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Cyclopropyl building blocks in organic synthesis, part 143. A two-step, three-component queuing cascade leading to dihydrobenzoxepine and dihydrobenzazepine derivatives
(Wiley-VCH Verlag Gmbh, Weinheim, 2007)
A palladium-catalyzed reaction of methylenespiropentane (11) with iodobenzene (12) under typical Heck conditions [Pd(OAC)(2), PPh3, Et3N, DMF] produced a mixture of the unstable [3]dendralene 13 and allylidenecyclopropane ...
Synthesis and characterization of poly(2-hydroxyethyl methacrylate/itaconic acid) copolymeric hydrogels
(Springer, New York, 2009)
In the present study poly(2-hydroxyethyl methacrylate-co-itaconic acid) (P(HEMA/IA)) hydrogels were synthesized by free-radical copolymerization of 2-hydroxyethyl methacrylate and itaconic acid in order to evaluate as ...
An inverse gas chromatography study of macroporous copolymers based on methyl and glycidyl methacrylate
(Elsevier, Amsterdam, 2000)
Adsorption properties of two laboratory synthesized macroporous copolymers based on methyl and glycidyl methacrylate were investigated by inverse gas chromatography. Retentions of 12 organic compounds were measured in the ...
Comparative studies of chloride and chloride/citrate based electrolytes for zinc-polyaniline batteries
(Pergamon-Elsevier Science Ltd, Oxford, 2006)
Electrochemical behavior of zinc and thin polyaniline (PANI) polymerized from 0.1 M HCl to 0.1 M aniline on graphite electrode, in 0.2 M ZnCl(2) and 0.50 M NH(4)Cl (chloride electrolyte) and with addition of 0.33 M Na-citrate ...
Electrodeposition and characterization of Zn-Ni alloys as sublayers for epoxy coating deposition
(Springer, Dordrecht, 2001)
The chemical composition and phase structure of Zn-Ni alloys obtained by electrodeposition under various conditions were investigated. The influence of the deposition solution and deposition current density on the composition, ...
Thermal properties of PS/TiO2 nanocomposites obtained by in situ bulk radical polymerization of styrene
(Elsevier Science Bv, Amsterdam, 2009)
TiO2 nanoparticles. surface modified with 6-palmitate ascorbic acid, were incorporated in polystyrene (PS) by in situ bulk radical polymerization of styrene using 2,2'-azobisisobutyronitrile as initiator. The molar mass ...
Non-isothermal crystallization of k2o center dot tio2 center dot 3geo(2) glass
(Springer, Dordrecht, 2009)
The crystallization of K2O center dot TiO2 center dot 3GeO(2) glass under non-isothermal condition was studied. In powdered glass with particle sizes less than 0.15 mm, surface crystallization was dominant and an activation ...
Identification of adsorption kinetics with dual mechanisms by nonlinear frequency response method
(Wiley-VCH Verlag Gmbh, Weinheim, 2001)
A characteristic example of the inability of the classical linear frequency response (FR) method to identify the correct kinetic mechanism is adsorption of n-hexane on silicalite-1. The linear FR has resulted in bimodal ...
A comparative study of the electrochemical properties of carbon nanotubes and carbon black
(Elsevier Science Sa, Lausanne, 2009)
Two samples of commercial multi-walled carbon nanotubes (Sigma-Aldrich and Sun Nanotech) and a sample of carbon black (Vulcan XC-72R) were investigated in raw state and after the activation in nitric and sulfuric acid by ...
Determination of selected pesticides in fruit juices by matrix solid-phase dispersion and liquid chromatography-tandem mass spectrometry
(Elsevier Sci Ltd, Oxford, 2009)
A rapid and sensitive liquid chromatography-tandem mass spectrometry method has been developed for the analysis of acephate, monocrotophos, carbendazim, acetamiprid, dimethoate, simazine, carbofuran, atrazine, diuron, DNOC ...