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The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study

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2019
4057.pdf (1.693Mb)
Authors
Mićović, Dragana
Pagnacco, Maja C.
Banković, Predrag
Maletaškić, Jelena
Matović, Branko
Đokić, Veljko
Stojmenović, Marija
Article (Published version)
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Abstract
Potential non-toxic pink and red ceramic pigments based on CeO2 were successfully synthesized by self-propagating room temperature method and thermally treated at 600, 900 and 1200 degrees C for 15 min. The structure, morphology and optical properties, as well as thermal stability of Ce1-xErxO2-delta and Ce1-xPrxO2-delta (x = 0.05) were examined. Single-phase composition of all obtained CeO2 pigments was confirmed using XRPD method and Raman spectroscopy and it was not dependent on temperature. The mechanism of structural behaviour was thoroughly examined using Raman and FTIR spectroscopy. Nanometric dimensions of the crystallites of all pigments were confirmed using XRPD, TEM and FE-SEM analysis. Colour properties were dependent on the temperature treatment, and their position in the chromaticity diagram was studied using UV/VIS spectrophotometry. Colour efficiency measurements were supplemented by colorimetric analysis. It is proved that all samples are thermally stable in the invest...igated temperature range (up to 1200 degrees C), and their potential application as environmentally friendly pigments of desired colour is confirmed.

Keywords:
CeO2 / Er and Pr doping / structure / optical properties / colour / pigments
Source:
Processing and Application of Ceramics, 2019, 13, 3, 310-321
Publisher:
  • Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)
  • Nanostructured Functional and Composite Materials in Catalytic and Sorption Processes (RS-45001)
  • Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-45007)
  • Dynamics of nonlinear physicochemical and biochemical systems with modeling and predicting of their behavior under nonequilibrium conditions (RS-172015)

DOI: 10.2298/PAC1903310M

ISSN: 1820-6131

WoS: 000488636100012

Scopus: 2-s2.0-85073593512
[ Google Scholar ]
3
2
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4060
Collections
  • Radovi istraživača (Inovacioni centar) / Researchers’ publications (Innovation Centre)
Institution/Community
Inovacioni centar
TY  - JOUR
AU  - Mićović, Dragana
AU  - Pagnacco, Maja C.
AU  - Banković, Predrag
AU  - Maletaškić, Jelena
AU  - Matović, Branko
AU  - Đokić, Veljko
AU  - Stojmenović, Marija
PY  - 2019
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4060
AB  - Potential non-toxic pink and red ceramic pigments based on CeO2 were successfully synthesized by self-propagating room temperature method and thermally treated at 600, 900 and 1200 degrees C for 15 min. The structure, morphology and optical properties, as well as thermal stability of Ce1-xErxO2-delta and Ce1-xPrxO2-delta (x = 0.05) were examined. Single-phase composition of all obtained CeO2 pigments was confirmed using XRPD method and Raman spectroscopy and it was not dependent on temperature. The mechanism of structural behaviour was thoroughly examined using Raman and FTIR spectroscopy. Nanometric dimensions of the crystallites of all pigments were confirmed using XRPD, TEM and FE-SEM analysis. Colour properties were dependent on the temperature treatment, and their position in the chromaticity diagram was studied using UV/VIS spectrophotometry. Colour efficiency measurements were supplemented by colorimetric analysis. It is proved that all samples are thermally stable in the investigated temperature range (up to 1200 degrees C), and their potential application as environmentally friendly pigments of desired colour is confirmed.
PB  - Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
T2  - Processing and Application of Ceramics
T1  - The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study
EP  - 321
IS  - 3
SP  - 310
VL  - 13
DO  - 10.2298/PAC1903310M
ER  - 
@article{
author = "Mićović, Dragana and Pagnacco, Maja C. and Banković, Predrag and Maletaškić, Jelena and Matović, Branko and Đokić, Veljko and Stojmenović, Marija",
year = "2019",
abstract = "Potential non-toxic pink and red ceramic pigments based on CeO2 were successfully synthesized by self-propagating room temperature method and thermally treated at 600, 900 and 1200 degrees C for 15 min. The structure, morphology and optical properties, as well as thermal stability of Ce1-xErxO2-delta and Ce1-xPrxO2-delta (x = 0.05) were examined. Single-phase composition of all obtained CeO2 pigments was confirmed using XRPD method and Raman spectroscopy and it was not dependent on temperature. The mechanism of structural behaviour was thoroughly examined using Raman and FTIR spectroscopy. Nanometric dimensions of the crystallites of all pigments were confirmed using XRPD, TEM and FE-SEM analysis. Colour properties were dependent on the temperature treatment, and their position in the chromaticity diagram was studied using UV/VIS spectrophotometry. Colour efficiency measurements were supplemented by colorimetric analysis. It is proved that all samples are thermally stable in the investigated temperature range (up to 1200 degrees C), and their potential application as environmentally friendly pigments of desired colour is confirmed.",
publisher = "Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad",
journal = "Processing and Application of Ceramics",
title = "The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study",
pages = "321-310",
number = "3",
volume = "13",
doi = "10.2298/PAC1903310M"
}
Mićović, D., Pagnacco, M. C., Banković, P., Maletaškić, J., Matović, B., Đokić, V.,& Stojmenović, M.. (2019). The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study. in Processing and Application of Ceramics
Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad., 13(3), 310-321.
https://doi.org/10.2298/PAC1903310M
Mićović D, Pagnacco MC, Banković P, Maletaškić J, Matović B, Đokić V, Stojmenović M. The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study. in Processing and Application of Ceramics. 2019;13(3):310-321.
doi:10.2298/PAC1903310M .
Mićović, Dragana, Pagnacco, Maja C., Banković, Predrag, Maletaškić, Jelena, Matović, Branko, Đokić, Veljko, Stojmenović, Marija, "The influence of short thermal treatment on structure, morphology and optical properties of Er and Pr doped ceria pigments: Comparative study" in Processing and Application of Ceramics, 13, no. 3 (2019):310-321,
https://doi.org/10.2298/PAC1903310M . .

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