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dc.creatorMladenović, Ivana O.
dc.creatorLamovec, Jelena S.
dc.creatorVasiljević-Radović, Dana G.
dc.creatorVasilić, Rastko
dc.creatorRadojević, Vesna
dc.creatorNikolić, Nebojša D.
dc.date.accessioned2022-03-04T11:17:53Z
dc.date.available2022-03-04T11:17:53Z
dc.date.issued2021
dc.identifier.issn2075-4701
dc.identifier.urihttp://TechnoRep.tmf.bg.ac.rs/handle/123456789/4816
dc.description.abstractThe influence of various electrolysis parameters, such as the type of cathode, composition of the electrolyte and electrolysis time, on the morphology, structure and hardness of copper coatings has been investigated. Morphology and structure of the coatings were analyzed by scanning electron microscope (SEM), atomic force microscope (AFM) and X-ray diffraction (XRD), while coating hardness was examined by Vickers microindentation test applying the Chicot-Lesage (C-L) composite hardness model. Depending on the conditions of electrolysis, two types of Cu coatings were obtained: fine-grained mat coatings with a strong (220) preferred orientation from the sulfate electrolyte and smooth mirror bright coatings with a strong (200) preferred orientation from the electrolyte with added leveling/brightening additives. The mat coatings showed larger both measured composite and calculated coating hardness than the mirror bright coatings, that can be explained by the phenomena on boundary among grains. Independent of electrolysis conditions, the critical relative indentation depth (RID) of 0.14 was established for all types of the Cu coatings, separating the zone in which the composite hardness can be equaled with the coating hardness and the zone requiring an application of the C-L model for a determination of the absolute hardness of the Cu coatings.en
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200026/RS//
dc.relationinfo:eu-repo/grantAgreement/MESTD/inst-2020/200135/RS//
dc.rightsopenAccess
dc.rights.urihttps://creativecommons.org/licenses/by/4.0/
dc.sourceMetals
dc.subjectelectrodepositionen
dc.subjectcopperen
dc.subjecthardnessen
dc.subjectSEMen
dc.subjectAFMen
dc.subjectXRDen
dc.subjectcomposite hardness modelen
dc.subjectthe Chicot-Lesage modelen
dc.titleImplementation of the Chicot-Lesage Composite Hardness Model in a Determination of Absolute Hardness of Copper Coatings Obtained by the Electrodeposition Processesen
dc.typearticle
dc.rights.licenseBY
dc.citation.issue11
dc.citation.other11(11): -
dc.citation.rankM21
dc.citation.volume11
dc.identifier.doi10.3390/met11111807
dc.identifier.fulltexthttp://TechnoRep.tmf.bg.ac.rs/bitstream/id/7736/bitstream_7736.pdf
dc.identifier.rcubconv_6241
dc.identifier.scopus2-s2.0-85118720313
dc.identifier.wos000727342400001
dc.type.versionpublishedVersion


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