Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites
Само за регистроване кориснике
2019
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
The novel global trends for waste materials processing and recycling, as well as new
European standards for sampling and testing of these materials, require better performances of
analytical methods for the chemical analysis and improvements regarding their matrices. In this
study, a new method for optical emission spectrometry with inductively coupled plasma (ICP-OES)
has been developed and subsequently validated for determination of 35 elements comprised in
leachates of fly ash and composites based on fly ash, i.e. cement pastes and mortars. Validation
performances and the uncertainty measurement were determined and calculated via three different
routes: validation method, participation in proficiency testing schemes and standard method. It is
proved that this method is acceptable for the determination of all 35 elements in this matrix. The
obtained results highlight a new simple and effective analyzing route for quantity determination of
undesired trace elements in fluids ...upon conducted leaching test.
Кључне речи:
analytical procedures / waste materials / industrial byproducts / leaching test / environmental safetyИзвор:
Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019, 2019, 70-76Издавач:
- Bor : University of Belgrade, Technical Faculty
Финансирање / пројекти:
- Развој и примена мултифункционалних материјала на бази домаћих сировина модернизацијом традиционалних технологија (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45008)
Институција/група
Tehnološko-metalurški fakultetTY - CONF AU - Mijatović, Nevenka AU - Terzić, Anja AU - Miličić, Ljiljana AU - Živojinović, Dragana PY - 2019 UR - http://TechnoRep.tmf.bg.ac.rs/handle/123456789/7313 AB - The novel global trends for waste materials processing and recycling, as well as new European standards for sampling and testing of these materials, require better performances of analytical methods for the chemical analysis and improvements regarding their matrices. In this study, a new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) has been developed and subsequently validated for determination of 35 elements comprised in leachates of fly ash and composites based on fly ash, i.e. cement pastes and mortars. Validation performances and the uncertainty measurement were determined and calculated via three different routes: validation method, participation in proficiency testing schemes and standard method. It is proved that this method is acceptable for the determination of all 35 elements in this matrix. The obtained results highlight a new simple and effective analyzing route for quantity determination of undesired trace elements in fluids upon conducted leaching test. PB - Bor : University of Belgrade, Technical Faculty C3 - Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019 T1 - Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites EP - 76 SP - 70 UR - https://hdl.handle.net/21.15107/rcub_technorep_7313 ER -
@conference{ author = "Mijatović, Nevenka and Terzić, Anja and Miličić, Ljiljana and Živojinović, Dragana", year = "2019", abstract = "The novel global trends for waste materials processing and recycling, as well as new European standards for sampling and testing of these materials, require better performances of analytical methods for the chemical analysis and improvements regarding their matrices. In this study, a new method for optical emission spectrometry with inductively coupled plasma (ICP-OES) has been developed and subsequently validated for determination of 35 elements comprised in leachates of fly ash and composites based on fly ash, i.e. cement pastes and mortars. Validation performances and the uncertainty measurement were determined and calculated via three different routes: validation method, participation in proficiency testing schemes and standard method. It is proved that this method is acceptable for the determination of all 35 elements in this matrix. The obtained results highlight a new simple and effective analyzing route for quantity determination of undesired trace elements in fluids upon conducted leaching test.", publisher = "Bor : University of Belgrade, Technical Faculty", journal = "Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019", title = "Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites", pages = "76-70", url = "https://hdl.handle.net/21.15107/rcub_technorep_7313" }
Mijatović, N., Terzić, A., Miličić, L.,& Živojinović, D.. (2019). Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites. in Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019 Bor : University of Belgrade, Technical Faculty., 70-76. https://hdl.handle.net/21.15107/rcub_technorep_7313
Mijatović N, Terzić A, Miličić L, Živojinović D. Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites. in Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019. 2019;:70-76. https://hdl.handle.net/21.15107/rcub_technorep_7313 .
Mijatović, Nevenka, Terzić, Anja, Miličić, Ljiljana, Živojinović, Dragana, "Validation of ICP–OES procedure for major and trace elements determination in the leachates of fly ash and fly ash based composites" in Proceedings / XIII International Mineral Processing and Recycling Conference, MPRC, Belgrade, Serbia, 8-10 May 2019 (2019):70-76, https://hdl.handle.net/21.15107/rcub_technorep_7313 .