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Ultra-high pressure densification and properties of nanostructured SiC
(Elsevier Science Bv, Amsterdam, 2016)
Cubic SiC nano-powder particles were synthesized by a sal-gel process with an average grains size of 9.5 nm which were subsequently densified by using a high-pressure "anvil-type with hollows" apparatus at a pressure of 4 ...
Prediction of bed expansion of polydisperse quartz sand mixtures fluidized with water
(Elsevier Science Bv, Amsterdam, 2016)
In this paper, the minimum fluidization velocity and bed expansion of polydisperse sand mixtures fluidized with water were investigated. The fluidization experiments were carried out using 19 different fractions of quartz ...
Supercritical carbon dioxide extraction of Trigonella foenum-graecum L. seeds: Process optimization using response surface methodology
(Elsevier Science Bv, Amsterdam, 2016)
Pretreatment of fenugreek (Trigonella foenum-graecum L, Fabaceae) seeds was achieved using the step of defatting and acid hydrolysis. The obtained hydro-isolate (HI) was used as initial feed for diosgenin isolation by ...
A method for reactor synthesis based on process intensification principles and optimization of superstructure consisting of phenomenological modules
(Inst Chemical Engineers, Rugby, 2016)
A novel method for reaction synthesis is proposed. The method establishes strong interconnection between process intensification (PI) principles and process system engineering (PSE) techniques, which are used for problem ...
Influence of a Low Content of PEO Segment on the Thermal, Surface and Morphological Properties of Triblock and Diblock PCL Copolymers
(Springer, Dordrecht, 2016)
Two series, one of triblock (PCL/PEO/PCL) and the other of diblock (PCL/PEO) copolymers were prepared by ring-opening polymerization of epsilon-caprolactone catalized with tin(II) octoate and by using dihydroxy or monohydroxy ...
Polypyrrole-based Enzyme Electrode with Immobilized Glucose Oxidase for Electrochemical Determination of Glucose
(Electrochemical Science Group, Beograd, 2016)
Polypyrrole enzyme electrode was formed by immobilization of glucose oxidase via glutaraldehyde into electrochemically synthesized polypyrrole on glassy carbon electrode. Electrochemical synthesis was performed in 0.5 mol ...
Co(III) complex with (E)-2-(2-(pyridine-2-ylmethylene)hydrazinyl)-4-(4-tolyl)-1,3-thiazole: structure and activity against 2-D and 3-D cancer cell models
(Taylor & Francis Ltd, Abingdon, 2016)
Co(III) complex with a 2-hydrazonylthiazole ligand was synthesized and characterized by single-crystal X-ray diffraction. In the inner sphere of the complex, two monoionic ligands are coordinated tridentately forming ...
Improvement of the epoxy coating properties by incorporation of polyaniline surface treated TiO2 nanoparticles previously modified with vitamin B6
(Elsevier Science Sa, Lausanne, 2016)
Novel TiO2-PANI core-shell nanocomposite, prepared by in situ oxidative polymerization of aniline in the presence of TiO2 nanoparticles surface modified with vitamin B6, was used to reinforce epoxy resin. The size of ...
Photocatalytic Ability of Visible-Light-Responsive TiO2 Nanoparticles
(Amer Chemical Soc, Washington, 2016)
The synthetic procedures for preparation of free-standing and attached to polymer support surface modified TiO2 nanoparticles (NPs) with absorption extended into the visible spectral region due to charge transfer complex ...
Solvatochromism of Thiouracil Azo Dyes
(Springer/Plenum Publishers, New York, 2016)
A series of sixteen synthesized thiouracil azo dyes was obtained by condensation of arylazo acetoacetic esters with thiourea. Purified products were characterized by UV-Vis, FT-IR, H-1 and C-13 NMR spectroscopy. The UV-Vis ...