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Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect

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2016
1820-61311603169P.pdf (2.280Mb)
Authors
Prekajski, Marija D.
Jokić, Bojan M.
Kalijadis, Ana
Maletaškić, Jelena
Stanković, Nadežda
Luković, Jelena M.
Matović, Branko
Article (Published version)
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Abstract
Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.
Keywords:
apatite / nanoparticles / nanoemulsion / Raman spectroscopy / X-ray diffraction
Source:
Processing and Application of Ceramics, 2016, 10, 3, 169-174
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)

DOI: 10.2298/PAC1603169P

ISSN: 1820-6131; 2406-1034

WoS: 000389218100006

Scopus: 2-s2.0-84990240377
[ Google Scholar ]
13
8
URI
http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5842
Collections
  • Radovi istraživača / Researchers’ publications (TMF)
Institution/Community
Tehnološko-metalurški fakultet
TY  - JOUR
AU  - Prekajski, Marija D.
AU  - Jokić, Bojan M.
AU  - Kalijadis, Ana
AU  - Maletaškić, Jelena
AU  - Stanković, Nadežda
AU  - Luković, Jelena M.
AU  - Matović, Branko
PY  - 2016
UR  - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5842
AB  - Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.
T2  - Processing and Application of Ceramics
T1  - Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect
EP  - 174
IS  - 3
SP  - 169
VL  - 10
DO  - 10.2298/PAC1603169P
ER  - 
@article{
author = "Prekajski, Marija D. and Jokić, Bojan M. and Kalijadis, Ana and Maletaškić, Jelena and Stanković, Nadežda and Luković, Jelena M. and Matović, Branko",
year = "2016",
abstract = "Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.",
journal = "Processing and Application of Ceramics",
title = "Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect",
pages = "174-169",
number = "3",
volume = "10",
doi = "10.2298/PAC1603169P"
}
Prekajski, M. D., Jokić, B. M., Kalijadis, A., Maletaškić, J., Stanković, N., Luković, J. M.,& Matović, B.. (2016). Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect. in Processing and Application of Ceramics, 10(3), 169-174.
https://doi.org/10.2298/PAC1603169P
Prekajski MD, Jokić BM, Kalijadis A, Maletaškić J, Stanković N, Luković JM, Matović B. Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect. in Processing and Application of Ceramics. 2016;10(3):169-174.
doi:10.2298/PAC1603169P .
Prekajski, Marija D., Jokić, Bojan M., Kalijadis, Ana, Maletaškić, Jelena, Stanković, Nadežda, Luković, Jelena M., Matović, Branko, "Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect" in Processing and Application of Ceramics, 10, no. 3 (2016):169-174,
https://doi.org/10.2298/PAC1603169P . .

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