Boron-doped carbons were produced using hydrothermal carbonization of
glucose carbohydrates under mild temperature (180oC). Boric acid was
introduced into glucose precursor solution in order to obtained boron
concentration of 0.2% and 1%. Two types of samples were prepared:
hydrothermal carbons (HTC) and hydrothermal carbons thermally treated to
1000oC (HTCc). Characterization of the samples obtained was performed by
scanning electron microscopy (SEM) and Fourier Transform Infrared
Spectroscopy (FTIR). SEM analysis showed that higher boron concentration
in the precursor solution caused enlargement of particle size for both type of
samples, while the thermal treatment induced decrease of particle size. FTIR
spectra showed that the different amount of boron in the precursor solution
induced quite diverse effects on the surface chemistry of hydrothermal
carbons before and after the thermal treatment.
Source:
12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings, 2014, 1, 679-682
TY - CONF
AU - Kalijadis, Ana
AU - Vukčević, Marija
AU - Maletić, Marina
AU - Laušević, Mila
AU - Laušević, Zoran
PY - 2014
UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6301
AB - Boron-doped carbons were produced using hydrothermal carbonization of
glucose carbohydrates under mild temperature (180oC). Boric acid was
introduced into glucose precursor solution in order to obtained boron
concentration of 0.2% and 1%. Two types of samples were prepared:
hydrothermal carbons (HTC) and hydrothermal carbons thermally treated to
1000oC (HTCc). Characterization of the samples obtained was performed by
scanning electron microscopy (SEM) and Fourier Transform Infrared
Spectroscopy (FTIR). SEM analysis showed that higher boron concentration
in the precursor solution caused enlargement of particle size for both type of
samples, while the thermal treatment induced decrease of particle size. FTIR
spectra showed that the different amount of boron in the precursor solution
induced quite diverse effects on the surface chemistry of hydrothermal
carbons before and after the thermal treatment.
PB - Society of Physical Chemists of Serbia
C3 - 12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings
T1 - Thermal treatment influence on the surface characteristics of the boron-doped hydrothermal carbon
EP - 682
SP - 679
VL - 1
UR - https://hdl.handle.net/21.15107/rcub_technorep_6301
ER -
@conference{
author = "Kalijadis, Ana and Vukčević, Marija and Maletić, Marina and Laušević, Mila and Laušević, Zoran",
year = "2014",
abstract = "Boron-doped carbons were produced using hydrothermal carbonization of
glucose carbohydrates under mild temperature (180oC). Boric acid was
introduced into glucose precursor solution in order to obtained boron
concentration of 0.2% and 1%. Two types of samples were prepared:
hydrothermal carbons (HTC) and hydrothermal carbons thermally treated to
1000oC (HTCc). Characterization of the samples obtained was performed by
scanning electron microscopy (SEM) and Fourier Transform Infrared
Spectroscopy (FTIR). SEM analysis showed that higher boron concentration
in the precursor solution caused enlargement of particle size for both type of
samples, while the thermal treatment induced decrease of particle size. FTIR
spectra showed that the different amount of boron in the precursor solution
induced quite diverse effects on the surface chemistry of hydrothermal
carbons before and after the thermal treatment.",
publisher = "Society of Physical Chemists of Serbia",
journal = "12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings",
title = "Thermal treatment influence on the surface characteristics of the boron-doped hydrothermal carbon",
pages = "682-679",
volume = "1",
url = "https://hdl.handle.net/21.15107/rcub_technorep_6301"
}
Kalijadis, A., Vukčević, M., Maletić, M., Laušević, M.,& Laušević, Z.. (2014). Thermal treatment influence on the surface characteristics of the boron-doped hydrothermal carbon. in 12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings
Society of Physical Chemists of Serbia., 1, 679-682.
https://hdl.handle.net/21.15107/rcub_technorep_6301
Kalijadis A, Vukčević M, Maletić M, Laušević M, Laušević Z. Thermal treatment influence on the surface characteristics of the boron-doped hydrothermal carbon. in 12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings. 2014;1:679-682.
https://hdl.handle.net/21.15107/rcub_technorep_6301 .
Kalijadis, Ana, Vukčević, Marija, Maletić, Marina, Laušević, Mila, Laušević, Zoran, "Thermal treatment influence on the surface characteristics of the boron-doped hydrothermal carbon" in 12th International Conference on Fundamental and Applied Aspects of Physical Chemistry, Proceedings, 1 (2014):679-682,
https://hdl.handle.net/21.15107/rcub_technorep_6301 .
