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dc.creatorKalijadis, Ana
dc.creatorĐorđević, Jelena S.
dc.creatorTrtić-Petrović, Tatjana M.
dc.creatorVukčević, Marija
dc.creatorPopović, Maja
dc.creatorMaksimović, Vesna
dc.creatorRakočević, Zlatko Lj.
dc.creatorLaušević, Zoran
dc.date.accessioned2021-03-10T12:50:38Z
dc.date.available2021-03-10T12:50:38Z
dc.date.issued2015
dc.identifier.issn0008-6223
dc.identifier.urihttp://TechnoRep.tmf.bg.ac.rs/handle/123456789/3074
dc.description.abstractBoron doped hydrothermal carbon microspheres were synthesized by introducing boric acid into glucose precursor solution to obtain boron concentration from 0.1 to 1 wt. %. Following hydrothermal treatment, samples were thermally treated to 1000 degrees C. For obtained samples structural and surface characterization were performed. Characterization of obtained samples as material for carbon paste electrode was achieved by measurement of the Fe (CN)(6)(3-/4-) redox couple and linuron determination. Catalytic effect of boric acid on hydrothermal reaction induced enlargement of particle size for boron doped samples. Significant reduction of specific surface area for samples with highest boron concentration was observed. Boron was substitutionally incorporated in the structure of doped samples and incorporation up to 0.6 wt. % in precursor solution generates structure ordering, which induces a reduction of surface active sites for oxygen adsorption in a greater extent. It was found that modified structural and surface characteristics are responsible for good electron transfer property of carbon paste electrode based on doped samples with nominal boron concentration range from 0.2 to 0.6 wt. %. However, it has been shown that sample with nominal boron concentration of 0.2 wt. % proved to be most promising candidate as a material for carbon paste electrode.en
dc.publisherPergamon-Elsevier Science Ltd, Oxford
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45006/RS//
dc.rightsrestrictedAccess
dc.sourceCarbon
dc.titlePreparation of boron-doped hydrothermal carbon from glucose for carbon paste electrodeen
dc.typearticle
dc.rights.licenseARR
dc.citation.epage50
dc.citation.other95: 42-50
dc.citation.rankM21
dc.citation.spage42
dc.citation.volume95
dc.identifier.doi10.1016/j.carbon.2015.08.016
dc.identifier.scopus2-s2.0-84943625299
dc.identifier.wos000363312900006
dc.type.versionpublishedVersion


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Приказ основних података о документу