Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements
Korelacija stepena konverzije i količine oslobođenih supstanci iz dentalnih kompozitnih cemenata
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This study examined the possible correlation between the degree of conversion (DC) and the amount of substances eluted from three commercial cured resin-based cements. The DC of the various resin-based cements was measured by Raman spectroscopy, while the quantity of unreacted monomers released from the cement matrix (triethylene glycol dimethacrylate, TEGDMA, urethane dimethacrylate, UDMA, 2-hydroxyethyl methacrylate, HEMA and bisphenol A) was determined by high pressure liquid chromatography (HPLC). The obtained results, after multiple statistical evaluation (one way ANOVA, LSD post hoc test), showed no significant differences in the DC values between the resin cements. On the contrary, the results of the HPLC analysis depicted statistically significant differences between the three materials with respect to the amount of leached monomers. In addition, no correlation between the DC and the amount of eluted substances from the tested cured composite cements was found.
Rad istražuje moguću korelaciju stepena konverzije (DC) i količine oslobođenih monomernih supstanci iz tri komercijalna preparata kompozitnih dentalnih cemenata. Stepen konverzije kompozitnih cemenata određen je metodom Raman spektroskopije, dok je količina neizreagovalih i oslobođenih monomera iz cementnog matriksa detektovana pomoću HPLC metode. Rezultati dobijeni nakon višestruke statističke evaluacije (one way ANOVA, LSD past hoc test) ne pokazuju značajne razlike u stepenu konverzije različitih preparata kompozitnih cemenata. Nasuprot tome, rezultati HPLC analize beleže značajne razlike u količini i vrsti monomernih supstanci otpuštenih iz kompozitnih cemenata. Takođe, statistička analiza u okviru ove studije nije pokazala korelaciju stepena konverzije ispitivanih kompozitnih dentalnih cemenata i količine oslobođenih supstanci iz ovih materijala.
Кључне речи:
dental resin-based cement / degree of conversion / eluted monomerИзвор:
Journal of the Serbian Chemical Society, 2011, 76, 9, 1307-1323Издавач:
- Srpsko hemijsko društvo, Beograd
DOI: 10.2298/JSC100610113O
ISSN: 0352-5139
WoS: 000295659800011
Scopus: 2-s2.0-80053104556
Институција/група
Tehnološko-metalurški fakultetTY - JOUR AU - Obradović-Đuričić, Kosovka AU - Medić, Vesna AU - Radišić, Marina AU - Laušević, Mila PY - 2011 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5633 AB - This study examined the possible correlation between the degree of conversion (DC) and the amount of substances eluted from three commercial cured resin-based cements. The DC of the various resin-based cements was measured by Raman spectroscopy, while the quantity of unreacted monomers released from the cement matrix (triethylene glycol dimethacrylate, TEGDMA, urethane dimethacrylate, UDMA, 2-hydroxyethyl methacrylate, HEMA and bisphenol A) was determined by high pressure liquid chromatography (HPLC). The obtained results, after multiple statistical evaluation (one way ANOVA, LSD post hoc test), showed no significant differences in the DC values between the resin cements. On the contrary, the results of the HPLC analysis depicted statistically significant differences between the three materials with respect to the amount of leached monomers. In addition, no correlation between the DC and the amount of eluted substances from the tested cured composite cements was found. AB - Rad istražuje moguću korelaciju stepena konverzije (DC) i količine oslobođenih monomernih supstanci iz tri komercijalna preparata kompozitnih dentalnih cemenata. Stepen konverzije kompozitnih cemenata određen je metodom Raman spektroskopije, dok je količina neizreagovalih i oslobođenih monomera iz cementnog matriksa detektovana pomoću HPLC metode. Rezultati dobijeni nakon višestruke statističke evaluacije (one way ANOVA, LSD past hoc test) ne pokazuju značajne razlike u stepenu konverzije različitih preparata kompozitnih cemenata. Nasuprot tome, rezultati HPLC analize beleže značajne razlike u količini i vrsti monomernih supstanci otpuštenih iz kompozitnih cemenata. Takođe, statistička analiza u okviru ove studije nije pokazala korelaciju stepena konverzije ispitivanih kompozitnih dentalnih cemenata i količine oslobođenih supstanci iz ovih materijala. PB - Srpsko hemijsko društvo, Beograd T2 - Journal of the Serbian Chemical Society T1 - Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements T1 - Korelacija stepena konverzije i količine oslobođenih supstanci iz dentalnih kompozitnih cemenata EP - 1323 IS - 9 SP - 1307 VL - 76 DO - 10.2298/JSC100610113O ER -
@article{ author = "Obradović-Đuričić, Kosovka and Medić, Vesna and Radišić, Marina and Laušević, Mila", year = "2011", abstract = "This study examined the possible correlation between the degree of conversion (DC) and the amount of substances eluted from three commercial cured resin-based cements. The DC of the various resin-based cements was measured by Raman spectroscopy, while the quantity of unreacted monomers released from the cement matrix (triethylene glycol dimethacrylate, TEGDMA, urethane dimethacrylate, UDMA, 2-hydroxyethyl methacrylate, HEMA and bisphenol A) was determined by high pressure liquid chromatography (HPLC). The obtained results, after multiple statistical evaluation (one way ANOVA, LSD post hoc test), showed no significant differences in the DC values between the resin cements. On the contrary, the results of the HPLC analysis depicted statistically significant differences between the three materials with respect to the amount of leached monomers. In addition, no correlation between the DC and the amount of eluted substances from the tested cured composite cements was found., Rad istražuje moguću korelaciju stepena konverzije (DC) i količine oslobođenih monomernih supstanci iz tri komercijalna preparata kompozitnih dentalnih cemenata. Stepen konverzije kompozitnih cemenata određen je metodom Raman spektroskopije, dok je količina neizreagovalih i oslobođenih monomera iz cementnog matriksa detektovana pomoću HPLC metode. Rezultati dobijeni nakon višestruke statističke evaluacije (one way ANOVA, LSD past hoc test) ne pokazuju značajne razlike u stepenu konverzije različitih preparata kompozitnih cemenata. Nasuprot tome, rezultati HPLC analize beleže značajne razlike u količini i vrsti monomernih supstanci otpuštenih iz kompozitnih cemenata. Takođe, statistička analiza u okviru ove studije nije pokazala korelaciju stepena konverzije ispitivanih kompozitnih dentalnih cemenata i količine oslobođenih supstanci iz ovih materijala.", publisher = "Srpsko hemijsko društvo, Beograd", journal = "Journal of the Serbian Chemical Society", title = "Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements, Korelacija stepena konverzije i količine oslobođenih supstanci iz dentalnih kompozitnih cemenata", pages = "1323-1307", number = "9", volume = "76", doi = "10.2298/JSC100610113O" }
Obradović-Đuričić, K., Medić, V., Radišić, M.,& Laušević, M.. (2011). Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements. in Journal of the Serbian Chemical Society Srpsko hemijsko društvo, Beograd., 76(9), 1307-1323. https://doi.org/10.2298/JSC100610113O
Obradović-Đuričić K, Medić V, Radišić M, Laušević M. Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements. in Journal of the Serbian Chemical Society. 2011;76(9):1307-1323. doi:10.2298/JSC100610113O .
Obradović-Đuričić, Kosovka, Medić, Vesna, Radišić, Marina, Laušević, Mila, "Correlation between the degree of conversion and the elution of leachable components from dental resin-based cements" in Journal of the Serbian Chemical Society, 76, no. 9 (2011):1307-1323, https://doi.org/10.2298/JSC100610113O . .