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Analysis of amphetamines illegally produced in Serbia

Analiza amfetamina ilegalno proizvedenog u Srbiji

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2008
0352-51390807691N.pdf (521.5Kb)
Authors
Nevešćanin, Marina
Banović-Stević, Sonja
Petrović, Slobodan
Vajs, Vlatka
article (publishedVersion)
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Abstract
Forensic practice in the Republic of Serbia faced the illegal production of amphetamine for the first time in 2003. This paper presents the results of the chemical characterization of 32 batches of amphetamine samples from three separate cases, for the purpose of identification of the active components and additives. Through the profiling of impurities of all samples, using gas chromatography/mass spectrometry (GC/MS), 30 compounds associated with amphetamine were identified. The results of the analysis of powder tartrate, sulfate and phosphate salts of amphetamine, as well as variously formulated tablets are presented in this study. The analyses showed that the amphetamines were synthesized by the Leuckart method in all cases.
Forenzička praksa u Republici Srbiji se prvi put srela sa ilegalnom proizvodnjom amfetamina 2003. godine. U ovom radu predstavljeni su rezultati hemijske karakterizacije 32 vrste uzoraka amfetamina koji potiču iz tri odvojena slučaja u cilju identifikacije aktivnih komponenti i aditiva. Profilisanjem nečistoća svih uzoraka pomoću gasno-masene spektrometrije identifikovano je 30 jedinjenja povezanih sa amfetaminom. Dati su rezultati analiza praškastih tartaratnih, sulfatnih i fosfatnih soli amfetamina kao i različito formulisanih tableta. Analize nečistoća su pokazale da je u svim slučajevima sinteza amfetamina vršena Leuckart-ovom reakcijom.
Keywords:
amphetamine / impurity profiling / Leuckart synthesis
Source:
Journal of the Serbian Chemical Society, 2008, 73, 7, 691-701
Publisher:
  • Serbian Chemical Society, Belgrade

ISSN: 0352-5139

WoS: 000257846900002

Scopus: 2-s2.0-47049118704
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URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1344
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  • Radovi istraživača / Researchers’ publications (TMF)
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