnološko-metalurški fakultetTY - CONF AU - Kaluđerović-Radoičić, Tatjana AU - Đuriš, Mihal AU - Jaćimovski, Darko AU - Arsenijević, Zorana PY - 2019 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4190 AB - In this paper, experimental investigation of the dynamics of the process of fluidized bed granulation was performed, in order to find optimal process conditions and binder concentration to achieve the desired granules development. The experiments were performed in batch system using corn flour as starting material. Ten experiments were performed in which sucrose solution of different concentrations (20, 30, 35 and 40 %) was used as binder. The temperature of the system was kept constant during the granulation process and amounted to 40-50°C. Samples were taken from the fluidized bed at time intervals of 3 min. The dynamics of granulation was examined by determining three different factors (bulk density, moisure content and particle size distribution) for each of the samples. It has been found that bulk density continuously decreases during the granulation process, while in the drying phase it remains constant. Particle size distribution has shown that the average diameter of the projected surface increases uniformly during the process. By comparing all of the three investigated factors, it was shown that the best quality of granules is achieved using 35 % sucrose solution . AB - U ovom radu izvršeno je eksperimentalno ispitivanje procesa mokre granulacije u fluidizovanom sloju u cilju pronalaženja optimalnih uslova izvođenja procesa i sastava veziva kojim će se ostvariti željena dinamika razvoja granula. Ispitivanje je izvršeno u šaržnom sistemu, a korišćeno je kukuruzno brašno kao polazni materijal. Izvršeno je 10 eksperimenata u kojima je kao vezivno sredstvo korišćen rastvor saharoze različitih koncentracija: 20, 30, 35 i 40 %. Temperatura je održavana konstantnom tokom procesa granulacije i iznosila je 40-50C. Uzorci su iz sloja uzimani u jednakim vremenskim intervalima od 3 min. Dinamika granulacije ispitivana je određivanjem tri različita faktora (nasipne gustina, vlažnosti i raspodele veličine čestica) za svaki od uzoraka. Utvrđeno je da nasipna gustina kontinualno opada tokom izvođenja procesa granulacije, dok u fazi sušenja ostaje konstantna. Raspodela veličina čestica je pokazala da srednji prečnik projektovane površine ravnomerno raste tokom procesa. Poređenjem sva tri ispitivana faktora pokazano je da se najbolji kvalitet granula postiže korišćenjem 35 % rastvora saharoze kao vezivnog sredstva. PB - Serbian Chemical Society, Belgrade C3 - 56th Meeting of the Serbian chemical Society - Proceedings T1 - Investigation of the dynamics of fluidized bed granulation process T1 - Ispitivanje dinamike granulacije praškastih materijala u fluidizovanom sloju EP - 59 SP - 55 UR - https://hdl.handle.net/21.15107/rcub_technorep_4190 ER -
@conference{ author = "Kaluđerović-Radoičić, Tatjana and Đuriš, Mihal and Jaćimovski, Darko and Arsenijević, Zorana", year = "2019", abstract = "In this paper, experimental investigation of the dynamics of the process of fluidized bed granulation was performed, in order to find optimal process conditions and binder concentration to achieve the desired granules development. The experiments were performed in batch system using corn flour as starting material. Ten experiments were performed in which sucrose solution of different concentrations (20, 30, 35 and 40 %) was used as binder. The temperature of the system was kept constant during the granulation process and amounted to 40-50°C. Samples were taken from the fluidized bed at time intervals of 3 min. The dynamics of granulation was examined by determining three different factors (bulk density, moisure content and particle size distribution) for each of the samples. It has been found that bulk density continuously decreases during the granulation process, while in the drying phase it remains constant. Particle size distribution has shown that the average diameter of the projected surface increases uniformly during the process. By comparing all of the three investigated factors, it was shown that the best quality of granules is achieved using 35 % sucrose solution ., U ovom radu izvršeno je eksperimentalno ispitivanje procesa mokre granulacije u fluidizovanom sloju u cilju pronalaženja optimalnih uslova izvođenja procesa i sastava veziva kojim će se ostvariti željena dinamika razvoja granula. Ispitivanje je izvršeno u šaržnom sistemu, a korišćeno je kukuruzno brašno kao polazni materijal. Izvršeno je 10 eksperimenata u kojima je kao vezivno sredstvo korišćen rastvor saharoze različitih koncentracija: 20, 30, 35 i 40 %. Temperatura je održavana konstantnom tokom procesa granulacije i iznosila je 40-50C. Uzorci su iz sloja uzimani u jednakim vremenskim intervalima od 3 min. Dinamika granulacije ispitivana je određivanjem tri različita faktora (nasipne gustina, vlažnosti i raspodele veličine čestica) za svaki od uzoraka. Utvrđeno je da nasipna gustina kontinualno opada tokom izvođenja procesa granulacije, dok u fazi sušenja ostaje konstantna. Raspodela veličina čestica je pokazala da srednji prečnik projektovane površine ravnomerno raste tokom procesa. Poređenjem sva tri ispitivana faktora pokazano je da se najbolji kvalitet granula postiže korišćenjem 35 % rastvora saharoze kao vezivnog sredstva.", publisher = "Serbian Chemical Society, Belgrade", journal = "56th Meeting of the Serbian chemical Society - Proceedings", title = "Investigation of the dynamics of fluidized bed granulation process, Ispitivanje dinamike granulacije praškastih materijala u fluidizovanom sloju", pages = "59-55", url = "https://hdl.handle.net/21.15107/rcub_technorep_4190" }
Kaluđerović-Radoičić, T., Đuriš, M., Jaćimovski, D.,& Arsenijević, Z.. (2019). Investigation of the dynamics of fluidized bed granulation process. in 56th Meeting of the Serbian chemical Society - Proceedings Serbian Chemical Society, Belgrade., 55-59. https://hdl.handle.net/21.15107/rcub_technorep_4190
Kaluđerović-Radoičić T, Đuriš M, Jaćimovski D, Arsenijević Z. Investigation of the dynamics of fluidized bed granulation process. in 56th Meeting of the Serbian chemical Society - Proceedings. 2019;:55-59. https://hdl.handle.net/21.15107/rcub_technorep_4190 .
Kaluđerović-Radoičić, Tatjana, Đuriš, Mihal, Jaćimovski, Darko, Arsenijević, Zorana, "Investigation of the dynamics of fluidized bed granulation process" in 56th Meeting of the Serbian chemical Society - Proceedings (2019):55-59, https://hdl.handle.net/21.15107/rcub_technorep_4190 .