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Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines

Authorized Users Only
2007
Authors
Marinović-Cincović, Milena
Babić, Dragan
Džunuzović, Enis
Popov-Pergal, Katarina
Rančić, Milica
Article (Published version)
Metadata
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Abstract
Polyimide resins were obtained from the reaction between N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and the following compounds with terminal amino groups: urea, 4-[(4-aminophenyl)sulfonyl] aniline, thiourea, 2-aminoethylamine, and 4.4'-diaminodiphenylmethane. The thermal and thermooxidative behaviour of the polyimide resins was studied by thermogravimetric measurements (TG) in oxygen and nitrogen. Polyimide resins have been irradiated (500 kGy) and their radiation stability evaluated on the basis of thermal and thermooxidative behaviour of irradiated samples. The thermal and oxidative degradation of the examined polyimides is complex and occurs in two phases. The first step occurs in both nitrogen and oxygen but it is somewhat less pronounced in oxygen due to oxidation and formation of more stable products. All samples showed very good radiation stability and there is almost no change in the first degradation step while the span of the peaks in the second ste...p is narrowed and temperatures are slightly lower.

Keywords:
polyimide resins / thermal stability / thermooxidative stability / radiation stability / N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetarnide
Source:
Polymer Degradation and Stability, 2007, 92, 9, 1730-1736
Publisher:
  • Elsevier Sci Ltd, Oxford

DOI: 10.1016/j.polymdegradstab.2007.05.021

ISSN: 0141-3910

WoS: 000250076900012

Scopus: 2-s2.0-34548404164
[ Google Scholar ]
5
5
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1133
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Marinović-Cincović, Milena
AU  - Babić, Dragan
AU  - Džunuzović, Enis
AU  - Popov-Pergal, Katarina
AU  - Rančić, Milica
PY  - 2007
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1133
AB  - Polyimide resins were obtained from the reaction between N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and the following compounds with terminal amino groups: urea, 4-[(4-aminophenyl)sulfonyl] aniline, thiourea, 2-aminoethylamine, and 4.4'-diaminodiphenylmethane. The thermal and thermooxidative behaviour of the polyimide resins was studied by thermogravimetric measurements (TG) in oxygen and nitrogen. Polyimide resins have been irradiated (500 kGy) and their radiation stability evaluated on the basis of thermal and thermooxidative behaviour of irradiated samples. The thermal and oxidative degradation of the examined polyimides is complex and occurs in two phases. The first step occurs in both nitrogen and oxygen but it is somewhat less pronounced in oxygen due to oxidation and formation of more stable products. All samples showed very good radiation stability and there is almost no change in the first degradation step while the span of the peaks in the second step is narrowed and temperatures are slightly lower.
PB  - Elsevier Sci Ltd, Oxford
T2  - Polymer Degradation and Stability
T1  - Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines
EP  - 1736
IS  - 9
SP  - 1730
VL  - 92
DO  - 10.1016/j.polymdegradstab.2007.05.021
ER  - 
@article{
author = "Marinović-Cincović, Milena and Babić, Dragan and Džunuzović, Enis and Popov-Pergal, Katarina and Rančić, Milica",
year = "2007",
abstract = "Polyimide resins were obtained from the reaction between N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and the following compounds with terminal amino groups: urea, 4-[(4-aminophenyl)sulfonyl] aniline, thiourea, 2-aminoethylamine, and 4.4'-diaminodiphenylmethane. The thermal and thermooxidative behaviour of the polyimide resins was studied by thermogravimetric measurements (TG) in oxygen and nitrogen. Polyimide resins have been irradiated (500 kGy) and their radiation stability evaluated on the basis of thermal and thermooxidative behaviour of irradiated samples. The thermal and oxidative degradation of the examined polyimides is complex and occurs in two phases. The first step occurs in both nitrogen and oxygen but it is somewhat less pronounced in oxygen due to oxidation and formation of more stable products. All samples showed very good radiation stability and there is almost no change in the first degradation step while the span of the peaks in the second step is narrowed and temperatures are slightly lower.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Polymer Degradation and Stability",
title = "Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines",
pages = "1736-1730",
number = "9",
volume = "92",
doi = "10.1016/j.polymdegradstab.2007.05.021"
}
Marinović-Cincović, M., Babić, D., Džunuzović, E., Popov-Pergal, K.,& Rančić, M.. (2007). Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines. in Polymer Degradation and Stability
Elsevier Sci Ltd, Oxford., 92(9), 1730-1736.
https://doi.org/10.1016/j.polymdegradstab.2007.05.021
Marinović-Cincović M, Babić D, Džunuzović E, Popov-Pergal K, Rančić M. Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines. in Polymer Degradation and Stability. 2007;92(9):1730-1736.
doi:10.1016/j.polymdegradstab.2007.05.021 .
Marinović-Cincović, Milena, Babić, Dragan, Džunuzović, Enis, Popov-Pergal, Katarina, Rančić, Milica, "Thermal, oxidative and radiation stability of polyimides. Part IV: Polyimides based on N-[4-benzoyl-2-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-phenyl]-acetamide and different diamines" in Polymer Degradation and Stability, 92, no. 9 (2007):1730-1736,
https://doi.org/10.1016/j.polymdegradstab.2007.05.021 . .

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