Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
Development of nanomaterials such as transition metal oxides with spinel
structure has been intensively examined because of their applications in catalysis,
energy storage, magnetic data storage and sensors [1]. Synthesis of these materials
has been realized by various approaches, such as hydrothermal synthesis, solid state
reactions and microwave synthesis [1]. In previous years, thermolysis of transition
metal complexes as precursors provides a new technique in preparing useful
nanomaterials due to the possibility to control their particle size and morphology [2].
The nano- and microparticles of Co3O4 have been prepared by direct calcination
of ternary Co(II) complex, [Co3(bipym)3(H3mell)2]·18H2O, where bipym is
2,2’-bipyrimidine and H3mell3–
is anion of 1,2,3,4,5,6-benzenehexacarboxylic
(mellitic) acid at 450 and 1000 °C in air atmosphere. The powder X-ray diffraction
(XRDP) and scanning electron microscopy (SEM) were used to investigate structure
and morphology of the ...obtained materials. The results indicated the formation of
pure Co3O4 phase, whose particles size depends on the calcination temperature.
Извор:
Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, 2019, 92-Издавач:
- Belgrade : Institute for Multidisciplinary Research, University
Финансирање / пројекти:
- 0-3D наноструктуре за примену у електроници и обновљивим изворима енергије: синтеза, карактеризација и процесирање (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45007)
Колекције
Институција/група
Inovacioni centarTY - CONF AU - Radovanović, Lidija AU - Vulić, Predrag AU - Radovanović, Željko AU - Rogan, Jelena PY - 2019 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6721 AB - Development of nanomaterials such as transition metal oxides with spinel structure has been intensively examined because of their applications in catalysis, energy storage, magnetic data storage and sensors [1]. Synthesis of these materials has been realized by various approaches, such as hydrothermal synthesis, solid state reactions and microwave synthesis [1]. In previous years, thermolysis of transition metal complexes as precursors provides a new technique in preparing useful nanomaterials due to the possibility to control their particle size and morphology [2]. The nano- and microparticles of Co3O4 have been prepared by direct calcination of ternary Co(II) complex, [Co3(bipym)3(H3mell)2]·18H2O, where bipym is 2,2’-bipyrimidine and H3mell3– is anion of 1,2,3,4,5,6-benzenehexacarboxylic (mellitic) acid at 450 and 1000 °C in air atmosphere. The powder X-ray diffraction (XRDP) and scanning electron microscopy (SEM) were used to investigate structure and morphology of the obtained materials. The results indicated the formation of pure Co3O4 phase, whose particles size depends on the calcination temperature. PB - Belgrade : Institute for Multidisciplinary Research, University C3 - Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia T1 - Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex SP - 92 UR - https://hdl.handle.net/21.15107/rcub_technorep_6721 ER -
@conference{ author = "Radovanović, Lidija and Vulić, Predrag and Radovanović, Željko and Rogan, Jelena", year = "2019", abstract = "Development of nanomaterials such as transition metal oxides with spinel structure has been intensively examined because of their applications in catalysis, energy storage, magnetic data storage and sensors [1]. Synthesis of these materials has been realized by various approaches, such as hydrothermal synthesis, solid state reactions and microwave synthesis [1]. In previous years, thermolysis of transition metal complexes as precursors provides a new technique in preparing useful nanomaterials due to the possibility to control their particle size and morphology [2]. The nano- and microparticles of Co3O4 have been prepared by direct calcination of ternary Co(II) complex, [Co3(bipym)3(H3mell)2]·18H2O, where bipym is 2,2’-bipyrimidine and H3mell3– is anion of 1,2,3,4,5,6-benzenehexacarboxylic (mellitic) acid at 450 and 1000 °C in air atmosphere. The powder X-ray diffraction (XRDP) and scanning electron microscopy (SEM) were used to investigate structure and morphology of the obtained materials. The results indicated the formation of pure Co3O4 phase, whose particles size depends on the calcination temperature.", publisher = "Belgrade : Institute for Multidisciplinary Research, University", journal = "Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia", title = "Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex", pages = "92", url = "https://hdl.handle.net/21.15107/rcub_technorep_6721" }
Radovanović, L., Vulić, P., Radovanović, Ž.,& Rogan, J.. (2019). Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia Belgrade : Institute for Multidisciplinary Research, University., 92. https://hdl.handle.net/21.15107/rcub_technorep_6721
Radovanović L, Vulić P, Radovanović Ž, Rogan J. Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex. in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia. 2019;:92. https://hdl.handle.net/21.15107/rcub_technorep_6721 .
Radovanović, Lidija, Vulić, Predrag, Radovanović, Željko, Rogan, Jelena, "Preparation Co3O4 nano- and microparticles by solid state thermolysis of cobalt(II) complex" in Programme and the Book of Abstracts / 5th Conference of The Serbian Society for Ceramic Materials, 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia (2019):92, https://hdl.handle.net/21.15107/rcub_technorep_6721 .