The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds
Само за регистроване кориснике
2022
Аутори
Milovanović, StojaLukić, Ivana
Stamenić, Marko
Kamiński, Piotr
Florkowski, Grzegorz
Tyśkiewicz, Katarzyna
Konkol, Marcin
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The present study was focused on improving the supercritical fluid extraction process dedicated to the recovery of highly valuable extract from Silybum marianum seeds. At first, the process was tested using supercritical CO2 at temperatures of 40 and 80 °C and pressures ranging from 100 to 300 bar. Obtained values were described using two literature models with acceptable agreement of experimental and calculated data. Further, the effect of the equipment design and process scale-up was investigated in four high-pressure units having volumes in the range from 280 mL to 40 L resulting in extraction yields up to 26 %. Based on the values of the parameters determined at the laboratory scale, the extraction process was successfully transferred to a semi-industrial scale. Finally, estimated costs for supercritical extract production in Poland for the year 2021 using a 1000 L high-pressure unit amounted to the price of 35.9 EUR per kg of extract.
Кључне речи:
Cost estimation / Milk thistle / ScCO2 / SFE scale-upИзвор:
Journal of Supercritical Fluids, 2022, 188, 105676-Издавач:
- Elsevier B.V.
Финансирање / пројекти:
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200135 (Универзитет у Београду, Технолошко-металуршки факултет) (RS-MESTD-inst-2020-200135)
- Polish National Agency for Academic Exchange ( NAWA ), Warsaw, Poland (the agreement number PPN/ULM/2020/1/00023/U/00001 )
Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Milovanović, Stoja AU - Lukić, Ivana AU - Stamenić, Marko AU - Kamiński, Piotr AU - Florkowski, Grzegorz AU - Tyśkiewicz, Katarzyna AU - Konkol, Marcin PY - 2022 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5175 AB - The present study was focused on improving the supercritical fluid extraction process dedicated to the recovery of highly valuable extract from Silybum marianum seeds. At first, the process was tested using supercritical CO2 at temperatures of 40 and 80 °C and pressures ranging from 100 to 300 bar. Obtained values were described using two literature models with acceptable agreement of experimental and calculated data. Further, the effect of the equipment design and process scale-up was investigated in four high-pressure units having volumes in the range from 280 mL to 40 L resulting in extraction yields up to 26 %. Based on the values of the parameters determined at the laboratory scale, the extraction process was successfully transferred to a semi-industrial scale. Finally, estimated costs for supercritical extract production in Poland for the year 2021 using a 1000 L high-pressure unit amounted to the price of 35.9 EUR per kg of extract. PB - Elsevier B.V. T2 - Journal of Supercritical Fluids T1 - The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds SP - 105676 VL - 188 DO - 10.1016/j.supflu.2022.105676 ER -
@article{ author = "Milovanović, Stoja and Lukić, Ivana and Stamenić, Marko and Kamiński, Piotr and Florkowski, Grzegorz and Tyśkiewicz, Katarzyna and Konkol, Marcin", year = "2022", abstract = "The present study was focused on improving the supercritical fluid extraction process dedicated to the recovery of highly valuable extract from Silybum marianum seeds. At first, the process was tested using supercritical CO2 at temperatures of 40 and 80 °C and pressures ranging from 100 to 300 bar. Obtained values were described using two literature models with acceptable agreement of experimental and calculated data. Further, the effect of the equipment design and process scale-up was investigated in four high-pressure units having volumes in the range from 280 mL to 40 L resulting in extraction yields up to 26 %. Based on the values of the parameters determined at the laboratory scale, the extraction process was successfully transferred to a semi-industrial scale. Finally, estimated costs for supercritical extract production in Poland for the year 2021 using a 1000 L high-pressure unit amounted to the price of 35.9 EUR per kg of extract.", publisher = "Elsevier B.V.", journal = "Journal of Supercritical Fluids", title = "The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds", pages = "105676", volume = "188", doi = "10.1016/j.supflu.2022.105676" }
Milovanović, S., Lukić, I., Stamenić, M., Kamiński, P., Florkowski, G., Tyśkiewicz, K.,& Konkol, M.. (2022). The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds. in Journal of Supercritical Fluids Elsevier B.V.., 188, 105676. https://doi.org/10.1016/j.supflu.2022.105676
Milovanović S, Lukić I, Stamenić M, Kamiński P, Florkowski G, Tyśkiewicz K, Konkol M. The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds. in Journal of Supercritical Fluids. 2022;188:105676. doi:10.1016/j.supflu.2022.105676 .
Milovanović, Stoja, Lukić, Ivana, Stamenić, Marko, Kamiński, Piotr, Florkowski, Grzegorz, Tyśkiewicz, Katarzyna, Konkol, Marcin, "The effect of equipment design and process scale-up on supercritical CO2 extraction: Case study for Silybum marianum seeds" in Journal of Supercritical Fluids, 188 (2022):105676, https://doi.org/10.1016/j.supflu.2022.105676 . .