Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives
Само за регистроване кориснике
2019
Аутори
Stasić, JovanaSelaković, Nenad
Puač, Nevena
Miletić, Maja
Malović, Gordana
Petrović, Zoran Lj
Veljović, Đorđe
Miletić, Vesna
Чланак у часопису (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
ObjectivesThe study aims to evaluate the effects of non-thermal atmospheric plasma (NTAP) treatments on dentin wetting and surface free energy (SFE) and compare the effects of NTAP treatment, etch-and-rinse, and self-etch protocols for application of universal adhesives.Materials and methodsMid-coronal dentin of intact third molars was used to measure contact angles of distilled water, ethylene-glycol, and diiodomethane and calculate SFE following different NTAP preset treatments (feeding gas consisting of pure He, He + 1% O-2, He + 1.5% O-2), power input (1 or 3W), and tip-to-surface distance (2, 4, or 8mm). Contact angles of reference liquids and SFE of dentin following He + 1.5% O-2 at 3-W and 4-mm treatment was compared to phosphoric acid etching. Contact angles of Single Bond Universal (SBU; 3M ESPE) and Clearfil Universal Bond (CUB; Kuraray Noritake) were measured following NTAP, etch-and-rinse, and self-etch protocols.ResultsNTAP significantly reduced contact angles of reference... liquids and increased dentin SFE compared to untreated dentin (p lt 0.05). O-2 intensified the effect of He NTAP (p lt 0.05). NTAP and phosphoric acid increased dentin polarity and Lewis base surface characteristics. Phosphoric acid increased contact angles of adhesives compared to the self-etch protocol (p lt 0.05). NTAP resulted in lower adhesive contact angles than phosphoric acid, the difference being statistically significant for CUB (p lt 0.05). Compared to the self-etch protocol, NTAP slightly reduced CUB contact angle but not that of SBU (p gt 0.05).ConclusionsHe NTAP with and without O-2 increased dentin wetting and SFE, surpassing the effect of phosphoric acid and lowering adhesive contact angles. NTAP produced no apparent micro-morphological changes on dentin surface comparable to acid etching.Clinical significanceNTAP treatment of dentin prior to adhesive application increases dentin wetting and surface free energy facilitating better adhesive distribution on dentin surface compared to phosphoric acid etching and similar to the self-etch application protocol.
Кључне речи:
Contact angle / Dentin / Non-thermal atmospheric plasma / Surface free energy / Universal adhesive / WettingИзвор:
Clinical Oral Investigations, 2019, 23, 3, 1383-1396Издавач:
- Springer Heidelberg, Heidelberg
Финансирање / пројекти:
- Примене нискотемпературних плазми у биомедицини, заштити човекове околине и нанотехнологијама (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-41011)
- Фундаментални процеси и примене транспорта честица у неравнотежним плазмама, траповима и наноструктурама (RS-MESTD-Basic Research (BR or ON)-171037)
- Развој и примена метода и материјала за мониторинг нових загађујућих и токсичних органских материја и тешких метала (RS-MESTD-Basic Research (BR or ON)-172007)
Напомена:
- Peer reviewed manuscript: http://technorep.tmf.bg.ac.rs/handle/123456789/5048
Повезане информације:
- Верзија документа
http://technorep.tmf.bg.ac.rs/handle/123456789/5048
DOI: 10.1007/s00784-018-2563-2
ISSN: 1432-6981
PubMed: 30022272
WoS: 000465332900041
Scopus: 2-s2.0-85050180607
Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Stasić, Jovana AU - Selaković, Nenad AU - Puač, Nevena AU - Miletić, Maja AU - Malović, Gordana AU - Petrović, Zoran Lj AU - Veljović, Đorđe AU - Miletić, Vesna PY - 2019 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4263 AB - ObjectivesThe study aims to evaluate the effects of non-thermal atmospheric plasma (NTAP) treatments on dentin wetting and surface free energy (SFE) and compare the effects of NTAP treatment, etch-and-rinse, and self-etch protocols for application of universal adhesives.Materials and methodsMid-coronal dentin of intact third molars was used to measure contact angles of distilled water, ethylene-glycol, and diiodomethane and calculate SFE following different NTAP preset treatments (feeding gas consisting of pure He, He + 1% O-2, He + 1.5% O-2), power input (1 or 3W), and tip-to-surface distance (2, 4, or 8mm). Contact angles of reference liquids and SFE of dentin following He + 1.5% O-2 at 3-W and 4-mm treatment was compared to phosphoric acid etching. Contact angles of Single Bond Universal (SBU; 3M ESPE) and Clearfil Universal Bond (CUB; Kuraray Noritake) were measured following NTAP, etch-and-rinse, and self-etch protocols.ResultsNTAP significantly reduced contact angles of reference liquids and increased dentin SFE compared to untreated dentin (p lt 0.05). O-2 intensified the effect of He NTAP (p lt 0.05). NTAP and phosphoric acid increased dentin polarity and Lewis base surface characteristics. Phosphoric acid increased contact angles of adhesives compared to the self-etch protocol (p lt 0.05). NTAP resulted in lower adhesive contact angles than phosphoric acid, the difference being statistically significant for CUB (p lt 0.05). Compared to the self-etch protocol, NTAP slightly reduced CUB contact angle but not that of SBU (p gt 0.05).ConclusionsHe NTAP with and without O-2 increased dentin wetting and SFE, surpassing the effect of phosphoric acid and lowering adhesive contact angles. NTAP produced no apparent micro-morphological changes on dentin surface comparable to acid etching.Clinical significanceNTAP treatment of dentin prior to adhesive application increases dentin wetting and surface free energy facilitating better adhesive distribution on dentin surface compared to phosphoric acid etching and similar to the self-etch application protocol. PB - Springer Heidelberg, Heidelberg T2 - Clinical Oral Investigations T1 - Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives EP - 1396 IS - 3 SP - 1383 VL - 23 DO - 10.1007/s00784-018-2563-2 ER -
@article{ author = "Stasić, Jovana and Selaković, Nenad and Puač, Nevena and Miletić, Maja and Malović, Gordana and Petrović, Zoran Lj and Veljović, Đorđe and Miletić, Vesna", year = "2019", abstract = "ObjectivesThe study aims to evaluate the effects of non-thermal atmospheric plasma (NTAP) treatments on dentin wetting and surface free energy (SFE) and compare the effects of NTAP treatment, etch-and-rinse, and self-etch protocols for application of universal adhesives.Materials and methodsMid-coronal dentin of intact third molars was used to measure contact angles of distilled water, ethylene-glycol, and diiodomethane and calculate SFE following different NTAP preset treatments (feeding gas consisting of pure He, He + 1% O-2, He + 1.5% O-2), power input (1 or 3W), and tip-to-surface distance (2, 4, or 8mm). Contact angles of reference liquids and SFE of dentin following He + 1.5% O-2 at 3-W and 4-mm treatment was compared to phosphoric acid etching. Contact angles of Single Bond Universal (SBU; 3M ESPE) and Clearfil Universal Bond (CUB; Kuraray Noritake) were measured following NTAP, etch-and-rinse, and self-etch protocols.ResultsNTAP significantly reduced contact angles of reference liquids and increased dentin SFE compared to untreated dentin (p lt 0.05). O-2 intensified the effect of He NTAP (p lt 0.05). NTAP and phosphoric acid increased dentin polarity and Lewis base surface characteristics. Phosphoric acid increased contact angles of adhesives compared to the self-etch protocol (p lt 0.05). NTAP resulted in lower adhesive contact angles than phosphoric acid, the difference being statistically significant for CUB (p lt 0.05). Compared to the self-etch protocol, NTAP slightly reduced CUB contact angle but not that of SBU (p gt 0.05).ConclusionsHe NTAP with and without O-2 increased dentin wetting and SFE, surpassing the effect of phosphoric acid and lowering adhesive contact angles. NTAP produced no apparent micro-morphological changes on dentin surface comparable to acid etching.Clinical significanceNTAP treatment of dentin prior to adhesive application increases dentin wetting and surface free energy facilitating better adhesive distribution on dentin surface compared to phosphoric acid etching and similar to the self-etch application protocol.", publisher = "Springer Heidelberg, Heidelberg", journal = "Clinical Oral Investigations", title = "Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives", pages = "1396-1383", number = "3", volume = "23", doi = "10.1007/s00784-018-2563-2" }
Stasić, J., Selaković, N., Puač, N., Miletić, M., Malović, G., Petrović, Z. L., Veljović, Đ.,& Miletić, V.. (2019). Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives. in Clinical Oral Investigations Springer Heidelberg, Heidelberg., 23(3), 1383-1396. https://doi.org/10.1007/s00784-018-2563-2
Stasić J, Selaković N, Puač N, Miletić M, Malović G, Petrović ZL, Veljović Đ, Miletić V. Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives. in Clinical Oral Investigations. 2019;23(3):1383-1396. doi:10.1007/s00784-018-2563-2 .
Stasić, Jovana, Selaković, Nenad, Puač, Nevena, Miletić, Maja, Malović, Gordana, Petrović, Zoran Lj, Veljović, Đorđe, Miletić, Vesna, "Effects of non-thermal atmospheric plasma treatment on dentin wetting and surface free energy for application of universal adhesives" in Clinical Oral Investigations, 23, no. 3 (2019):1383-1396, https://doi.org/10.1007/s00784-018-2563-2 . .