Prikaz osnovnih podataka o dokumentu
Determination of carbendazim residues in fruit juices by liquid chromatography-tandem mass spectrometry
dc.creator | Grujić, Svetlana | |
dc.creator | Radišić, Marina | |
dc.creator | Vasiljević, Tatjana | |
dc.creator | Laušević, Mila | |
dc.date.accessioned | 2023-03-14T09:42:39Z | |
dc.date.available | 2023-03-14T09:42:39Z | |
dc.date.issued | 2005 | |
dc.identifier.issn | 0265–203X | |
dc.identifier.uri | http://TechnoRep.tmf.bg.ac.rs/handle/123456789/6052 | |
dc.description.abstract | In this paper a rapid optimized method for routine analysis of carbendazim residues in fruit juices is reported. The procedure is based on matrix solid-phase dispersion (MSPD) with diatomaceous earth and analysis of the extract by liquid chromatography-tandem mass spectrometry, with electrospray ionization (LC-ESI-MS/MS). In the method optimization, finding of the optimal pH for the extraction of carbendazim from juice was particularly critical. Significant matrix effects were observed, but could be eliminated using matrix-matched standards. High recoveries (82-102%), good repeatability (RSD≤12%) and low limits of detection (0.03 ng ml -1 ) and quantification (0.1 ng ml -1 ) were achieved with this method. | sr |
dc.language.iso | en | sr |
dc.publisher | Taylor & Francis | sr |
dc.rights | closedAccess | sr |
dc.source | Food Additives and Contaminants | sr |
dc.subject | Carbendazim | sr |
dc.subject | Fruit juice | sr |
dc.subject | Ion trap | sr |
dc.subject | LC-MS/MS | sr |
dc.subject | Matrix effect | sr |
dc.subject | MSPD | sr |
dc.title | Determination of carbendazim residues in fruit juices by liquid chromatography-tandem mass spectrometry | sr |
dc.type | article | sr |
dc.rights.license | ARR | sr |
dc.citation.epage | 1137 | |
dc.citation.issue | 11 | |
dc.citation.spage | 1132 | |
dc.citation.volume | 22 | |
dc.identifier.doi | 10.1080/02652030500352863 | |
dc.identifier.scopus | 2-s2.0-31644443943 | |
dc.type.version | publishedVersion | sr |