Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity
Ispitivanje mogućnosti sinteze inovativnih sorbenata i nosača katalizatora na bazi keramike kontrolisane otvorene poroznosti
2022
Preuzimanje 🢃
Autori
Nikolić, VesnaĐokić, Jovana
Kamberović, Željko
Marinković, Aleksandar
Jevtić, Sanja
Anđić, Zoran
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
The aim of this study was to investigate a possibility of synthesis of porous ceramics with controlled open porosity, which could be used as sorbents and catalyst supports. Two organic additives were used to obtain open porosity: polystyrene beads and cellulose fibers, which are mixed with kaolin clay powder and the appropriate water content. Samples were sintered at 1050 oC for 1 h. Characterization of the obtained products included X-ray powder diffraction analysis (XRPD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA) and elemental CHNS analysis. In addition, porosity was examined by quantification of visual information. The specific surface areas were determined by the Brunauer–Emmett–Teller (BET) method. Also, density and compressive strength of the obtained samples were assessed. It was determined that by sintering, the organic component completely leaves the system. For samples prepared with polystyrene beads ...and with cellulose fibers, satisfactory mechanical properties were obtained: compressive strengths were 1.42 and 1.56 MPa, respectively. It was noted that significantly higher open porosity was obtained by using polystyrene beads as a sacrificial template (porosity of ~56 %) instead of cellulose fibers (porosity of ~6 %).
Ključne reči:
porous sintered clay / kaolin / polystyrene / cellulose fibersIzvor:
Hemijska industrija, 2022, 76, 2, 87-95Finansiranje / projekti:
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200135 (Univerzitet u Beogradu, Tehnološko-metalurški fakultet) (RS-MESTD-inst-2020-200135)
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200288 (Inovacioni centar Hemijskog fakulteta u Beogradu doo) (RS-MESTD-inst-2020-200288)
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200288 (Inovacioni centar Hemijskog fakulteta u Beogradu doo) (RS-MESTD-inst-2020-200288)
Kolekcije
Institucija/grupa
Inovacioni centarTY - JOUR AU - Nikolić, Vesna AU - Đokić, Jovana AU - Kamberović, Željko AU - Marinković, Aleksandar AU - Jevtić, Sanja AU - Anđić, Zoran PY - 2022 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5192 AB - The aim of this study was to investigate a possibility of synthesis of porous ceramics with controlled open porosity, which could be used as sorbents and catalyst supports. Two organic additives were used to obtain open porosity: polystyrene beads and cellulose fibers, which are mixed with kaolin clay powder and the appropriate water content. Samples were sintered at 1050 oC for 1 h. Characterization of the obtained products included X-ray powder diffraction analysis (XRPD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA) and elemental CHNS analysis. In addition, porosity was examined by quantification of visual information. The specific surface areas were determined by the Brunauer–Emmett–Teller (BET) method. Also, density and compressive strength of the obtained samples were assessed. It was determined that by sintering, the organic component completely leaves the system. For samples prepared with polystyrene beads and with cellulose fibers, satisfactory mechanical properties were obtained: compressive strengths were 1.42 and 1.56 MPa, respectively. It was noted that significantly higher open porosity was obtained by using polystyrene beads as a sacrificial template (porosity of ~56 %) instead of cellulose fibers (porosity of ~6 %). T2 - Hemijska industrija T1 - Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity T1 - Ispitivanje mogućnosti sinteze inovativnih sorbenata i nosača katalizatora na bazi keramike kontrolisane otvorene poroznosti EP - 95 IS - 2 SP - 87 VL - 76 DO - 10.2298/HEMIND210809005N ER -
@article{ author = "Nikolić, Vesna and Đokić, Jovana and Kamberović, Željko and Marinković, Aleksandar and Jevtić, Sanja and Anđić, Zoran", year = "2022", abstract = "The aim of this study was to investigate a possibility of synthesis of porous ceramics with controlled open porosity, which could be used as sorbents and catalyst supports. Two organic additives were used to obtain open porosity: polystyrene beads and cellulose fibers, which are mixed with kaolin clay powder and the appropriate water content. Samples were sintered at 1050 oC for 1 h. Characterization of the obtained products included X-ray powder diffraction analysis (XRPD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA) and elemental CHNS analysis. In addition, porosity was examined by quantification of visual information. The specific surface areas were determined by the Brunauer–Emmett–Teller (BET) method. Also, density and compressive strength of the obtained samples were assessed. It was determined that by sintering, the organic component completely leaves the system. For samples prepared with polystyrene beads and with cellulose fibers, satisfactory mechanical properties were obtained: compressive strengths were 1.42 and 1.56 MPa, respectively. It was noted that significantly higher open porosity was obtained by using polystyrene beads as a sacrificial template (porosity of ~56 %) instead of cellulose fibers (porosity of ~6 %).", journal = "Hemijska industrija", title = "Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity, Ispitivanje mogućnosti sinteze inovativnih sorbenata i nosača katalizatora na bazi keramike kontrolisane otvorene poroznosti", pages = "95-87", number = "2", volume = "76", doi = "10.2298/HEMIND210809005N" }
Nikolić, V., Đokić, J., Kamberović, Ž., Marinković, A., Jevtić, S.,& Anđić, Z.. (2022). Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity. in Hemijska industrija, 76(2), 87-95. https://doi.org/10.2298/HEMIND210809005N
Nikolić V, Đokić J, Kamberović Ž, Marinković A, Jevtić S, Anđić Z. Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity. in Hemijska industrija. 2022;76(2):87-95. doi:10.2298/HEMIND210809005N .
Nikolić, Vesna, Đokić, Jovana, Kamberović, Željko, Marinković, Aleksandar, Jevtić, Sanja, Anđić, Zoran, "Investigating possibilities for synthesis of novel sorbents and catalyst carriers based on ceramics with controlled open porosity" in Hemijska industrija, 76, no. 2 (2022):87-95, https://doi.org/10.2298/HEMIND210809005N . .