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Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology
Kinetic and operational electrolysis parameters determine the polarization characteristics, electrodeposition current efficiency, morphology, chemical composition and microstructure of nickel/iron/tungsten alloy deposits. The alloys electrodeposited at a current density of 50 mA cm(-2) to 1000 mA cm(-2) contain an amorphous phase and nanocrystals of an FCC solid solution of iron and tungsten in nickel. During annealing at temperatures above 500 degrees C, amorphous phase crystallization, crystalline grain growth of the FCC phase and a reduction in both internal microstrain and minimum density of chaotically distributed dislocations take place in the alloy. Milling the spongy deposit of the alloy causes amorphous phase crystallization, FCC-phase crystalline grain growth, and size reduction and rounding of powder particles.
TY - JOUR
AU - Cirović, N.
AU - Spasojević, Pavle
AU - Ribić-Zelenović, Lenka
AU - Masković, Pavle
AU - Spasojević, M.
PY - 2015
UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3002
AB - Kinetic and operational electrolysis parameters determine the polarization characteristics, electrodeposition current efficiency, morphology, chemical composition and microstructure of nickel/iron/tungsten alloy deposits. The alloys electrodeposited at a current density of 50 mA cm(-2) to 1000 mA cm(-2) contain an amorphous phase and nanocrystals of an FCC solid solution of iron and tungsten in nickel. During annealing at temperatures above 500 degrees C, amorphous phase crystallization, crystalline grain growth of the FCC phase and a reduction in both internal microstrain and minimum density of chaotically distributed dislocations take place in the alloy. Milling the spongy deposit of the alloy causes amorphous phase crystallization, FCC-phase crystalline grain growth, and size reduction and rounding of powder particles.
PB - Međunarodni Institut za nauku o sinterovanju, Beograd
T2 - Science of Sintering
T1 - Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology
EP - 365
IS - 3
SP - 347
VL - 47
DO - 10.2298/SOS1503347C
ER -
@article{
author = "Cirović, N. and Spasojević, Pavle and Ribić-Zelenović, Lenka and Masković, Pavle and Spasojević, M.",
year = "2015",
abstract = "Kinetic and operational electrolysis parameters determine the polarization characteristics, electrodeposition current efficiency, morphology, chemical composition and microstructure of nickel/iron/tungsten alloy deposits. The alloys electrodeposited at a current density of 50 mA cm(-2) to 1000 mA cm(-2) contain an amorphous phase and nanocrystals of an FCC solid solution of iron and tungsten in nickel. During annealing at temperatures above 500 degrees C, amorphous phase crystallization, crystalline grain growth of the FCC phase and a reduction in both internal microstrain and minimum density of chaotically distributed dislocations take place in the alloy. Milling the spongy deposit of the alloy causes amorphous phase crystallization, FCC-phase crystalline grain growth, and size reduction and rounding of powder particles.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology",
pages = "365-347",
number = "3",
volume = "47",
doi = "10.2298/SOS1503347C"
}
Cirović, N., Spasojević, P., Ribić-Zelenović, L., Masković, P.,& Spasojević, M.. (2015). Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 47(3), 347-365.
https://doi.org/10.2298/SOS1503347C
Cirović N, Spasojević P, Ribić-Zelenović L, Masković P, Spasojević M. Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology. in Science of Sintering. 2015;47(3):347-365.
doi:10.2298/SOS1503347C .
Cirović, N., Spasojević, Pavle, Ribić-Zelenović, Lenka, Masković, Pavle, Spasojević, M., "Synthesis, Structure and Properties of Nickel-Iron-Tungsten Alloy Electrodeposits PART I: Effect of Synthesis Parameters on Chemical Composition, Microstructure and Morphology" in Science of Sintering, 47, no. 3 (2015):347-365,
https://doi.org/10.2298/SOS1503347C . .
