Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect
Authors
Prekajski, Marija D.Jokić, Bojan M.
Kalijadis, Ana

Maletaškić, Jelena
Stanković, Nadežda

Luković, Jelena M.

Matović, Branko

Article (Published version)
Metadata
Show full item recordAbstract
Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.
Keywords:
apatite / nanoparticles / nanoemulsion / Raman spectroscopy / X-ray diffractionSource:
Processing and Application of Ceramics, 2016, 10, 3, 169-174Funding / projects:
DOI: 10.2298/PAC1603169P
ISSN: 1820-6131; 2406-1034
WoS: 000389218100006
Scopus: 2-s2.0-84990240377
Institution/Community
Tehnološko-metalurški fakultetTY - JOUR AU - Prekajski, Marija D. AU - Jokić, Bojan M. AU - Kalijadis, Ana AU - Maletaškić, Jelena AU - Stanković, Nadežda AU - Luković, Jelena M. AU - Matović, Branko PY - 2016 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5842 AB - Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres. T2 - Processing and Application of Ceramics T1 - Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect EP - 174 IS - 3 SP - 169 VL - 10 DO - 10.2298/PAC1603169P ER -
@article{ author = "Prekajski, Marija D. and Jokić, Bojan M. and Kalijadis, Ana and Maletaškić, Jelena and Stanković, Nadežda and Luković, Jelena M. and Matović, Branko", year = "2016", abstract = "Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 degrees C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.", journal = "Processing and Application of Ceramics", title = "Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect", pages = "174-169", number = "3", volume = "10", doi = "10.2298/PAC1603169P" }
Prekajski, M. D., Jokić, B. M., Kalijadis, A., Maletaškić, J., Stanković, N., Luković, J. M.,& Matović, B.. (2016). Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect. in Processing and Application of Ceramics, 10(3), 169-174. https://doi.org/10.2298/PAC1603169P
Prekajski MD, Jokić BM, Kalijadis A, Maletaškić J, Stanković N, Luković JM, Matović B. Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect. in Processing and Application of Ceramics. 2016;10(3):169-174. doi:10.2298/PAC1603169P .
Prekajski, Marija D., Jokić, Bojan M., Kalijadis, Ana, Maletaškić, Jelena, Stanković, Nadežda, Luković, Jelena M., Matović, Branko, "Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect" in Processing and Application of Ceramics, 10, no. 3 (2016):169-174, https://doi.org/10.2298/PAC1603169P . .