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Polymerization studies: The application of differential thermogravimetric analysis

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1993
Authors
Popović, Ivanka
Katsikas, Lynne
Weller, Horst
Schrötter, S.
Veličković, Jovan S.
article (publishedVersion)
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Abstract
The application of differential thermogravimetric analysis (DTGA) to the study of polymerization mechanisms is illustrated using as examples the radical polymerization of di‐n‐alkyl itaconates and methyl methacrylate (MMA). Five poly(di‐n‐alkyl itaconates) were prepared in bulk, both in the presence and absence of n‐dodecyl mercaptan and in solution using AIBN as initiator. The poly(methyl methacrylate) (PMMA) was photoinitiated using colloidal CdS as a photosensitizer. The thermal properties of the resulting polymers are described in terms of the proposed polymerization mechanisms. The advantages and disadvantages of DTGA for the identification of thermally weak structures are discussed.
Source:
Journal of Applied Polymer Science, 1993, 50, 8, 1475-1482
Publisher:
  • Wiley, Hoboken

DOI: 10.1002/app.1993.070500819

ISSN: 0021-8995

PubMed:

Scopus: 2-s2.0-0027695337
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URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/46
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  • Radovi istraživača / Researchers’ publications (TMF)
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Tehnološko-metalurški fakultet

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