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dc.creatorZdravković, Jelena D.
dc.creatorRadovanović, Lidija
dc.creatorPoleti, Dejan
dc.creatorRogan, Jelena R.
dc.creatorVulić, Predrag J.
dc.creatorRadovanović, Željko
dc.creatorMinić, Dragica M.
dc.date.accessioned2021-03-10T13:51:00Z
dc.date.available2021-03-10T13:51:00Z
dc.date.issued2018
dc.identifier.issn1293-2558
dc.identifier.urihttp://TechnoRep.tmf.bg.ac.rs/handle/123456789/4003
dc.description.abstractThe design of mixed-ligand complexes are of increasing interest from fundamental as well as technological and curative aspects. Having that in mind, we studied zinc complex containing 2,2'-dipyridylamine (dipya) and dianion of isophthalic acid (ipht), [Zn(dipya)(ipht)](n), as promising precursor for synthesis of nanostructured metal oxide. In that sense, the mechanism and degradation kinetics of [Zn(dipya)(ipht)](n), was analyzed under non-isothermal conditions in nitrogen and in air atmospheres. Peak deconvolution of the [Zn(dipya)(ipht)](n), decomposition profile, in the form of a derivative thermogram (DTG), in nitrogen atmosphere, revealed the presence of three decomposition steps, while in air five single steps were isolated. In both cases ZnO is formed as residue at 530 degrees C: pure (in air) or in amorphous matrix (nitrogen). In air we obtained well crystalized ZnO nanospheres (-25 nm), by thermal treatment in temperature range 370-530 degrees C showing that this complex could be considered as good precursor for production of nanosized ZnO.en
dc.publisherElsevier Masson SAS
dc.relationinfo:eu-repo/grantAgreement/MESTD/Integrated and Interdisciplinary Research (IIR or III)/45007/RS//
dc.rightsrestrictedAccess
dc.sourceSolid State Sciences
dc.subjectMechanism and kinetics of degradationen
dc.subjectDeconvolutionen
dc.subjectThermodynamicsen
dc.subjectProductionen
dc.titleMechanism and degradation kinetics of zinc complex containing isophthalato and 2,2 '-dipyridylamine ligands under different atmospheresen
dc.typearticle
dc.rights.licenseARR
dc.citation.epage131
dc.citation.other80: 123-131
dc.citation.rankM22
dc.citation.spage123
dc.citation.volume80
dc.identifier.doi10.1016/j.solidstatesciences.2018.04.013
dc.identifier.scopus2-s2.0-85047637094
dc.identifier.wos000432824000016
dc.type.versionpublishedVersion


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