The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys
Abstract
The effect of coarse intermetallic particles on the fracture process in 7000 alloy forgings was investigated using three alloys with different (Fe + Si) impurity levels. The intermetallic particles were identified by selective etching and energy dispersive spectroscopy analysis conducted on a scanning electron microscope. Their geometrical parameters were estimated by image analysis and then correlated with area fractions of different fracture modes on the broken fracture toughness test specimens. It was found that the dominant fracture mode varies with the (Fe + Si) content. The coarse voiding at large intermetallic particles increases systematically with an increase of the impurity level, which in turn increases the amount and size of particles containing Fe and Si while decreasing their spacing. That the crack nucleation and propagation are accelerated by these particles was revealed by in situ scanning electron microscopy observation of the fracture process.
Keywords:
7000 Alloys / Alloy purity / Fracture modes / In situ tensile test / Intermetallics / Scanning electron microscopySource:
Journal of Microscopy, 2006, 224, 1, 117-120Publisher:
- Wiley-Blackwell
Funding / projects:
- Specijalne teme mehanike loma materijala (RS-144027)
DOI: 10.1111/j.1365-2818.2006.01683.x
ISSN: 1365-2818
WoS: 000241893300032
Scopus: 2-s2.0-33750810812
Institution/Community
Tehnološko-metalurški fakultetTY - JOUR AU - Vratnica, M. AU - Cvijović, Zorica AU - Degische, H.P. AU - Requena, G.C. PY - 2006 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5469 AB - The effect of coarse intermetallic particles on the fracture process in 7000 alloy forgings was investigated using three alloys with different (Fe + Si) impurity levels. The intermetallic particles were identified by selective etching and energy dispersive spectroscopy analysis conducted on a scanning electron microscope. Their geometrical parameters were estimated by image analysis and then correlated with area fractions of different fracture modes on the broken fracture toughness test specimens. It was found that the dominant fracture mode varies with the (Fe + Si) content. The coarse voiding at large intermetallic particles increases systematically with an increase of the impurity level, which in turn increases the amount and size of particles containing Fe and Si while decreasing their spacing. That the crack nucleation and propagation are accelerated by these particles was revealed by in situ scanning electron microscopy observation of the fracture process. PB - Wiley-Blackwell T2 - Journal of Microscopy T1 - The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys EP - 120 IS - 1 SP - 117 VL - 224 DO - 10.1111/j.1365-2818.2006.01683.x ER -
@article{ author = "Vratnica, M. and Cvijović, Zorica and Degische, H.P. and Requena, G.C.", year = "2006", abstract = "The effect of coarse intermetallic particles on the fracture process in 7000 alloy forgings was investigated using three alloys with different (Fe + Si) impurity levels. The intermetallic particles were identified by selective etching and energy dispersive spectroscopy analysis conducted on a scanning electron microscope. Their geometrical parameters were estimated by image analysis and then correlated with area fractions of different fracture modes on the broken fracture toughness test specimens. It was found that the dominant fracture mode varies with the (Fe + Si) content. The coarse voiding at large intermetallic particles increases systematically with an increase of the impurity level, which in turn increases the amount and size of particles containing Fe and Si while decreasing their spacing. That the crack nucleation and propagation are accelerated by these particles was revealed by in situ scanning electron microscopy observation of the fracture process.", publisher = "Wiley-Blackwell", journal = "Journal of Microscopy", title = "The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys", pages = "120-117", number = "1", volume = "224", doi = "10.1111/j.1365-2818.2006.01683.x" }
Vratnica, M., Cvijović, Z., Degische, H.P.,& Requena, G.C.. (2006). The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys. in Journal of Microscopy Wiley-Blackwell., 224(1), 117-120. https://doi.org/10.1111/j.1365-2818.2006.01683.x
Vratnica M, Cvijović Z, Degische H, Requena G. The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys. in Journal of Microscopy. 2006;224(1):117-120. doi:10.1111/j.1365-2818.2006.01683.x .
Vratnica, M., Cvijović, Zorica, Degische, H.P., Requena, G.C., "The effect of coarse intermetallic particles on the fracture process in forged 7000 alloys" in Journal of Microscopy, 224, no. 1 (2006):117-120, https://doi.org/10.1111/j.1365-2818.2006.01683.x . .