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PZT ceramics obtained from mechanochemically synthesized powders
(Kluwer Academic Publ, Dordrecht, 2003)
PZT ceramics were obtained from the mechanochemically synthesized powders. Milling and sintering conditions were optimized based on results of density measurements, as well as on microstructural and electrical characterization. ...
Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agent
(Pergamon-Elsevier Science Ltd, Oxford, 2003)
Colorless plate-like crystals (AIPO-1,2DAP) crystallize from a clear 'AlPO4-1,2-diaminopropane' reaction system. The results of elemental, thermal and FTIR analyses give the following chemical formula: (NH4+)(1,2-H(2)DAP ...
New inorganic-organic hybrid: Synthesis and structural characterization of an alumino(oxalato)phosphate
(Amer Chemical Soc, Washington, 2003)
A new 3-D alumino(oxalato)phosphate, [H3NCH(CH3)CH2NH3](2)[Al4P6O20(OH)(4)(C2O4)(H2O)], consists of aluminophosphate layers which are pillared by oxalate anions. It contains a hybrid 12-membered channel where guest species, ...
The effect of segment length on some properties of thermoplastic poly(ester-siloxane)s
(John Wiley and Sons Ltd, 2003)
A series of novel thermoplastic elastomers, based on poly(dimethylsiloxane) (PDMS) as the soft segment and poly(butylene terephthalate) (PBT) as the hard segment, were synthesized by catalyzed two-step, melt transesterification ...
Adsorption of oxygen containing species and their effect on oxygen reduction on Pt3Co electrode
(Elsevier Science Sa, Lausanne, 2003)
A rotating Pt3Co, thermally prepared alloy disc is used to study electrochemical oxygen reduction in alkaline solutions of different pH. In all solutions two Tafel regions are found: at low current densities partial ...
Characterization of alumina films electrodeposited on steel from water suspensions
(InterCeram: International Ceramic Review, 2003)
Alumina films were electrodeposited on steel from water suspensions using the constant voltage method. The morphology of deposited films was investigated using optical microscopy coupled with image analysis which enabled ...
Synthesis of nanostructured boehmite powder by sol-gel method from industrial Na-aluminate solution
(Techna Srl, Faenza, 2003)
Supersaturated Na-aluminate solution from KAP's Alumina plant Bayer process was chosen, as a precursor to synthesize low sodium content nanostructured boehmite powder. Firstly, the solution, was neutralized with strong ...
Solid-state NMR study of an open-framework aluminophosphate-oxalate hybrid
(Amer Chemical Soc, Washington, 2003)
Short-range order within a novel aluminophosphate-oxalate hybrid material with the unit cell formula CH2(NH3)CH(NH3)CH3Al4P6O20(OH)(4)(C2O4)H2O was studied by multinuclear solid-state NMR measurements. The C-13, Al-27, and ...
Recycled wool-based nonwoven material as an oil sorbent
(Amer Chemical Soc, Washington, 2003)
The aim of this study was to highlight the possibility of using recycled wool-based nonwoven material as a sorbent in an oil spill cleanup. This material sorbed higher amounts of base oil SN 150 than diesel or crude oil ...
Influence of the mobile-phase modifier on the retention of some para-substituted amides; Correlation with compound lipophilicity
(Springer Heidelberg, Heidelberg, 2003)
The chromatographic behavior of Para-substituted amides of alpha-phenylacetic, benzoic, propanoic, and 2,2-dimethylpropanoic acid has been studied in reversed-phase thin-layer chromatography on silica gel impregnated with ...