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The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra

Uticaj vezujućih agenasa na poboljšanje interakcija u kompozitnim gorivima utvrđen korišćenjem FTIR spektara

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2009
1440.pdf (1.297Mb)
Authors
Petković, Jelena
Wali, Amhamed
Mijin, Dušan
Ušćumlić, Gordana
Article (Published version)
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Abstract
Bonding agents synthesized in this research are 1, 3, 5-trisubstituted isocyanurates (substituents: 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl and 2, 3-epoxypropyl). All syntheses reactions were carried out according to a modified literature procedure. All the synthesized isocyanurates were identified by their melting point and FTIR, 1H NMR and UV spectroscopic data. The Fourier transform infrared spectrophotometry was also used to study the interaction between ammonium perchlorate, hydroxyl terminated poly(butadiene), carboxyl terminated poly(butadiene), cyclotetramethylenetetranitramine, tris[1-(2-methyl)aziridinyl]phosphine oxide and the compounds synthesized in this work. The results show that 1,3,5-tri(2-hydroxyethyl)isocyanurate is a universal bonding agent for the ammonium perchlorate/carboxyl terminated poly(butadiene)/cyclotetramethylenetetranitramine composite propellant system. .
Vezujući agensi sintetizovani u ovom radu predstavljaju 1,3,5-trisupstituisane izocijanurate (supstituenti: 2-hidroksietil, 3-hidroksipropil, 2-hidroksipropil i 2,3-epoksipropil). Sve sintetske reakcije su izvedene koristeći modifikovane literaturne postupke. Svi dobijeni izocijanurati su okarakterisani temperaturama topljenja, FTIR, 1H NMR, i UV spektroskopskim podacima. FTIR je takođe korišćen za proučavanje interakcija između amonijum-perhlorata (AP), poli(butadiena) sa hidroksi i karboksi krajnim grupama (HTPB i CTPB), tetrametilentetranitramina (HMX) i jedinjenja sintetizovanih u ovom radu. Rezultati su pokazali da se 1,3,5-tri(2-hidroksietil)izocijanurat može koristiti kao univerzalni vezujući agens za AP/CTPB/HMX sistem kompozitnih goriva. .
Keywords:
composite propellant / rocket composite propellant / binder / isocyanurates / kompozitno gorivo / raketno kompozitno gorivo / vezivo / izocijanourat
Source:
Scientific Technical Review, 2009, 59, 3-4, 12-16
Publisher:
  • Military Technical Institute, Belgrade

ISSN: 1820-0206

[ Google Scholar ]
Handle
https://hdl.handle.net/21.15107/rcub_technorep_1443
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1443
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Petković, Jelena
AU  - Wali, Amhamed
AU  - Mijin, Dušan
AU  - Ušćumlić, Gordana
PY  - 2009
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1443
AB  - Bonding agents synthesized in this research are 1, 3, 5-trisubstituted isocyanurates (substituents: 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl and 2, 3-epoxypropyl). All syntheses reactions were carried out according to a modified literature procedure. All the synthesized isocyanurates were identified by their melting point and FTIR, 1H NMR and UV spectroscopic data. The Fourier transform infrared spectrophotometry was also used to study the interaction between ammonium perchlorate, hydroxyl terminated poly(butadiene), carboxyl terminated poly(butadiene), cyclotetramethylenetetranitramine, tris[1-(2-methyl)aziridinyl]phosphine oxide and the compounds synthesized in this work. The results show that 1,3,5-tri(2-hydroxyethyl)isocyanurate is a universal bonding agent for the ammonium perchlorate/carboxyl terminated poly(butadiene)/cyclotetramethylenetetranitramine composite propellant system. .
AB  - Vezujući agensi sintetizovani u ovom radu predstavljaju 1,3,5-trisupstituisane izocijanurate (supstituenti: 2-hidroksietil, 3-hidroksipropil, 2-hidroksipropil i 2,3-epoksipropil). Sve sintetske reakcije su izvedene koristeći modifikovane literaturne postupke. Svi dobijeni izocijanurati su okarakterisani temperaturama topljenja, FTIR, 1H NMR, i UV spektroskopskim podacima. FTIR je takođe korišćen za proučavanje interakcija između amonijum-perhlorata (AP), poli(butadiena) sa hidroksi i karboksi krajnim grupama (HTPB i CTPB), tetrametilentetranitramina (HMX) i jedinjenja sintetizovanih u ovom radu. Rezultati su pokazali da se 1,3,5-tri(2-hidroksietil)izocijanurat može koristiti kao univerzalni vezujući agens za AP/CTPB/HMX sistem kompozitnih goriva. .
PB  - Military Technical Institute, Belgrade
T2  - Scientific Technical Review
T1  - The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra
T1  - Uticaj vezujućih agenasa na poboljšanje interakcija u kompozitnim gorivima utvrđen korišćenjem FTIR spektara
EP  - 16
IS  - 3-4
SP  - 12
VL  - 59
UR  - https://hdl.handle.net/21.15107/rcub_technorep_1443
ER  - 
@article{
author = "Petković, Jelena and Wali, Amhamed and Mijin, Dušan and Ušćumlić, Gordana",
year = "2009",
abstract = "Bonding agents synthesized in this research are 1, 3, 5-trisubstituted isocyanurates (substituents: 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl and 2, 3-epoxypropyl). All syntheses reactions were carried out according to a modified literature procedure. All the synthesized isocyanurates were identified by their melting point and FTIR, 1H NMR and UV spectroscopic data. The Fourier transform infrared spectrophotometry was also used to study the interaction between ammonium perchlorate, hydroxyl terminated poly(butadiene), carboxyl terminated poly(butadiene), cyclotetramethylenetetranitramine, tris[1-(2-methyl)aziridinyl]phosphine oxide and the compounds synthesized in this work. The results show that 1,3,5-tri(2-hydroxyethyl)isocyanurate is a universal bonding agent for the ammonium perchlorate/carboxyl terminated poly(butadiene)/cyclotetramethylenetetranitramine composite propellant system. ., Vezujući agensi sintetizovani u ovom radu predstavljaju 1,3,5-trisupstituisane izocijanurate (supstituenti: 2-hidroksietil, 3-hidroksipropil, 2-hidroksipropil i 2,3-epoksipropil). Sve sintetske reakcije su izvedene koristeći modifikovane literaturne postupke. Svi dobijeni izocijanurati su okarakterisani temperaturama topljenja, FTIR, 1H NMR, i UV spektroskopskim podacima. FTIR je takođe korišćen za proučavanje interakcija između amonijum-perhlorata (AP), poli(butadiena) sa hidroksi i karboksi krajnim grupama (HTPB i CTPB), tetrametilentetranitramina (HMX) i jedinjenja sintetizovanih u ovom radu. Rezultati su pokazali da se 1,3,5-tri(2-hidroksietil)izocijanurat može koristiti kao univerzalni vezujući agens za AP/CTPB/HMX sistem kompozitnih goriva. .",
publisher = "Military Technical Institute, Belgrade",
journal = "Scientific Technical Review",
title = "The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra, Uticaj vezujućih agenasa na poboljšanje interakcija u kompozitnim gorivima utvrđen korišćenjem FTIR spektara",
pages = "16-12",
number = "3-4",
volume = "59",
url = "https://hdl.handle.net/21.15107/rcub_technorep_1443"
}
Petković, J., Wali, A., Mijin, D.,& Ušćumlić, G.. (2009). The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra. in Scientific Technical Review
Military Technical Institute, Belgrade., 59(3-4), 12-16.
https://hdl.handle.net/21.15107/rcub_technorep_1443
Petković J, Wali A, Mijin D, Ušćumlić G. The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra. in Scientific Technical Review. 2009;59(3-4):12-16.
https://hdl.handle.net/21.15107/rcub_technorep_1443 .
Petković, Jelena, Wali, Amhamed, Mijin, Dušan, Ušćumlić, Gordana, "The influence of bonding agents in improving interactions in composite propellants, determined using the FTIR spectra" in Scientific Technical Review, 59, no. 3-4 (2009):12-16,
https://hdl.handle.net/21.15107/rcub_technorep_1443 .

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