Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V)... and for longer deposition time (20 min) and then converted to hydroxyapatite.
TY - JOUR
AU - Đošić, Marija
AU - Mišković-Stanković, Vesna
AU - Kačarević-Popović, Zorica M.
AU - Jokić, Bojan
AU - Bibić, Nataša M.
AU - Mitrić, Miodrag
AU - Milonjić, Slobodan K.
AU - Jančić-Heinemann, Radmila
AU - Stojanović, Jovica
PY - 2009
UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1514
AB - Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V) and for longer deposition time (20 min) and then converted to hydroxyapatite.
PB - Elsevier Science Bv, Amsterdam
T2 - Colloids and Surfaces A-Physicochemical and Engineering Aspects
T1 - Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium
EP - 117
IS - 1-3
SP - 110
VL - 341
DO - 10.1016/j.colsurfa.2009.03.046
ER -
@article{
author = "Đošić, Marija and Mišković-Stanković, Vesna and Kačarević-Popović, Zorica M. and Jokić, Bojan and Bibić, Nataša M. and Mitrić, Miodrag and Milonjić, Slobodan K. and Jančić-Heinemann, Radmila and Stojanović, Jovica",
year = "2009",
abstract = "Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V) and for longer deposition time (20 min) and then converted to hydroxyapatite.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Colloids and Surfaces A-Physicochemical and Engineering Aspects",
title = "Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium",
pages = "117-110",
number = "1-3",
volume = "341",
doi = "10.1016/j.colsurfa.2009.03.046"
}
Đošić, M., Mišković-Stanković, V., Kačarević-Popović, Z. M., Jokić, B., Bibić, N. M., Mitrić, M., Milonjić, S. K., Jančić-Heinemann, R.,& Stojanović, J.. (2009). Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium. in Colloids and Surfaces A-Physicochemical and Engineering Aspects
Elsevier Science Bv, Amsterdam., 341(1-3), 110-117.
https://doi.org/10.1016/j.colsurfa.2009.03.046
Đošić M, Mišković-Stanković V, Kačarević-Popović ZM, Jokić B, Bibić NM, Mitrić M, Milonjić SK, Jančić-Heinemann R, Stojanović J. Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium. in Colloids and Surfaces A-Physicochemical and Engineering Aspects. 2009;341(1-3):110-117.
doi:10.1016/j.colsurfa.2009.03.046 .
Đošić, Marija, Mišković-Stanković, Vesna, Kačarević-Popović, Zorica M., Jokić, Bojan, Bibić, Nataša M., Mitrić, Miodrag, Milonjić, Slobodan K., Jančić-Heinemann, Radmila, Stojanović, Jovica, "Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium" in Colloids and Surfaces A-Physicochemical and Engineering Aspects, 341, no. 1-3 (2009):110-117,
https://doi.org/10.1016/j.colsurfa.2009.03.046 . .
