In this work, Zn(CH3 COO)(2) 2 H-2 O with AgNO3 content from 0 to 6 mol% was solvothermally treated at 120 C for 18 h in the presence of poly(vinyl pyrrolidone), ethylene glycol and sodium hydroxide. The structural , microstructural and photocatalytic properties of the unmodified and Ag modified ZnO powders have been investigated by the XRPD, FESEM, TEM, UV-vis, Raman and BET techniques. The Ag modified samples consist of ZnO nanocrystals and metallic Ag on the surface. The average crystallite size of all samples was about 20 nm. The FESEM revealed the uniformity in size and approximately spherical shape of ZnO nanopar-ticles. The BET data suggest that all prepared samples are mesoporous. All prepared samples showed higher photocatalytic efficiency in the degradation of the Reactive Orange 16 (RO16) azo dye than the commercial ZnO. In addition, Ag modified ZnO powders, especially those with 1.5 and 0.75 mol% of Ag, were more efficient than the unmodified one.
TY - JOUR
AU - Simović, Bojana
AU - Poleti, Dejan
AU - Golubović, Aleksandar
AU - Matković, Aleksandar
AU - Šćepanović, Maja
AU - Babić, Biljana M.
AU - Branković, Goran
PY - 2017
UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5817
AB - In this work, Zn(CH3 COO)(2) 2 H-2 O with AgNO3 content from 0 to 6 mol% was solvothermally treated at 120 C for 18 h in the presence of poly(vinyl pyrrolidone), ethylene glycol and sodium hydroxide. The structural , microstructural and photocatalytic properties of the unmodified and Ag modified ZnO powders have been investigated by the XRPD, FESEM, TEM, UV-vis, Raman and BET techniques. The Ag modified samples consist of ZnO nanocrystals and metallic Ag on the surface. The average crystallite size of all samples was about 20 nm. The FESEM revealed the uniformity in size and approximately spherical shape of ZnO nanopar-ticles. The BET data suggest that all prepared samples are mesoporous. All prepared samples showed higher photocatalytic efficiency in the degradation of the Reactive Orange 16 (RO16) azo dye than the commercial ZnO. In addition, Ag modified ZnO powders, especially those with 1.5 and 0.75 mol% of Ag, were more efficient than the unmodified one.
PB - Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
T2 - Processing and Application of Ceramics
T1 - Enhanced photocatalytic degradation of RO16 dye using Ag modified ZnO nanopowders prepared by the solvothermal method
EP - 38
IS - 1
SP - 27
VL - 11
DO - 10.2298/PAC1701027S
ER -
@article{
author = "Simović, Bojana and Poleti, Dejan and Golubović, Aleksandar and Matković, Aleksandar and Šćepanović, Maja and Babić, Biljana M. and Branković, Goran",
year = "2017",
abstract = "In this work, Zn(CH3 COO)(2) 2 H-2 O with AgNO3 content from 0 to 6 mol% was solvothermally treated at 120 C for 18 h in the presence of poly(vinyl pyrrolidone), ethylene glycol and sodium hydroxide. The structural , microstructural and photocatalytic properties of the unmodified and Ag modified ZnO powders have been investigated by the XRPD, FESEM, TEM, UV-vis, Raman and BET techniques. The Ag modified samples consist of ZnO nanocrystals and metallic Ag on the surface. The average crystallite size of all samples was about 20 nm. The FESEM revealed the uniformity in size and approximately spherical shape of ZnO nanopar-ticles. The BET data suggest that all prepared samples are mesoporous. All prepared samples showed higher photocatalytic efficiency in the degradation of the Reactive Orange 16 (RO16) azo dye than the commercial ZnO. In addition, Ag modified ZnO powders, especially those with 1.5 and 0.75 mol% of Ag, were more efficient than the unmodified one.",
publisher = "Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad",
journal = "Processing and Application of Ceramics",
title = "Enhanced photocatalytic degradation of RO16 dye using Ag modified ZnO nanopowders prepared by the solvothermal method",
pages = "38-27",
number = "1",
volume = "11",
doi = "10.2298/PAC1701027S"
}
Simović, B., Poleti, D., Golubović, A., Matković, A., Šćepanović, M., Babić, B. M.,& Branković, G.. (2017). Enhanced photocatalytic degradation of RO16 dye using Ag modified ZnO nanopowders prepared by the solvothermal method. in Processing and Application of Ceramics
Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad., 11(1), 27-38.
https://doi.org/10.2298/PAC1701027S
Simović B, Poleti D, Golubović A, Matković A, Šćepanović M, Babić BM, Branković G. Enhanced photocatalytic degradation of RO16 dye using Ag modified ZnO nanopowders prepared by the solvothermal method. in Processing and Application of Ceramics. 2017;11(1):27-38.
doi:10.2298/PAC1701027S .
Simović, Bojana, Poleti, Dejan, Golubović, Aleksandar, Matković, Aleksandar, Šćepanović, Maja, Babić, Biljana M., Branković, Goran, "Enhanced photocatalytic degradation of RO16 dye using Ag modified ZnO nanopowders prepared by the solvothermal method" in Processing and Application of Ceramics, 11, no. 1 (2017):27-38,
https://doi.org/10.2298/PAC1701027S . .
