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Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent
dc.creator | Rajić, Nevenka | |
dc.creator | Zabukovec-Logar, Nataša | |
dc.creator | Golobić, Amalija | |
dc.creator | Kaučič, Venčeslav | |
dc.date.accessioned | 2021-03-10T10:06:01Z | |
dc.date.available | 2021-03-10T10:06:01Z | |
dc.date.issued | 2003 | |
dc.identifier.issn | 0022-3697 | |
dc.identifier.uri | http://TechnoRep.tmf.bg.ac.rs/handle/123456789/517 | |
dc.description.abstract | Colorless plate-like crystals (AIPO-1,2DAP) crystallize from a clear 'AlPO4-1,2-diaminopropane' reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH4+)(1,2-H(2)DAP)(2+)(AlP2O8)(3-), confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150 K reveal the space group Pc2(1)n with a = 8.2788(2), b = 16.7882(3), c = 8.6608(2) Angstrom, and V = 1203.73(5) Angstrom(3). The AIPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH4+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network. | en |
dc.publisher | Pergamon-Elsevier Science Ltd, Oxford | |
dc.rights | restrictedAccess | |
dc.source | Journal of Physics and Chemistry of Solids | |
dc.subject | crystal structure | en |
dc.subject | X-ray diffraction | en |
dc.title | Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent | en |
dc.type | article | |
dc.rights.license | ARR | |
dc.citation.epage | 1103 | |
dc.citation.issue | 7 | |
dc.citation.other | 64(7): 1097-1103 | |
dc.citation.rank | M22 | |
dc.citation.spage | 1097 | |
dc.citation.volume | 64 | |
dc.identifier.doi | 10.1016/S0022-3697(03)00002-7 | |
dc.identifier.scopus | 2-s2.0-0038216933 | |
dc.identifier.wos | 000182996800007 | |
dc.type.version | publishedVersion |