The synthesis of 2-mercaptoethyl methacrylate from methacrylic acid and 2-mercaptoethanol by etherification using acetyl chloride as catalyst was optimized. The purity of the obtained product was controlled by gas chromatography and its identity confirmed by H-NMR and FTIR spectroscopy. 2-Mercapto-ethyl methacrylate could find application as a chain transfer agent in radical polymerizations.
Sinteza 2-merkaptoetil metakrilata esterifikacijom metakrilne kiseline 2-merkaptoetanolom je optimizovana. Čistoća dobijenog proizvoda je kontrolisana gasnom hromatografijom i potvrđena 1H-NMR i FTIR spektroskopijom. 2-Merkaptoetil metakrilat može da se primeni kao sredstvo za prenošenje aktivnosti lanca u radikalnim polimerizacijama.
Keywords:
2-mercaptoethyl methacrylate / chain transfer agent / synthesis / characterization / 2-merkaptoetil metakrilat / sredstvo za prenošenje aktivnosti lanca / sinteza / karakterizacija
TY - JOUR
AU - Knežević, Marija
AU - Katsikas, Lynne
AU - Popović, Ivanka
PY - 2005
UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/761
AB - The synthesis of 2-mercaptoethyl methacrylate from methacrylic acid and 2-mercaptoethanol by etherification using acetyl chloride as catalyst was optimized. The purity of the obtained product was controlled by gas chromatography and its identity confirmed by H-NMR and FTIR spectroscopy. 2-Mercapto-ethyl methacrylate could find application as a chain transfer agent in radical polymerizations.
AB - Sinteza 2-merkaptoetil metakrilata esterifikacijom metakrilne kiseline 2-merkaptoetanolom je optimizovana. Čistoća dobijenog proizvoda je kontrolisana gasnom hromatografijom i potvrđena 1H-NMR i FTIR spektroskopijom. 2-Merkaptoetil metakrilat može da se primeni kao sredstvo za prenošenje aktivnosti lanca u radikalnim polimerizacijama.
PB - Association of Chemical Engineers of Serbia
T2 - Hemijska industrija
T1 - The synthesis and characterization of 2-mercaptoethyl methacrylate
T1 - Sinteza i karakterizacija 2-merkaptoetil metakrilata
EP - 323
IS - 11-12
SP - 321
VL - 59
DO - 10.2298/HEMIND0512321K
ER -
@article{
author = "Knežević, Marija and Katsikas, Lynne and Popović, Ivanka",
year = "2005",
abstract = "The synthesis of 2-mercaptoethyl methacrylate from methacrylic acid and 2-mercaptoethanol by etherification using acetyl chloride as catalyst was optimized. The purity of the obtained product was controlled by gas chromatography and its identity confirmed by H-NMR and FTIR spectroscopy. 2-Mercapto-ethyl methacrylate could find application as a chain transfer agent in radical polymerizations., Sinteza 2-merkaptoetil metakrilata esterifikacijom metakrilne kiseline 2-merkaptoetanolom je optimizovana. Čistoća dobijenog proizvoda je kontrolisana gasnom hromatografijom i potvrđena 1H-NMR i FTIR spektroskopijom. 2-Merkaptoetil metakrilat može da se primeni kao sredstvo za prenošenje aktivnosti lanca u radikalnim polimerizacijama.",
publisher = "Association of Chemical Engineers of Serbia",
journal = "Hemijska industrija",
title = "The synthesis and characterization of 2-mercaptoethyl methacrylate, Sinteza i karakterizacija 2-merkaptoetil metakrilata",
pages = "323-321",
number = "11-12",
volume = "59",
doi = "10.2298/HEMIND0512321K"
}
Knežević, M., Katsikas, L.,& Popović, I.. (2005). The synthesis and characterization of 2-mercaptoethyl methacrylate. in Hemijska industrija
Association of Chemical Engineers of Serbia., 59(11-12), 321-323.
https://doi.org/10.2298/HEMIND0512321K
Knežević M, Katsikas L, Popović I. The synthesis and characterization of 2-mercaptoethyl methacrylate. in Hemijska industrija. 2005;59(11-12):321-323.
doi:10.2298/HEMIND0512321K .
Knežević, Marija, Katsikas, Lynne, Popović, Ivanka, "The synthesis and characterization of 2-mercaptoethyl methacrylate" in Hemijska industrija, 59, no. 11-12 (2005):321-323,
https://doi.org/10.2298/HEMIND0512321K . .
