Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O
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2011
Authors
Luković Golić, DanijelaBranković, Goran
Počuča-Nešić, Milica
Vojisavljević, Katarina
Recnik, Aleksander
Daneu, Nina
Bernik, Slavko
Šćepanović, Maja
Poleti, Dejan
Branković, Zorica
Article (Published version)
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Show full item recordAbstract
Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals.
Source:
Nanotechnology, 2011, 22, 39Publisher:
- IOP Publishing Ltd, Bristol
Funding / projects:
- Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45007)
- Slovenian Research AgencySlovenian Research Agency - Slovenia [P2-0084-0106]
DOI: 10.1088/0957-4484/22/39/395603
ISSN: 0957-4484
PubMed: 21891855
WoS: 000294723700016
Scopus: 2-s2.0-80052538080
Institution/Community
Tehnološko-metalurški fakultetTY - JOUR AU - Luković Golić, Danijela AU - Branković, Goran AU - Počuča-Nešić, Milica AU - Vojisavljević, Katarina AU - Recnik, Aleksander AU - Daneu, Nina AU - Bernik, Slavko AU - Šćepanović, Maja AU - Poleti, Dejan AU - Branković, Zorica PY - 2011 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/5657 AB - Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals. PB - IOP Publishing Ltd, Bristol T2 - Nanotechnology T1 - Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O IS - 39 VL - 22 DO - 10.1088/0957-4484/22/39/395603 ER -
@article{ author = "Luković Golić, Danijela and Branković, Goran and Počuča-Nešić, Milica and Vojisavljević, Katarina and Recnik, Aleksander and Daneu, Nina and Bernik, Slavko and Šćepanović, Maja and Poleti, Dejan and Branković, Zorica", year = "2011", abstract = "Zinc oxide nanopowders were synthesized by the sol-gel method from an ethanol solution of zinc acetate dihydrate. Detailed structural and microstructural investigations were carried out using x-ray diffraction, Raman spectroscopy, thermogravimetric and differential thermal analyses, as well as high-resolution transmission electron microscopy (TEM) and field-emission scanning electron microscopy. The intermediate compound of the reaction was layered zinc hydroxide acetate that further transforms into hexagonally shaped ZnO crystalline nanoplates (d(m) = 4 nm), which aggregate into larger spherical particles. According to the TEM analysis the ZnO nanoparticles were self-assembled into larger particles with the same orientation, i.e. aligned lattice planes of the particles. A further solvothermal treatment resulted in hexagonal, prismatic ZnO mesocrystals.", publisher = "IOP Publishing Ltd, Bristol", journal = "Nanotechnology", title = "Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O", number = "39", volume = "22", doi = "10.1088/0957-4484/22/39/395603" }
Luković Golić, D., Branković, G., Počuča-Nešić, M., Vojisavljević, K., Recnik, A., Daneu, N., Bernik, S., Šćepanović, M., Poleti, D.,& Branković, Z.. (2011). Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O. in Nanotechnology IOP Publishing Ltd, Bristol., 22(39). https://doi.org/10.1088/0957-4484/22/39/395603
Luković Golić D, Branković G, Počuča-Nešić M, Vojisavljević K, Recnik A, Daneu N, Bernik S, Šćepanović M, Poleti D, Branković Z. Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O. in Nanotechnology. 2011;22(39). doi:10.1088/0957-4484/22/39/395603 .
Luković Golić, Danijela, Branković, Goran, Počuča-Nešić, Milica, Vojisavljević, Katarina, Recnik, Aleksander, Daneu, Nina, Bernik, Slavko, Šćepanović, Maja, Poleti, Dejan, Branković, Zorica, "Structural characterization of self-assembled ZnO nanoparticles obtained by the sol-gel method from Zn(CH3COO)(2)center dot 2H(2)O" in Nanotechnology, 22, no. 39 (2011), https://doi.org/10.1088/0957-4484/22/39/395603 . .