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dc.creatorAntonović, Dušan
dc.creatorStojanović, ND
dc.creatorBožić, Biljana M.
dc.creatorNikolić, AD
dc.creatorPetrović, Slobodan
dc.date.accessioned2021-03-10T09:41:09Z
dc.date.available2021-03-10T09:41:09Z
dc.date.issued1997
dc.identifier.issn0022-2860
dc.identifier.urihttp://TechnoRep.tmf.bg.ac.rs/handle/123456789/133
dc.description.abstractIn the present work we investigated the conformations of some N-mono-substituted propanamides of general formula CH3CH2CONHR, wherein R is chosen from n-(C-1-C-9)alkyl, cyclo(C-3-C-6)alkyl, some branched (C-3-C-6)alkyl or phenyl. The amides were synthesised by the well known Schotten-Baumann reaction-acylation of the corresponding amines with propionyl chloride. On the basis of FTIR data for diluted solutions (concentrations below 10(-3) mol dm(-3)) of N-mono-substituted propanamides in carbon tetrachloride, chloroform, dichloromethane, or a 1:1.5 mixture of benzene and carbon tetrachloride the exact position of the N-H stretching band was established. For spectroscopic data the different conformational isomers were assigned and its structures unequivocally proven. These results are in good accordance with H-1 NMR and MS data.en
dc.publisherElsevier, Amsterdam
dc.rightsrestrictedAccess
dc.sourceJournal of Molecular Structure
dc.subjectconformational isomersen
dc.subjectFTIR spectroscopyen
dc.subjectN-monosubstituted propanamidesen
dc.subjectN-H stretching banden
dc.titleSynthesis and FTIR spectroscopic study of some N-monosubstituted propanamidesen
dc.typeconferenceObject
dc.rights.licenseARR
dc.citation.epage423
dc.citation.other408: 421-423
dc.citation.spage421
dc.citation.volume408
dc.identifier.doi10.1016/S0022-2860(96)09743-8
dc.identifier.rcubconv_6345
dc.identifier.scopus2-s2.0-0030869053
dc.identifier.wosA1997XM03300077
dc.type.versionpublishedVersion


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