ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine
Authors
Zdravković, JelenaRadovanović, Lidija
Simović, Bojana
Poleti, Dejan
Rogan, Jelena
Radovanović, Željko
Mihajlovski, Katarina
Conference object (Published version)
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Coordination chemistry provides the know-how for the synthesis of the
precursor compounds with variable composition and structures, while the thermal
induced changes may control the crystalline structure, phase composition,
morphology, size, texture, and other properties of their pyrolytic products [1]. In
terms of coordination chemistry and thermal analysis, our research has been focused
on the synthesis of mixed ligand complexes [2] that can be used as precursors for
obtaining diverse (compositional and structural) oxides, depending on their
thermoreactivity.
The main goal of this approach was the reduction of the temperature at which
the oxides are formed (up to 600–700 °C) comparative to the standard ceramic
methods. The effect of the different atmospheres (dynamic air or N2) on the thermal
decomposition of Zn benzenedicarboxylate complexes with 2,2’-dipyridylamine was
investigated. The formation of ZnO nanopowders was identified using XRPD and
FESEM techniques. The in...fluence of the adopted architecture of ternary metal
complexes used as templates for ZnO nanopowders was discussed. The thermal
decomposition kinetics of precursors was studied under non-isothermal conditions.
In addition, the antibacterial activity of obtained ZnO nanopowders was also
analyzed.
Source:
Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia, 2017, 79-Publisher:
- Belgrade : Institute for Multidisciplinary Research, University
Funding / projects:
- Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45007)
- Synthesis, processing and applications of nanostructured multifunctional materials with defined properties (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45019)
- Application of biotechnological methods for sustainable exploitation of by-products of agro-industry (RS-MESTD-Technological Development (TD or TR)-31035)
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Institution/Community
Inovacioni centarTY - CONF AU - Zdravković, Jelena AU - Radovanović, Lidija AU - Simović, Bojana AU - Poleti, Dejan AU - Rogan, Jelena AU - Radovanović, Željko AU - Mihajlovski, Katarina PY - 2017 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6157 AB - Coordination chemistry provides the know-how for the synthesis of the precursor compounds with variable composition and structures, while the thermal induced changes may control the crystalline structure, phase composition, morphology, size, texture, and other properties of their pyrolytic products [1]. In terms of coordination chemistry and thermal analysis, our research has been focused on the synthesis of mixed ligand complexes [2] that can be used as precursors for obtaining diverse (compositional and structural) oxides, depending on their thermoreactivity. The main goal of this approach was the reduction of the temperature at which the oxides are formed (up to 600–700 °C) comparative to the standard ceramic methods. The effect of the different atmospheres (dynamic air or N2) on the thermal decomposition of Zn benzenedicarboxylate complexes with 2,2’-dipyridylamine was investigated. The formation of ZnO nanopowders was identified using XRPD and FESEM techniques. The influence of the adopted architecture of ternary metal complexes used as templates for ZnO nanopowders was discussed. The thermal decomposition kinetics of precursors was studied under non-isothermal conditions. In addition, the antibacterial activity of obtained ZnO nanopowders was also analyzed. PB - Belgrade : Institute for Multidisciplinary Research, University C3 - Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia T1 - ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine SP - 79 UR - https://hdl.handle.net/21.15107/rcub_technorep_6157 ER -
@conference{ author = "Zdravković, Jelena and Radovanović, Lidija and Simović, Bojana and Poleti, Dejan and Rogan, Jelena and Radovanović, Željko and Mihajlovski, Katarina", year = "2017", abstract = "Coordination chemistry provides the know-how for the synthesis of the precursor compounds with variable composition and structures, while the thermal induced changes may control the crystalline structure, phase composition, morphology, size, texture, and other properties of their pyrolytic products [1]. In terms of coordination chemistry and thermal analysis, our research has been focused on the synthesis of mixed ligand complexes [2] that can be used as precursors for obtaining diverse (compositional and structural) oxides, depending on their thermoreactivity. The main goal of this approach was the reduction of the temperature at which the oxides are formed (up to 600–700 °C) comparative to the standard ceramic methods. The effect of the different atmospheres (dynamic air or N2) on the thermal decomposition of Zn benzenedicarboxylate complexes with 2,2’-dipyridylamine was investigated. The formation of ZnO nanopowders was identified using XRPD and FESEM techniques. The influence of the adopted architecture of ternary metal complexes used as templates for ZnO nanopowders was discussed. The thermal decomposition kinetics of precursors was studied under non-isothermal conditions. In addition, the antibacterial activity of obtained ZnO nanopowders was also analyzed.", publisher = "Belgrade : Institute for Multidisciplinary Research, University", journal = "Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia", title = "ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine", pages = "79", url = "https://hdl.handle.net/21.15107/rcub_technorep_6157" }
Zdravković, J., Radovanović, L., Simović, B., Poleti, D., Rogan, J., Radovanović, Ž.,& Mihajlovski, K.. (2017). ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine. in Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia Belgrade : Institute for Multidisciplinary Research, University., 79. https://hdl.handle.net/21.15107/rcub_technorep_6157
Zdravković J, Radovanović L, Simović B, Poleti D, Rogan J, Radovanović Ž, Mihajlovski K. ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine. in Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia. 2017;:79. https://hdl.handle.net/21.15107/rcub_technorep_6157 .
Zdravković, Jelena, Radovanović, Lidija, Simović, Bojana, Poleti, Dejan, Rogan, Jelena, Radovanović, Željko, Mihajlovski, Katarina, "ZnO nanopowders obtained by thermolysis of zinc benzenedicarboxylate complexes with 2,2’-dipyridylamine" in Programme and the Book of Abstracts / 4th Conference of The Serbian Society for Ceramic Materials, 4CSCS-2017, June 14-16, 2017, Belgrade, Serbia (2017):79, https://hdl.handle.net/21.15107/rcub_technorep_6157 .