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The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent

Authorized Users Only
2017
Authors
Bucko, M.
Culliton, D.
Betts, A. J.
Bajat, Jelena
Article (Published version)
Metadata
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Abstract
Electrochemical and microscopic techniques were used for the characterisation of Zn-Mn coatings electrodeposited from choline chloride-urea deep eutectic solvent. Cyclic voltammograms show that there was no discernible Mn reduction peak when only Mn2+ was present in DES solution. The distinct Mn peak developed only upon addition of Zn2+ to the solution, probably due to previous Zn nucleation on the steel substrate. It was found that 22-27 wt-% Mn deposited at current densities of 3-8 mA cm(-2), amounts significantly higher than those obtained from aqueous electrolytes. Since higher deposition current densities resulted in the formation of a porous surface consisting of clusters of nodular crystallites, the optimal deposition c.d was determined to be 3 mA cm(-2).
Keywords:
Zn-Mn coating / Electrodeposition / Deep eutectic solvent / Choline chloride / Urea / Ionic liquid / Cyclic voltammetry / Alloy
Source:
Transactions of the Institute of Metal Finishing, 2017, 95, 1, 60-64
Publisher:
  • Taylor & Francis Ltd, Abingdon
Funding / projects:
  • Synthesis, processing and applications of nanostructured multifunctional materials with defined properties (RS-45019)
  • COST ActionEuropean Cooperation in Science and Technology (COST) [MP1407]

DOI: 10.1080/00202967.2017.1255412

ISSN: 0020-2967

WoS: 000394497000012

Scopus: 2-s2.0-85009997377
[ Google Scholar ]
23
18
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3700
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Bucko, M.
AU  - Culliton, D.
AU  - Betts, A. J.
AU  - Bajat, Jelena
PY  - 2017
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/3700
AB  - Electrochemical and microscopic techniques were used for the characterisation of Zn-Mn coatings electrodeposited from choline chloride-urea deep eutectic solvent. Cyclic voltammograms show that there was no discernible Mn reduction peak when only Mn2+ was present in DES solution. The distinct Mn peak developed only upon addition of Zn2+ to the solution, probably due to previous Zn nucleation on the steel substrate. It was found that 22-27 wt-% Mn deposited at current densities of 3-8 mA cm(-2), amounts significantly higher than those obtained from aqueous electrolytes. Since higher deposition current densities resulted in the formation of a porous surface consisting of clusters of nodular crystallites, the optimal deposition c.d was determined to be 3 mA cm(-2).
PB  - Taylor & Francis Ltd, Abingdon
T2  - Transactions of the Institute of Metal Finishing
T1  - The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent
EP  - 64
IS  - 1
SP  - 60
VL  - 95
DO  - 10.1080/00202967.2017.1255412
ER  - 
@article{
author = "Bucko, M. and Culliton, D. and Betts, A. J. and Bajat, Jelena",
year = "2017",
abstract = "Electrochemical and microscopic techniques were used for the characterisation of Zn-Mn coatings electrodeposited from choline chloride-urea deep eutectic solvent. Cyclic voltammograms show that there was no discernible Mn reduction peak when only Mn2+ was present in DES solution. The distinct Mn peak developed only upon addition of Zn2+ to the solution, probably due to previous Zn nucleation on the steel substrate. It was found that 22-27 wt-% Mn deposited at current densities of 3-8 mA cm(-2), amounts significantly higher than those obtained from aqueous electrolytes. Since higher deposition current densities resulted in the formation of a porous surface consisting of clusters of nodular crystallites, the optimal deposition c.d was determined to be 3 mA cm(-2).",
publisher = "Taylor & Francis Ltd, Abingdon",
journal = "Transactions of the Institute of Metal Finishing",
title = "The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent",
pages = "64-60",
number = "1",
volume = "95",
doi = "10.1080/00202967.2017.1255412"
}
Bucko, M., Culliton, D., Betts, A. J.,& Bajat, J.. (2017). The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent. in Transactions of the Institute of Metal Finishing
Taylor & Francis Ltd, Abingdon., 95(1), 60-64.
https://doi.org/10.1080/00202967.2017.1255412
Bucko M, Culliton D, Betts AJ, Bajat J. The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent. in Transactions of the Institute of Metal Finishing. 2017;95(1):60-64.
doi:10.1080/00202967.2017.1255412 .
Bucko, M., Culliton, D., Betts, A. J., Bajat, Jelena, "The electrochemical deposition of Zn-Mn coating from choline chloride-urea deep eutectic solvent" in Transactions of the Institute of Metal Finishing, 95, no. 1 (2017):60-64,
https://doi.org/10.1080/00202967.2017.1255412 . .

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