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Structural, microstructural and mechanical properties of sintered iron-doped mullite

Authorized Users Only
2020
Authors
Ilić, Svetlana M.
Ivanovski, Valentin N.
Radovanović, Željko
Egelja, Adela
Kokunesoski, Maja
Saponjić, Aleksandra
Matović, Branko
Article (Published version)
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Abstract
The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure.
Keywords:
Mullite / Iron / XRD / Mossbauer spectroscopy / Microstructure / Microhardness
Source:
Materials Science and Engineering B-Advanced Functional Solid-State Materials, 2020, 256
Publisher:
  • Elsevier, Amsterdam
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)

DOI: 10.1016/j.mseb.2020.114543

ISSN: 0921-5107

WoS: 000528213200003

Scopus: 2-s2.0-85083155366
[ Google Scholar ]
3
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URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4502
Collections
  • Radovi istraživača (Inovacioni centar) / Researchers’ publications (Innovation Centre)
Institution/Community
Inovacioni centar
TY  - JOUR
AU  - Ilić, Svetlana M.
AU  - Ivanovski, Valentin N.
AU  - Radovanović, Željko
AU  - Egelja, Adela
AU  - Kokunesoski, Maja
AU  - Saponjić, Aleksandra
AU  - Matović, Branko
PY  - 2020
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4502
AB  - The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure.
PB  - Elsevier, Amsterdam
T2  - Materials Science and Engineering B-Advanced Functional Solid-State Materials
T1  - Structural, microstructural and mechanical properties of sintered iron-doped mullite
VL  - 256
DO  - 10.1016/j.mseb.2020.114543
ER  - 
@article{
author = "Ilić, Svetlana M. and Ivanovski, Valentin N. and Radovanović, Željko and Egelja, Adela and Kokunesoski, Maja and Saponjić, Aleksandra and Matović, Branko",
year = "2020",
abstract = "The study of an effect of iron doping on the structural, microstructural and mechanical properties of sintered iron-doped mullite is presented. The results of phase composition, performed in detail by Mossbauer spectroscopy and XRD analysis, revealed that all added iron was inside the mullite lattice forming the single phase up to 12% by weight of Fe2O3 and 1300 degrees C. Samples, which were processed at 1550 degrees C, contained secondary phases, hematite or magnetite, regardless of the amount of added iron. Furthermore, the addition of iron decreases the values of relative linear shrinkage comparing to the values of undoped one (similar to 18%) while the densities of the sintered samples rise as well as their values of microhardness. Even though the density values were not too high (90 TD%), the obtained values of microhardness were excellent, 1634 HV0.1 for maximum iron content due to the characteristic mullite microstructure.",
publisher = "Elsevier, Amsterdam",
journal = "Materials Science and Engineering B-Advanced Functional Solid-State Materials",
title = "Structural, microstructural and mechanical properties of sintered iron-doped mullite",
volume = "256",
doi = "10.1016/j.mseb.2020.114543"
}
Ilić, S. M., Ivanovski, V. N., Radovanović, Ž., Egelja, A., Kokunesoski, M., Saponjić, A.,& Matović, B.. (2020). Structural, microstructural and mechanical properties of sintered iron-doped mullite. in Materials Science and Engineering B-Advanced Functional Solid-State Materials
Elsevier, Amsterdam., 256.
https://doi.org/10.1016/j.mseb.2020.114543
Ilić SM, Ivanovski VN, Radovanović Ž, Egelja A, Kokunesoski M, Saponjić A, Matović B. Structural, microstructural and mechanical properties of sintered iron-doped mullite. in Materials Science and Engineering B-Advanced Functional Solid-State Materials. 2020;256.
doi:10.1016/j.mseb.2020.114543 .
Ilić, Svetlana M., Ivanovski, Valentin N., Radovanović, Željko, Egelja, Adela, Kokunesoski, Maja, Saponjić, Aleksandra, Matović, Branko, "Structural, microstructural and mechanical properties of sintered iron-doped mullite" in Materials Science and Engineering B-Advanced Functional Solid-State Materials, 256 (2020),
https://doi.org/10.1016/j.mseb.2020.114543 . .

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