Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium
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2009
Authors
Đošić, MarijaMišković-Stanković, Vesna

Kačarević-Popović, Zorica M.

Jokić, Bojan
Bibić, Nataša M.
Mitrić, Miodrag

Milonjić, Slobodan K.

Jančić-Heinemann, Radmila

Stojanović, Jovica
Article (Published version)

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Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V)... and for longer deposition time (20 min) and then converted to hydroxyapatite.
Keywords:
Monetite / Hydroxyapatite / Nanoparticle / Electrochemical synthesis / Electrophoretic deposition / TitaniumSource:
Colloids and Surfaces A-Physicochemical and Engineering Aspects, 2009, 341, 1-3, 110-117Publisher:
- Elsevier Science Bv, Amsterdam
Funding / projects:
- Elektrohemijske karakteristike oksidnih i polimernih prevlaka na modifikovanim površinama metala (RS-142061)
DOI: 10.1016/j.colsurfa.2009.03.046
ISSN: 0927-7757
WoS: 000266544400016
Scopus: 2-s2.0-67349117057
Institution/Community
Tehnološko-metalurški fakultetTY - JOUR AU - Đošić, Marija AU - Mišković-Stanković, Vesna AU - Kačarević-Popović, Zorica M. AU - Jokić, Bojan AU - Bibić, Nataša M. AU - Mitrić, Miodrag AU - Milonjić, Slobodan K. AU - Jančić-Heinemann, Radmila AU - Stojanović, Jovica PY - 2009 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/1514 AB - Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V) and for longer deposition time (20 min) and then converted to hydroxyapatite. PB - Elsevier Science Bv, Amsterdam T2 - Colloids and Surfaces A-Physicochemical and Engineering Aspects T1 - Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium EP - 117 IS - 1-3 SP - 110 VL - 341 DO - 10.1016/j.colsurfa.2009.03.046 ER -
@article{ author = "Đošić, Marija and Mišković-Stanković, Vesna and Kačarević-Popović, Zorica M. and Jokić, Bojan and Bibić, Nataša M. and Mitrić, Miodrag and Milonjić, Slobodan K. and Jančić-Heinemann, Radmila and Stojanović, Jovica", year = "2009", abstract = "Electrochemical synthesis of nanosized monetite powder was performed galvanostatically from homogeneous Solution of Na(2)H(2)EDTA center dot 2H(2)O, NaH2PO4 and CaCl2 at a concentration relationship Ca/EDTA/PO43- of 0.25/0.25/0.15 M at current density of 137 mA cm(-2) and pH value of 5.0. The synthesized monetite powder was characterized by X-ray diffraction, infrared spectroscopy, size distribution measurements, thermogravimetric and differential thermal analysis and scanning electron microscopy. Monetite powder was electrophoretically deposited on titanium from ethanol Suspension, using constant voltage method. The deposition was performed at constant voltage between 10 and 50 V and for a constant deposition time between 1 and 30 min. The influence of the applied voltage and deposition time on the mass and morphology of monetite deposits was investigated. It was shown that monetite deposits of the highest thickness and the lowest porosity can be formed at lower applied voltage (30 V) and for longer deposition time (20 min) and then converted to hydroxyapatite.", publisher = "Elsevier Science Bv, Amsterdam", journal = "Colloids and Surfaces A-Physicochemical and Engineering Aspects", title = "Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium", pages = "117-110", number = "1-3", volume = "341", doi = "10.1016/j.colsurfa.2009.03.046" }
Đošić, M., Mišković-Stanković, V., Kačarević-Popović, Z. M., Jokić, B., Bibić, N. M., Mitrić, M., Milonjić, S. K., Jančić-Heinemann, R.,& Stojanović, J.. (2009). Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium. in Colloids and Surfaces A-Physicochemical and Engineering Aspects Elsevier Science Bv, Amsterdam., 341(1-3), 110-117. https://doi.org/10.1016/j.colsurfa.2009.03.046
Đošić M, Mišković-Stanković V, Kačarević-Popović ZM, Jokić B, Bibić NM, Mitrić M, Milonjić SK, Jančić-Heinemann R, Stojanović J. Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium. in Colloids and Surfaces A-Physicochemical and Engineering Aspects. 2009;341(1-3):110-117. doi:10.1016/j.colsurfa.2009.03.046 .
Đošić, Marija, Mišković-Stanković, Vesna, Kačarević-Popović, Zorica M., Jokić, Bojan, Bibić, Nataša M., Mitrić, Miodrag, Milonjić, Slobodan K., Jančić-Heinemann, Radmila, Stojanović, Jovica, "Electrochemical synthesis of nanosized monetite powder and its electrophoretic deposition on titanium" in Colloids and Surfaces A-Physicochemical and Engineering Aspects, 341, no. 1-3 (2009):110-117, https://doi.org/10.1016/j.colsurfa.2009.03.046 . .