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Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide

Authorized Users Only
2017
Authors
Pajnik, Jelena
Stamenić, Marko
Radetić, Maja
Tomanović, Snežana
Sukara, Ratko
Mihaljica, Darko
Žižović, Irena
Article (Published version)
Metadata
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Abstract
This study discusses a possibility of cotton fabric impregnation with pyrethrum extract as a tick repellent in supercritical carbon dioxide. A solubility of pyrethrum extract in supercritical carbon dioxide has been determined at 35 and 40 degrees C and pressures ranging from 8 to 20 MPa. The highest solubility of 48.69 kg/m(3) was obtained at temperature of 35 degrees C and pressure of 20 MPa. Density -based equations of Chrastil, Adachi-Lu and del Valle-Aguilera were employed to correlate the experimental data. Based on the solubility data, conditions for the impregnation of cotton fabric were selected. Conditions at 40 degrees C and 8 MPa provided targeted quantities of the impregnated extract of 0.5% and 1% after 1 h and 2 h of the impregnation, respectively. The presence of pyrethrins on the cotton fabric's surface was confirmed by FTIR analysis. Repellent activity of both impregnated cotton fabrics (pyrethrum extract contents of 0.5% and 1%) was proven against ticks.
Keywords:
Supercritical carbon dioxide / Pyrethrum extract / Pyrethrin / Solubility / Supercritical solvent impregnation / Tick repellent activity
Source:
Journal of Supercritical Fluids, 2017, 128, 66-72
Publisher:
  • Elsevier Science Bv, Amsterdam
Funding / projects:
  • Functional physiologically active plant materials with additional values for application in pharmaceutical and food industry (RS-45017)
  • Enzootic transmission cycles of tick-borne pathogen microorganisms (RS-173006)

DOI: 10.1016/j.supflu.2017.05.006

ISSN: 0896-8446

WoS: 000408287400009

Scopus: 2-s2.0-85019869531
[ Google Scholar ]
15
14
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3574
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
  • Radovi istraživača (Inovacioni centar) / Researchers’ publications (Innovation Centre)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Pajnik, Jelena
AU  - Stamenić, Marko
AU  - Radetić, Maja
AU  - Tomanović, Snežana
AU  - Sukara, Ratko
AU  - Mihaljica, Darko
AU  - Žižović, Irena
PY  - 2017
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3574
AB  - This study discusses a possibility of cotton fabric impregnation with pyrethrum extract as a tick repellent in supercritical carbon dioxide. A solubility of pyrethrum extract in supercritical carbon dioxide has been determined at 35 and 40 degrees C and pressures ranging from 8 to 20 MPa. The highest solubility of 48.69 kg/m(3) was obtained at temperature of 35 degrees C and pressure of 20 MPa. Density -based equations of Chrastil, Adachi-Lu and del Valle-Aguilera were employed to correlate the experimental data. Based on the solubility data, conditions for the impregnation of cotton fabric were selected. Conditions at 40 degrees C and 8 MPa provided targeted quantities of the impregnated extract of 0.5% and 1% after 1 h and 2 h of the impregnation, respectively. The presence of pyrethrins on the cotton fabric's surface was confirmed by FTIR analysis. Repellent activity of both impregnated cotton fabrics (pyrethrum extract contents of 0.5% and 1%) was proven against ticks.
PB  - Elsevier Science Bv, Amsterdam
T2  - Journal of Supercritical Fluids
T1  - Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide
EP  - 72
SP  - 66
VL  - 128
DO  - 10.1016/j.supflu.2017.05.006
ER  - 
@article{
author = "Pajnik, Jelena and Stamenić, Marko and Radetić, Maja and Tomanović, Snežana and Sukara, Ratko and Mihaljica, Darko and Žižović, Irena",
year = "2017",
abstract = "This study discusses a possibility of cotton fabric impregnation with pyrethrum extract as a tick repellent in supercritical carbon dioxide. A solubility of pyrethrum extract in supercritical carbon dioxide has been determined at 35 and 40 degrees C and pressures ranging from 8 to 20 MPa. The highest solubility of 48.69 kg/m(3) was obtained at temperature of 35 degrees C and pressure of 20 MPa. Density -based equations of Chrastil, Adachi-Lu and del Valle-Aguilera were employed to correlate the experimental data. Based on the solubility data, conditions for the impregnation of cotton fabric were selected. Conditions at 40 degrees C and 8 MPa provided targeted quantities of the impregnated extract of 0.5% and 1% after 1 h and 2 h of the impregnation, respectively. The presence of pyrethrins on the cotton fabric's surface was confirmed by FTIR analysis. Repellent activity of both impregnated cotton fabrics (pyrethrum extract contents of 0.5% and 1%) was proven against ticks.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Journal of Supercritical Fluids",
title = "Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide",
pages = "72-66",
volume = "128",
doi = "10.1016/j.supflu.2017.05.006"
}
Pajnik, J., Stamenić, M., Radetić, M., Tomanović, S., Sukara, R., Mihaljica, D.,& Žižović, I.. (2017). Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide. in Journal of Supercritical Fluids
Elsevier Science Bv, Amsterdam., 128, 66-72.
https://doi.org/10.1016/j.supflu.2017.05.006
Pajnik J, Stamenić M, Radetić M, Tomanović S, Sukara R, Mihaljica D, Žižović I. Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide. in Journal of Supercritical Fluids. 2017;128:66-72.
doi:10.1016/j.supflu.2017.05.006 .
Pajnik, Jelena, Stamenić, Marko, Radetić, Maja, Tomanović, Snežana, Sukara, Ratko, Mihaljica, Darko, Žižović, Irena, "Impregnation of cotton fabric with pyrethrum extract in supercritical carbon dioxide" in Journal of Supercritical Fluids, 128 (2017):66-72,
https://doi.org/10.1016/j.supflu.2017.05.006 . .

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