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Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method

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2021
Synthesis_of_Silica_pub_2021.pdf (3.654Mb)
Authors
Stopic, Srecko
Wenz, Felix
Volkov-Husović, Tatjana
Friedrich, Bernd
Article (Published version)
Metadata
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Abstract
Silica has sparked strong interest in hydrometallurgy, catalysis, the cement industry, and paper coating. The synthesis of silica particles was performed at 900 degrees C using the ultrasonic spray pyrolysis (USP) method. Ideally, spherical particles are obtained in one horizontal reactor from an aerosol. The controlled synthesis of submicron particles of silica was reached by changing the concentration of precursor solution. The experimentally obtained particles were compared with theoretically calculated values of silica particles. The characterization was performed using a scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS). X-ray diffraction, frequently abbreviated as XRD, was used to analyze the structure of obtained materials. The obtained silica by ultrasonic spray pyrolysis had an amorphous structure. In comparison to other methods such as sol-gel, acidic treatment, thermal decomposition, stirred bead milling, and high-pressure carbonation, the adv...antage of the ultrasonic spray method for preparation of nanosized silica controlled morphology is the simplicity of setting up individual process segments and changing their configuration, one-step continuous synthesis, and the possibility of synthesizing nanoparticles from various precursors.

Keywords:
silica / ultrasonic spray pyrolysis / synthesis
Source:
Metals, 2021, 11, 3

DOI: 10.3390/met11030463

ISSN: 2075-4701

WoS: 000633864900001

Scopus: 2-s2.0-85102179497
[ Google Scholar ]
9
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4902
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Stopic, Srecko
AU  - Wenz, Felix
AU  - Volkov-Husović, Tatjana
AU  - Friedrich, Bernd
PY  - 2021
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/4902
AB  - Silica has sparked strong interest in hydrometallurgy, catalysis, the cement industry, and paper coating. The synthesis of silica particles was performed at 900 degrees C using the ultrasonic spray pyrolysis (USP) method. Ideally, spherical particles are obtained in one horizontal reactor from an aerosol. The controlled synthesis of submicron particles of silica was reached by changing the concentration of precursor solution. The experimentally obtained particles were compared with theoretically calculated values of silica particles. The characterization was performed using a scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS). X-ray diffraction, frequently abbreviated as XRD, was used to analyze the structure of obtained materials. The obtained silica by ultrasonic spray pyrolysis had an amorphous structure. In comparison to other methods such as sol-gel, acidic treatment, thermal decomposition, stirred bead milling, and high-pressure carbonation, the advantage of the ultrasonic spray method for preparation of nanosized silica controlled morphology is the simplicity of setting up individual process segments and changing their configuration, one-step continuous synthesis, and the possibility of synthesizing nanoparticles from various precursors.
T2  - Metals
T1  - Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method
IS  - 3
VL  - 11
DO  - 10.3390/met11030463
ER  - 
@article{
author = "Stopic, Srecko and Wenz, Felix and Volkov-Husović, Tatjana and Friedrich, Bernd",
year = "2021",
abstract = "Silica has sparked strong interest in hydrometallurgy, catalysis, the cement industry, and paper coating. The synthesis of silica particles was performed at 900 degrees C using the ultrasonic spray pyrolysis (USP) method. Ideally, spherical particles are obtained in one horizontal reactor from an aerosol. The controlled synthesis of submicron particles of silica was reached by changing the concentration of precursor solution. The experimentally obtained particles were compared with theoretically calculated values of silica particles. The characterization was performed using a scanning electron microscope (SEM) and energy-dispersive X-ray spectroscopy (EDS). X-ray diffraction, frequently abbreviated as XRD, was used to analyze the structure of obtained materials. The obtained silica by ultrasonic spray pyrolysis had an amorphous structure. In comparison to other methods such as sol-gel, acidic treatment, thermal decomposition, stirred bead milling, and high-pressure carbonation, the advantage of the ultrasonic spray method for preparation of nanosized silica controlled morphology is the simplicity of setting up individual process segments and changing their configuration, one-step continuous synthesis, and the possibility of synthesizing nanoparticles from various precursors.",
journal = "Metals",
title = "Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method",
number = "3",
volume = "11",
doi = "10.3390/met11030463"
}
Stopic, S., Wenz, F., Volkov-Husović, T.,& Friedrich, B.. (2021). Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method. in Metals, 11(3).
https://doi.org/10.3390/met11030463
Stopic S, Wenz F, Volkov-Husović T, Friedrich B. Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method. in Metals. 2021;11(3).
doi:10.3390/met11030463 .
Stopic, Srecko, Wenz, Felix, Volkov-Husović, Tatjana, Friedrich, Bernd, "Synthesis of Silica Particles Using Ultrasonic Spray Pyrolysis Method" in Metals, 11, no. 3 (2021),
https://doi.org/10.3390/met11030463 . .

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