Structural, microstructural and mechanical properties of sintered iron-doped mullite
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2020
Authors
Ilić, Svetlana M.
Ivanovski, Valentin N.

Radovanović, Željko

Egelja, Adela

Kokunesoski, Maja

Saponjić, Aleksandra
Matović, Branko

Article (Published version)

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The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure.
Keywords:
Mullite / Iron / XRD / Mossbauer spectroscopy / Microstructure / MicrohardnessSource:
Materials Science and Engineering B-Advanced Functional Solid-State Materials, 2020, 256Publisher:
- Elsevier, Amsterdam
Funding / projects:
DOI: 10.1016/j.mseb.2020.114543
ISSN: 0921-5107
WoS: 000528213200003
Scopus: 2-s2.0-85083155366
Institution/Community
Inovacioni centarTY - JOUR AU - Ilić, Svetlana M. AU - Ivanovski, Valentin N. AU - Radovanović, Željko AU - Egelja, Adela AU - Kokunesoski, Maja AU - Saponjić, Aleksandra AU - Matović, Branko PY - 2020 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4502 AB - The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure. PB - Elsevier, Amsterdam T2 - Materials Science and Engineering B-Advanced Functional Solid-State Materials T1 - Structural, microstructural and mechanical properties of sintered iron-doped mullite VL - 256 DO - 10.1016/j.mseb.2020.114543 ER -
@article{ author = "Ilić, Svetlana M. and Ivanovski, Valentin N. and Radovanović, Željko and Egelja, Adela and Kokunesoski, Maja and Saponjić, Aleksandra and Matović, Branko", year = "2020", abstract = "The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure.", publisher = "Elsevier, Amsterdam", journal = "Materials Science and Engineering B-Advanced Functional Solid-State Materials", title = "Structural, microstructural and mechanical properties of sintered iron-doped mullite", volume = "256", doi = "10.1016/j.mseb.2020.114543" }
Ilić, S. M., Ivanovski, V. N., Radovanović, Ž., Egelja, A., Kokunesoski, M., Saponjić, A.,& Matović, B.. (2020). Structural, microstructural and mechanical properties of sintered iron-doped mullite. in Materials Science and Engineering B-Advanced Functional Solid-State Materials Elsevier, Amsterdam., 256. https://doi.org/10.1016/j.mseb.2020.114543
Ilić SM, Ivanovski VN, Radovanović Ž, Egelja A, Kokunesoski M, Saponjić A, Matović B. Structural, microstructural and mechanical properties of sintered iron-doped mullite. in Materials Science and Engineering B-Advanced Functional Solid-State Materials. 2020;256. doi:10.1016/j.mseb.2020.114543 .
Ilić, Svetlana M., Ivanovski, Valentin N., Radovanović, Željko, Egelja, Adela, Kokunesoski, Maja, Saponjić, Aleksandra, Matović, Branko, "Structural, microstructural and mechanical properties of sintered iron-doped mullite" in Materials Science and Engineering B-Advanced Functional Solid-State Materials, 256 (2020), https://doi.org/10.1016/j.mseb.2020.114543 . .